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高导电H_3PMo_(12)O_(40)掺杂聚苯胺微米棒的合成与表征 被引量:8

Synthesis and characterization of high conducting PAn doped with H_3PMo_(12)O_(40)
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摘要 分别以静电纺丝法制备的H3PMo12O40/PVA和纯H3PMo12O40微米管为模板,制备了H3PMo12O40掺杂的聚苯胺微米棒材料,并运用红外光谱、X射线粉末衍射和扫描电镜进行了表征.四探针法测定了产品的电导率.结果表明:聚苯胺微米棒的直径在400 nm左右;最高电导率为3.3 S/cm. H3PMo12O40/PVA and pure H3PMo12O40 microtubes template method synthesized PAn microrods doped with H3PMo12O40, respectively. The PAn microrods were characterized by IR, XRD spectra and SEM photographs. The conductivity of the materials was investigated by a standard four - point probe method. All results showed that the average diameter of the PAn mlcrorods was 400 nm and the highest conductivity of the PAn microrods was 3.3 S/cm.
出处 《东北师大学报(自然科学版)》 CAS CSCD 北大核心 2005年第3期41-44,共4页 Journal of Northeast Normal University(Natural Science Edition)
基金 教育部归国留学基金资助项目(2003406) 吉林省自然科学基金资助项目(20030505-4)
关键词 模板 聚苯胺微米棒 杂多酸 电导率 template PAn microrods heteropoly conductivity
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参考文献12

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