摘要
建立了RP-HPLC法测定克乳痛胶囊中丹皮酚和芍药甙的含量,均用十八烷基硅烷键合硅胶为固定相;前者以甲醇-醋酸-水(58240)为流动相,检测波长为274nm;后者以乙腈-水(2080)为流动相,检测波长为243nm。本法简便、快速、重现性好。
A RP HPLC method was described for the determination of paeonol in Kerutong Capsules. The paeonol was separated on a Resolve ODS C 18 column, using methanol HAc H 2O(58∶2∶40) as the mobile phase and detected at 274 nm. Another RP HPLC method was described for the determination of paeoniflorin in Kerutong Capsules. The paeoniflorin was separated on a Resolve ODS C 18 column, using acetonitrile H 2O(80∶20) as the mobile phase and detected at 243 nm.
出处
《中国药科大学学报》
CAS
CSCD
北大核心
1999年第2期119-120,共2页
Journal of China Pharmaceutical University