摘要
[目的]研究镰形棘豆(Oxytropis falcataBunge)的化学成分。[方法]应用正、反相硅胶柱色谱法进行分离纯化,根据理化性质和波谱数据鉴定化合物结构。[结果]从镰形棘豆95%乙醇提取物中分离得到了8种化合物,分别鉴定为β-谷甾醇(1)、柚皮素(2)、5,6-二羟基-2,7,3′,4′-四甲氧基黄酮醇(3)、5,6-二羟基-2,7,4′-三甲氧基黄酮醇(4)、3′,4′,5,7-四羟基双氢黄酮(5)、黄芹素(6)、7α-hydrox-ysitosterol(7)、7-oxositosterol(8)。[结论]化合物28为首次从该植物中分离得到。
[Objective] To study the chemical constituents of the whole plant of Oxytropis falcata Bunge.[Method] The chemical constituents were isolated by the column chromatography of silica gel and RP-18 gel.Their chemical structures were elucidated on the basis of physicochemical properties and spectral data analysis.[Result] 8 compounds were obtained and identified as β-sitosterol(1),naringenin(2),5,6-dihydroxy-3,7,3',4'-tetramethoxyflavonol(3),5,6-dihydroxy-3,7,4'-trmiethoxyflavonol(4),3',4',5,7-4-hydroxy-flavanone(5),apigenin(6),7a-hydroxysitosterol(7),7-oxositosterol(8).[Conclusion] Compounds 2-8 were isolated from the plant for the first time.
出处
《安徽农业科学》
CAS
北大核心
2010年第26期14340-14341,14344,共3页
Journal of Anhui Agricultural Sciences
关键词
镰形棘豆
化学成分
Oxytropis falcata Bunge; Chemical constituents;