摘要
以间苯二甲酸二甲酯为起始原料,经酰肼化、关环和硫醚化反应合成了8个新型的1,3-双(2-取代硫醚-1,3,4-噁二唑-5-基)苯,其结构经1H NMR,MS和元素分析表征。初步的生物活性测试结果表明,部分化合物具有较好的杀菌活性。
Eight novel 1,3-bis（2-alkylthio-1,3,4-oxadiazole-5-yl）phenylenes were synthesized from dimethyl m-phthalate by the reaction of hydrazidation,cyclization and thioetherification.The structures were charactrerized by 1H NMR,MS and elemental analysis.Preliminary bioassay indicated that some of them exhibited excellent fungicidal activities.
出处
《合成化学》
CAS
CSCD
北大核心
2010年第4期473-475,489,共4页
Chinese Journal of Synthetic Chemistry
基金
湖北省教育厅自然科学基金资助项目(D20086001)
