摘要
利用3种双酯型乌头碱(乌头碱、新乌头碱、次乌头碱)经水解得到3种乌头碱型生物原碱,即乌头原碱、新乌头原碱、次乌头原碱.应用一维和二维核磁共振(NMR,包括1H-1HCOSY,HMQC和HMBC)对这3种化合物的结构进行了分析,并对其1H和13C化学位移进行了全归属.
Three aconines：aconine,mesaconine,hypaconine were separated from the hydrolyzates of three diester-diterpenoid aconines aconitine,mesaconitine and hypaconitine.1H and 13 C NMR spectra（including 1 H-1 H COSY,HMQC and HMBC） of the compounds were acquired and assigned.The structures of the compounds were elucidated.The chemical shift assignments of 1H and 13C were made.
出处
《吉林大学学报（理学版）》
CAS
CSCD
北大核心
2010年第1期127-132,共6页
Journal of Jilin University:Science Edition
基金
国家"十一五"技术支撑计划项目(批准号:2006BAI14B01)
