摘要
目的对周氏克金岩方有效部位Ⅰ的成分进行定性定量分析,为深入研究周氏克金岩方抗肺癌有效部位群物质基础奠定基础。方法通过试管反应和TLC方法定性鉴别有效部位成分,建立亚硝酸钠-硝酸铝比色法测定总黄酮含量、香兰素-冰醋酸-高氯酸比色法测定总皂苷的含量。结果周氏克金岩方有效部位Ⅰ中主要含黄酮、皂苷类成分,含量分别为0.85%、 1.07%,纯度分别为29.7%、 37.4%。结论周氏克金岩方有效部位Ⅰ中主要含有黄酮和皂苷类成分,总纯度为67.1%。
Objective To study material basis of Zhou＇s prescription, components of effective parts I in Zhou＇s prescription was gualitative and quantitative analyzed. Methods The components of effective part I was identified by test-tube reaction and qualitative TLC method, the content of saponins and flavones was quantitative analyzed. Results Total content of the saponins and flavone are 1.07% and 0.85% in Zhou＇s Prescription. The purity of saponins and flavones in effective parts I are 37.4% and 29.7%. Conclusion The main components of effective part I in Zhou＇s Prescription were flavones and saponins.
出处
《中国中医药信息杂志》
CAS
CSCD
2009年第11期38-40,共3页
Chinese Journal of Information on Traditional Chinese Medicine
基金
国家"十一五"科技支撑计划(2006BA I 11B08-1)
关键词
周氏克金岩方
定性鉴别
黄酮
皂苷
Zhou＇sprescription
qualitative identification
saponins
flavones
