摘要
目的：为建立黄麦合剂的质量标准进行相关研究。方法：采用薄层鉴别法对处方中制何首乌、黄芪进行了鉴别,用HPLC法测定了制何首乌中二苯乙烯苷的含量。结果：薄层鉴别检出制何首乌、黄芪;二苯乙烯苷浓度在6.25-200μg/mL范围内与峰面积呈良好线性关系（r=0.999 7）,平均回收率为100.4%,RSD为1.40%。结论：本法专属性强、重现性好,适用于该制剂的质量控制。
Objective： To perform a relative study for establishing the quality standard of Huangmai mixture. Methods： Radix Polygoni Multiflori Praeparata Cure Sueco Glycines Sotae and Radix Astragali were identified by TLC method. Stilbene glucoside in Radix Polygoni Multiflori Praeparata Cum Suceo Glyeines Sotae was determined by HPLC method. Results.. Radix Polygoni Multiflori Praeparata Cum Sueco Glycines Sotae and Radix Astragali could be detected by TLC method. Stilbene glueoside showed a good linear relationship with peak area in the range of 6.25-200 μg/mL （r=0. 999 7）. The average recovery was 100.4% and RSD was 1.40%. Conclusion： The method is feasible with good specificity and reproducibility and can be used for quality control of Huangmai mixture.
出处
《药学服务与研究》
CAS
CSCD
2009年第4期289-291,共3页
Pharmaceutical Care and Research
基金
上海申康医院发展中心"市级医院中医药验方临床评价"项目(No.SHDC12007414)
关键词
黄麦合剂
制何首乌
黄芪
二苯乙烯苷
色谱法
薄层
色谱法
高压液相
Huangmai mixture
Radix Polygoni Multiflori Praeparata Cum Succo Glycines Sotae
Radix Astragali
stilbene glucoside
chromatography, thin layer
chromatography, high pressure liquid
