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喷雾干燥过程条件对HNS微粉化形貌的影响 被引量:8

The Influence of Conditions in Spray Drying Process on Morphology of Micronization HNS
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摘要 采用喷雾干燥法对HNS炸药进行了微粉化,研究了不同入口温度、溶液浓度、泵速率对颗粒形貌的影响。结果表明,随着入口温度的降低,颗粒表面逐渐出现大的裂缝;当浓度过大,颗粒尺寸增大,而浓度过小颗粒表面裂缝增大。泵速率对颗粒形貌影响较小,但颗粒尺寸随泵速度的其增加而增加。建立了HNS喷雾干燥的结晶模型,并验证了模型的正确性。 HNS explosive was micronized by spray drying process. The influence of factors such as different entrance temperature, solution concentration and pump velocity on the particles' morphology were investigated. The results indicate that the surface of the particles will gradually appear large crack with increasing of entrance temperature. While for too large solution concentration, the particle size will become larger. The surface crack will augment if the solution concentration is too little. The pump velocity has little effect on the particle morphology. However, it was shown that an increase in the pump velocity results in a significant increase in particle size. The experimental results will establish foundation for preparation of micronized HNS. Crystallization model of HNS in spray drying process was established and validated.
出处 《火炸药学报》 EI CAS CSCD 2008年第5期5-8,共4页 Chinese Journal of Explosives & Propellants
关键词 材料科学 喷雾干燥 HNS 微粉化 形貌 结晶模型 materials science spray drying HNS micronization morphology crystallization model
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参考文献8

  • 1Stepanov V,Krasnoperov L N,Elkina I B,et al. Procluction of nanocrystalline RDX by rapid expansion of supercritical solutions [J]. Propellants, Explosives, Pyrotechnics, 2005,30:178-183.
  • 2Kim Y H, Lee K, Koo K K, et al. Comparison study of mixing effect on batch cooling crystallization of 3- nitro-1, 2, 4-triazol-5-one (NTO) using mechanical stirrer and ultrasound irradiation [J]. Cryst Res Techrlol,2002, 37(9): 928-944.
  • 3Muller D, Helfrich M. Spherical RDX of small par ticle size by spray drying [C]// Annual Meeting onEnergetic Materials for Munitions Proceedings. Mass:Camp Edwards, 1994 : 67-81.
  • 4张杰,杨荣杰,刘云飞,谭惠民.硝酸铵喷雾干燥表面改性[J].推进技术,2002,23(6):521-524. 被引量:6
  • 5杨光成,聂福德,曾贵玉.超细TATB-BTF核-壳型复合粒子的制备[J].火炸药学报,2005,28(2):72-74. 被引量:13
  • 6van der Heijden A E D M, Creyghton Y L M, Emanuela M, et al. Energetic materials: crystallization, characterization and insensitive plastic bonded explosives[ J]. Propellants, Explosives, Pyrotechnics,2008,33(1):25-32.
  • 7Russell R J. Modification of ballistic properties of HMX by spray drying: US, 4092383[P]. 1978.
  • 8Elversson J. Spray-dried powders for inhalation:particle formation and formulation concepts [D]. Uppsala: Uppsala University, 2005.

二级参考文献16

  • 1杜仕国,施冬梅,邓辉.偶联剂对硝酸铵的表面改性及其应用研究[J].飞航导弹,2000(11):47-49. 被引量:1
  • 2陈天云,刘祖亮,彭新华,陆明.硝酸铵防吸湿性研究[J].爆破器材,1994,23(5):30-33. 被引量:8
  • 3李君励,张惠坤.复合推进剂中使用的改性硝酸铵[J].推进技术,1994,15(1):58-64. 被引量:11
  • 4陈天云 吕春绪.表面活性剂和添加剂降低硝酸铵的吸湿性研究[J].火炸药学报,1998,(4):19-21.
  • 5殷永霞 杨荣杰.微胶囊技术在硝酸铵改性的应用研究[J].辽宁化工,2001,30(4):139-144.
  • 6张杰.硝酸铵表面改性技术研究[M].北京:北京理工大学,2000..
  • 7殷永霞.硝酸铵的包覆改性及表征[M].北京:北京理工大学,2001..
  • 8张付清 李凤生.亚铬酸铜/高氯酸铵超细复合粒子研究进展[J].化工新型材料,1999,27(5):3-3.
  • 9Honda H. Preparation of monolayer particle coated powder by the dry impact blending process utilizing mechanico-chemical treatment [J]. Physico-chemical and Engineering Aspects, 1994,(82):117-128.
  • 10董强,蒋若志,崔树民,董刚.硝化棉包覆硝酸铵的工艺研究[J].含能材料,1997,5(3):114-120. 被引量:8

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