摘要
介绍了超微盘电极、超微半扁球电极、超微半球电极的制备方法及其在电化学研究中的应用.测量表明,苯醌在 McIlvaine 缓冲溶液中超微电极上的还原行为与常规电极上不同.提出将超微电极与常规电极连用,研究电化学反应机理的方法.
The method for preparation of ultramierodisk electrode,ultramicro hemispheroid electrode and ultramicro hemispherical electrode is described.The applications of these electrodes in electrochemistry are also introduced.The difference for the electrochemical reduction of benzoquinone on ultramicroelectrode and normal electrode are researched.A method for researching the mechanism of electrode reaction by both using uhramicroelectrode and normal electrode is also proposed.
