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硝酸咪康唑制剂的气相色谱测定 被引量:1

GAS CHROMATOGRAPHY OF MICONAZOLE NITRATE CREAM AND INJECTION
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摘要 采用气相色谱法测定硝酸咪康唑霜剂和注射剂的含量。其平均回收率分别为97.7%和101.4%,RSD分别为2.2%和1.3%。方法快速、准确。 A gas chromatographic method for direct determination of miconazole nitrate cream and injection was developed. The conditions were:detector, FID; stationary phase, 5%SE 30; support, Chromosorb W (AW DMCS,80~100 mesh); packed column, 3 m×3 mm i.d.; column temperature, 275°C; injector temperature, 290°C; diisoocty1 sebacate as internal standard. The average recoveries of cream and injection were 97.7% and 101.4%, respectively. The RSD s were 2.2% and 1.3%, respectively.
出处 《中国医药工业杂志》 CAS CSCD 北大核心 1997年第10期454-455,共2页 Chinese Journal of Pharmaceuticals
关键词 气相色谱 硝酸咪康唑 霜剂 测定 抗真菌药 gas chromatography, miconazole nitrate, cream, injection, determination
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