摘要
目的:建立尿毒康合剂的质量控制方法。方法:采用薄层色谱法鉴别黄芪、大黄。用高效液相色谱法测定大黄中的大黄酚含量。结果:大黄酚在48～132μg范围内线性关系良好(r=0.9996),平均回收率为97.54%,RSD为3.67%。结论:本方法操作简便,结果可靠,重现性好,可作为尿毒康合剂的质量控制方法。
Objective ： Establish a method for the quality control of Niaodukang mixture. Methods ： RadixAstragali, Radix et Rhizoma Rheii, Radix Salviae mitiorrh izae were identified by TLC. Chrysophanol was determined by the method of HPLC. Results ：The quantification method had the linearrange of 48 - 132μg and the linearity relation was fine（ r = 0.99963 ）. The average recovery was 100.89% and its RSD was 3.67%. Conclusion ：The quality standard of the mixture was provided. The methods for identification and quantification were simple, reproducible and realizable. It was the quality control method of the niaodukang mixture.
出处
《中华中医药学刊》
CAS
2008年第3期593-595,共3页
Chinese Archives of Traditional Chinese Medicine
基金
中山市科技计划项目基金资助项目(2005A117)
