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百部总生物碱含量测定方法的研究 被引量:3

Study on the Assay of Total Alkaloids from Stemona tuberosa Lour.
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摘要 分别运用酸碱滴定法和雷氏盐吸收系数法对百部中总生物碱的含量进行了测定,并加以比较。结果表明:雷氏盐吸收系数法的测定结果比酸碱滴定法的测定结果稍高,提取步骤少,操作简单,更能最大限度的减少干扰因素的影响,方法学考察均符合规定,可以用来测定百部总碱的含量. The comparison was made between the acid-base titration and Reinecke salt UV method which were used to determine the content of total alkaloids from Stemona tuberosa Lour.. The result suggested that the Reinecke salt UV method was better than acid-base titration in higher yields ,fewer and more simple process. It can reduce the influence of interfere to the maximum and be suitable to determine the assay of total alkaloids.
机构地区 广州中医药大学
出处 《天然产物研究与开发》 CAS CSCD 2007年第B05期124-126,共3页 Natural Product Research and Development
关键词 百部 总生物碱 酸碱滴定法 雷氏盐比色法 Stemona tuberosa Lour. total alkaloids acid-base titration reinecke salt UV method
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  • 2Xu GJ(徐国钧).Variety and Quality Study of Chinese Herbs in Common Use, Vol 2(常用中药材品种整理和质量研究).Fuzhou : Fujiang Science & Technology Press, 1997.85.
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