摘要
采用超声波提取技术，用正己烷提取氧化塘出水中己二酸二（2-乙基己基）酯增塑剂，以气相色谱／质谱联用选择离子监测法检测，外标法定量。对己二酸二（2-乙基己基）酯的检出限为0.4μg·L^-1（S／N=3）；回收率为90％～95％，相对标准偏差为5．02％。该方法简便、快速、准确，适用于氧化塘出水中己二酸二（2-乙基己基）酯的测定。
The di （2 - ethyl hexyl ）adipate （DEHA） in oxidation pond water was extracted by hexane with ultrasonic generator. The determination of Di （2 - ethyl hexyl） Adipate was carried out by gas chromatography/mass with selected ion monitoring （SIM） mode, using external standard method. The detection limit of DEHA was 0. 4μg·L^-1（ S/N = 3 ）, recoveries were in the range of 90% - 95% , the RSD were in the range of 0. 12% -0. 28%. This method was of simple, fast, accurate which was suitable to the determination of Di （2 -ethyl hexyl） Adipate in Oxidation pond water.
出处
《化学工程师》
CAS
2008年第1期24-25,共2页
Chemical Engineer
