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镧化合物催化合成醋酸异戊酯

A Study on Derivative UV-Spectrophotometric Method of Benzyl Alcohol and Benzaldehyde in Benzyl Alcohol Injection
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摘要 考察了含镧化合物(La2O3、LaCl3、La-Y型分子筛)对醋酸异戊酯合成的催化活性,实验结果表明:三者的活性顺序为La-Y型分子筛>LaCl3>La2O3.La-Y型分子筛具有稳定的重复催化活性. A method was proposed for determination of benzyl alcohol in benzyl alcohol injection by the fouth order derivative UV-spectrophotometry.Benzaldehyde did not interfere with the determination of benzyl alcohol,when the concentration of benzaldehyde was less than 16 0 μg/ml.The calibration curve is linear in the concentration range of 180~400 μg/ml,and the relative standard derivation is less than 0 5%.The recovery of standard addition is from 99% to 101%.
机构地区 河南大学化学系
出处 《河南大学学报(自然科学版)》 CAS 1997年第2期47-50,共4页 Journal of Henan University:Natural Science
关键词 催化 分子筛 醋酸异戊酯 催化合成 derivative spectrophotometry benzyl alcohol benzaldehyde
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