摘要
采用反复的硅胶柱色谱进行分离、纯化,根据理化性质和波谱数据进行结构鉴定。从番泻叶中分离鉴定了8个化合物:Tinnevellin glycoside(Ⅰ)、异鼠李素-3-O-β-龙胆二糖苷(Ⅱ)、芹菜素-6,8-二-C-葡萄糖苷(Ⅲ)、大黄素-8-O-β-D-吡喃葡萄糖苷(Ⅳ)、山柰酚(Ⅴ)、芦荟大黄素(Ⅵ)、D-3-O-甲基肌醇(Ⅶ)、蔗糖(Ⅷ)。结论:化合物Ⅲ、Ⅶ、Ⅷ为首次从该植物中分离得到。
Objective ： To study the chemical constituents from the leaves of Cassia angustifolia. Methods ： Compounds were isolated and repeatedly purified by chromatographic techniques on silica gel column. Their structures were elucidated by chemical and spectral methods. Results： eight compounds were isolated from the leaves of Cassia angustifolia, and identified as tinnevellin glycoside（ Ⅰ ）, isorhamnetin-3-O-β-gentiobioside（ Ⅱ ）, apigenin-6,8-di-C-glycoside（ Ⅲ）, emodin-8-O-β-D-glucopyranoside（ Ⅳ ） , kaempferol（ Ⅴ ）, aloe emodin（ Ⅵ ） , D-3-O-methylinositol（ Ⅶ ） , sucrose（Ⅷ）. Conclusion：Compounds Ⅲ, Ⅶ and Ⅷ are isolated from the plant for the first time.
出处
《中药材》
CAS
CSCD
北大核心
2007年第10期1250-1252,共3页
Journal of Chinese Medicinal Materials
关键词
番泻叶
化学成分
Cassia angustifolia Vahl.
Chemical constituents
