摘要
以异丁醇和乙炔作为原料,在醇钾盐催化剂的作用下,在一定的反应温度和反应压力下合成了异丁基乙烯基醚,并进行了分离与提纯。同时对产物用红外光谱、质谱及气相色谱分析进行了表征。讨论了催化剂、反应温度、反应压力等对产率与纯度的影响。
Acetylene reacted with isobutal to give isobutal vinyl ether at certain temperature and pressure. The product was purified and characterized by gas chromatography, mass spectrograph and infrared spectroscopy. The effect of catalyst,reaction temperature,reaction pressure on conversion and purity of isobutal vinyl ether was discussed.
出处
《浙江化工》
CAS
2006年第12期1-3,20,共4页
Zhejiang Chemical Industry
关键词
异丁基乙烯基醚
醇钾盐
异丁醇
乙炔法
isobutal vinyl ether
potassium alkoxide
isobutal
acetylene
