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球形α-Fe_2O_3纳米粉体的超声水解法合成与表征 被引量:7

Synthesis and Characterization of Spherical Hematite (α-Fe_2O_3) Nanopowder by Sonochemical Hydrolysis Method
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摘要 Hematite (α-Fe2O3) nanopowder was synthesized from 0.1 mol·L-1 FeCl3 solution by sonochemical hydrolysis method, and characterized by X-ray diffraction (XRD), transmission electron micrograph (TEM), Fourier transform infrared (FTIR), Fourier transform Raman (FT-Raman) and X-ray photoelectron spectroscopy (XPS). The results showed that the spherical, well-dispersed α-Fe2O3 nanopowder was obtained with the average size of 20 nm. The possible mechanism for the formation of α-Fe2O3 nanoparticals was also discussed. Hematite (a-Fe2O3) nanopowder was synthesized from 0.1 mol-L-1 FeCl3 solution by sonochemical hydrolysis method, and characterized by X-ray diffraction (XRD), transmission electron micrograph (TEM), Fourier transform infrared (FTIR), Fourier transform Raman (FT-Raman) and X-ray photoelectron spectroscopy (XPS). The results showed that the spherical, well-dispersed a-Fe2O3 nanopowder was obtained with the average size of 20 nm. The possible mechanism for the formation of a-Fe2O3 nanoparticals was also discussed.
出处 《无机化学学报》 SCIE CAS CSCD 北大核心 2006年第7期1317-1320,共4页 Chinese Journal of Inorganic Chemistry
基金 国家自然科学基金项目(No.20471048) 陕西省教育厅科研计划项目(No.05JK033) 陕西省高校省级重点实验室重点科研基金项目(No.05JS38)资助
关键词 超声水解 a-Fe2O3 纳米粉体 sonochemical hydrolysis a-Fe2O3 nanopowder
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