摘要
本文报道了使用杂多酸(钨硅酸)作催化剂液相合成己酸烯丙酯的结果。考察了催化剂用量、反应时间、醇酸比和带水剂量的影响。得到了合成该酯的适宜条件。在此条件下,其酯化率为96.1%,产物收率为89.4%。
Heteropoly acid(tungstosilicic acid)was used as homogeneous catalyst for the esterification of allyl caproate. Effects of the amount of the catalyst, the reaction time, the ratio of reactants and the amount of an agent which taking of water were investigated. A suitable condition for synthesizihg the ester was obtained. The esterification was 96.1%. Under the optimum condition,the yield of allyl caproate could reach 89.4%.
出处
《化学与粘合》
CAS
1996年第2期70-71,共2页
Chemistry and Adhesion
基金
辽宁省科委基金资助课题
