摘要
[目的]制定痛风止痛涂膜剂的质量标准,使其具有较好的质量可控性。[方法]以大黄对照药材为对照品,以苯-乙酸乙酯-甲酸-甲醇-水(30∶10∶0.5∶2∶5)的上层溶液为展开剂进行薄层色谱鉴别,并按有关规定进行常规检验。[结果]供试品(痛风止痛涂膜剂)色谱中,在与对照药材色谱相应的位置上,显相同颜色的斑点,阴性对照液无干扰;其他各检查项均符合相关规定。[结论]该方法简单易行、重现性好,可作为痛风止痛涂膜剂质量控制标准。
[Objective] To institute the quality criteria on arthrolithiasis odynolysis plastics and make a better quality controllability. [Methods] The rhubarb was control article in the experiment. The developing agent was upper stratum solution of which comprised of benzeneaeetidin-formic acid-methanol-water. To made an identify by thin layer chromatography （TLC） method and carry out routine analysis according to related regulation. [Results] The colourspectrum sponding of arthrolithiasis odynolysis plastics showed up identical colour speckle in corre- position with colour spectrum of control article. The negative control solution was non-interference and all the examination fitted with correlated regulation. [Conclusion] The method was simple, reasonable and owned a good reproducibility. The method may become the quality criteria of arthrolithiasis odynolysis plastics.
出处
《天津中医学院学报》
2005年第3期129-130,共2页
Journal of Tianjin College of Traditional Chinese Medicine
关键词
痛风止痛涂膜剂
质量标准
薄层鉴别
arthrolithiasis odynolysis plastics
quality criteria
lamella identify
