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紫外分光光度法测定注射用双半胱氨酸中双半胱氨酸含量 被引量:1

Determination of Content of Ethylenedicysteine in L,L-Ethylene Dicysteine for Injection by UV Spectrophotometry
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摘要 目的:建立注射用双半胱氨酸药盒中双半胱氨酸的含量测定方法。方法:采用紫外分光光度法,UV 检测波长为230nm。结果:该法线性范围为0~30μg·mL^(-1);平均回收率99.4%,RsD=0.9%,n=7。结论:该法简便可行,结果稳定,可用于对药盒的质控。 Objective:To establish an ultraviolet spectrophotometry method for the determination of ethylenedicysteine in ethylenedicysteine for injection. Method : The UV spectrophotometry is based on absorption of the sample itself. The wavelength of detection was 230 nm. Result: The calibration curve of ethylenedicysteine was linear ( r = 0. 9999)over the range of 0 -30 μg ·mL^-1. The mean recovery was 99.4% and RSD =0. 9% (n =7). Conclusion: This method is simple and easy to do. It may be adopted for quality control of this drug.
出处 《药物分析杂志》 CAS CSCD 北大核心 2005年第8期988-989,共2页 Chinese Journal of Pharmaceutical Analysis
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