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柔毛路边青挥发性成分研究 被引量:13

Studies on the Chemical Constituents of the Volatile Oil from Herba gei
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摘要 目的:研究柔毛路边青(Herba gei)挥发油成分,为有效控制中成药蓝止安脑胶囊质量及中药二次开发提供理论依据。方法:利用水蒸气蒸馏法提取柔毛路边青挥发油,用GC/MS进行分离测定,结合计算机检索技术对分离的化合物进行结构鉴定,应用色谱峰面积归一化法计算各成分的相对百分含量。结果:分离出59个成分,确定了43个化合物,占挥发油总量的87.51%。结论:柔毛路边青挥发油成分大于5%的为α-蒎烯10.73%,松金娘烷醇13.63%,松金娘烯醛7.19%,松金娘烯醇5.03%,二环[3,1,1,]-6,6-二甲基-3-亚甲基庚烷6.83%,丁子香酚15.82%。其中含量最高的物质为丁子香酚。 Objective:To study the chemical constituents of the volatile oil from Herba gei and give essential numbers for controlling quality and studies.Methods:The oil was obtained by steam distillation.The chemical compositions were separated and identified by GC/MS.The relative contents in the oil were determined by are a nomalization.Results:Fifty-nine components were detected in the volatile constituents of Caulis Lonicerae.;of which forty-three components representing 87.51% of the oil were characterized.Conclusion:The major constituents are α-pinene 10.73%,myrtanal 13.63%,myrtenal 7.19%,myrtenol 5.03%,bicydo[3,1,1]heptane,6,6-dimethyl-3-methylene 6.83%,eugenol 15.82%.The highest content in the oil is eugenol.
出处 《生物技术》 CAS CSCD 2005年第2期52-54,共3页 Biotechnology
基金 贵州省跨世纪科技人才工程专项资金资助项目["贵州生物技术制药产业前期研究" 黔科合人专字(2000)9816号]
关键词 柔毛路边青 水蒸气蒸馏 挥发油 气相色谱-质谱联用 Herba gei steam distillation volatile oil GC/MS
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参考文献3

  • 1贵州省医药监督管理局.贵州省中药材、民族药材质量标准[S].贵州:贵州科技出版社,2003.387.
  • 2江苏新医学院.中药大词典(上册)[M].上海:上海科学技术出版社,1986.1751.
  • 3.国家中成药标准汇编(内科心系分册)[S].[S].国家药品监督管理局,2002.65.

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