摘要
毛细管气相色谱法测定果蔬中20种有机磷农药残留量庄无忌周昱(中国商检技术研究所北京100025)(厦门商检局厦门361012)1前言食品中多种有机磷农药残留量的测定国外已有报道 ̄[1~4],国内也正在开展此项工作。李聪等 ̄[5]曾报道了低脂肪样品中1...
method for the determination of 20 organophosphorus pesticide residues in fruits and vegetables hasbeen developed. Determination of pesticides was performed by GC,FPD using a BPI0 capillary column,Theextraction solvent was ethyl acetate. The RC and CV ranges were 80.5~112.6%and 2.0~14. 5%respec-tively. The detection linlit range was 0.2~40μg/kg Since we use the split/splitless injector of the EPP tocontroI the carrier gas, a good separation within 40min for the 20 organophosphorus pesticides has been ob-tained.
出处
《色谱》
CAS
CSCD
北大核心
1994年第3期202-203,共2页
Chinese Journal of Chromatography
关键词
水果
蔬菜
有机磷农药
残留量
色谱
gas chromatography, organophosphorus pesticides,orange,pesticide residues analysis