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麒麟丸调控CYP11A1/testosterone/CYP19A1/E2/ESR1通路治疗雷公藤多苷诱导的大鼠少弱精子症 被引量:2
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作者 刘嘉 王春玲 +4 位作者 陈栢皓 徐玉蓉 贾亚旭 林翠萍 黄丽丽 《药物评价研究》 北大核心 2025年第2期439-447,共9页
目的探究麒麟丸治疗少弱精子症(AS)的作用机制。方法SD大鼠随机分为对照组、模型组、左卡尼汀(阳性药,100 mg·kg^(-1))和麒麟丸低、高剂量(0.5、1.5 mg·kg^(-1))组,除对照组外,其余4组ig给予雷公藤多苷35 mg·kg^(-1)7 d... 目的探究麒麟丸治疗少弱精子症(AS)的作用机制。方法SD大鼠随机分为对照组、模型组、左卡尼汀(阳性药,100 mg·kg^(-1))和麒麟丸低、高剂量(0.5、1.5 mg·kg^(-1))组,除对照组外,其余4组ig给予雷公藤多苷35 mg·kg^(-1)7 d诱导AS模型,从造模开始即给药,每天1次,共ig给药21 d。称量睾丸和附睾组织质量,计算大鼠生殖器官指数;通过精子参数检测系统检测各组动物的精子质量和精子形态;ELISA测定大鼠血清中性激素含量;HE染色观察给药后各组大鼠睾丸组织病理学改变,并统计生精细胞和间质细胞数量;通过免疫荧光染色检测大鼠睾丸组织中支持细胞数量;Western blotting和实时荧光定量PCR(qRT-PCR)法检测细胞色素P450家族19亚家族A成员1(CYP19A1)、细胞色素P450家族11亚家族A成员1(CYP11A1)和雌激素受体α(ESR1)的蛋白和基因表达水平。结果与对照组相比,模型组精子质量和血清睾酮(T)、雌二醇(E2)含量显著降低(P<0.01),血清黄体生成素(LH)含量显著升高(P<0.01),生殖器官指数和睾丸生精细胞、间质细胞和支持细胞数量显著降低(P<0.01),睾丸组织性激素合成限速酶CYP11A1和CYP19A1、ESR1的基因和蛋白显著下调(P<0.01);与模型组相比,麒麟丸高剂量组精子质量和血清T、E2含量显著增加(P<0.01),血清LH含量显著降低(P<0.01),生殖器官指数、睾丸生精细胞、间质细胞和支持细胞数量显著升高(P<0.01),CYP11A1和CYP19A1、ESR1基因和蛋白显著上调(P<0.01)。结论麒麟丸可通过上调性激素合成限速酶CYP11A1和CYP19A1,上调体内性激素表达治疗AS。 展开更多
关键词 麒麟丸 少弱精子症 CYP11A1 CYP19A1 雌激素受体Α 性激素 睾酮 雌二醇 黄体生成素 精子质量
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Discussion on Practical Strategies of Quality Control Technology for Energy Efficiency Testing of Electronic and Electrical Products
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作者 Xianfu Wang 《Journal of Electronic Research and Application》 2025年第4期178-183,共6页
In the current social environment,the importance of energy conservation and emission reduction is increasing day by day for both the country and its people.Electronic and electrical products,as important items for peo... In the current social environment,the importance of energy conservation and emission reduction is increasing day by day for both the country and its people.Electronic and electrical products,as important items for people’s production and life,require high attention from industry insiders in terms of their energy efficiency testing.Relying on energy efficiency testing can achieve the goal of energy conservation and emission reduction,and related quality control technologies will also inject new momentum into the green development of the industry.This article will discuss the practical strategies of quality control technology for energy efficiency testing of electronic and electrical products based on the significance of such testing,hoping to provide some help. 展开更多
关键词 Electronics and electrical appliances Product energy efficiency testing Testing significance Quality control technology Practical strategies
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Research of NOx Sensors Performance Test
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作者 Zhengang Zhang Zhonggang Tang +3 位作者 Wei Gao Li Liu Cong Wang Hourui Sun 《Journal of Materials Science and Chemical Engineering》 2025年第2期23-30,共8页
NOx sensors, as a core component of diesel engine exhaust treatment system, play an important role in exhaust emission control, which can accurately and quickly detect the NOx and O2 concentration. It has become a nec... NOx sensors, as a core component of diesel engine exhaust treatment system, play an important role in exhaust emission control, which can accurately and quickly detect the NOx and O2 concentration. It has become a necessary option for the detection of existing exhaust emission standards. At present, there is limited and scattered information on knowledge and test methods of NOx sensors, the research of NOx sensors has become a challenging research topic at home and abroad. Based on these requirements, the article systematically integrates the knowledge of principle and testing methods. First of all, through introducing functional description of NOx sensors and the basic principle of NOx sensors, the relevant scholars can have an overall understanding of the product and master the operation mode of products. Secondly, the current status of performance test bench and methods of NOx sensors were described, which can contribute to having a clear understanding of the development process. After that, a new structure of NOx sensors test bench was purposed, which contains six major units including standard gas source, gas mixing unit, analyzer measurement unit, sensor measurement unit, data processing and display unit, exhaust gas treatment unit. And the test bench was validated. The experimental results show that the test bench has the advantages of high-repeatability, high reliability and low cost. And it can realize automatic detection of multiple target values, which is worthy further promotion. Thereby, the article can contribute to the development of its technology indirectly. 展开更多
关键词 NOx Sensors FUNCTION Performance Test Basic Principle
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Application Strategy of Ultrasonic Nondestructive Testing Technology in Bridge Engineering
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作者 Shulin Tan Xu Meng +1 位作者 Lei Chen Zhi Tu 《Journal of Architectural Research and Development》 2025年第3期111-117,共7页
The purpose of this study is to analyze the application of ultrasonic non-destructive testing technology in bridge engineering.During the research phase,based on literature collection and reading,as well as the analys... The purpose of this study is to analyze the application of ultrasonic non-destructive testing technology in bridge engineering.During the research phase,based on literature collection and reading,as well as the analysis of bridge inspection materials,the principle of ultrasonic non-destructive testing technology and its adaptability to bridge engineering are elaborated.Subsequently,starting from the preparation work before inspection until damage assessment,the entire process of ultrasonic non-destructive testing is studied,and finally,a technical system of ultrasonic non-destructive testing for bridge engineering that runs through the entire process is formed.It is hoped that this article can provide technical reference value for relevant units in China,and promote the high-quality development of China’s bridge engineering from a macro perspective. 展开更多
关键词 ULTRASONIC Bridge engineering Non-destructive testing Signal filtering
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Smartphone-assisted electrochemiluminescence imaging test strips towards dual-signal visualized and sensitive monitoring of aflatoxin B1 in corn samples
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作者 Miao-Miao Chen Min-Ling Zhang +5 位作者 Xiao Song Jun Jiang Xiaoqian Tang Qi Zhang Xiuhua Zhang Peiwu Li 《Chinese Chemical Letters》 2025年第1期464-468,共5页
Aflatoxins B1(AFB1)contamination in agro-food holds great threaten to human and animal health.Conventional test strips for rapid AFB1 visualized monitoring remains challenged by improvement of sensitivity and matrix i... Aflatoxins B1(AFB1)contamination in agro-food holds great threaten to human and animal health.Conventional test strips for rapid AFB1 visualized monitoring remains challenged by improvement of sensitivity and matrix interference resistance.In this case,we developed a portable electrochemiluminescence(ECL)imaging test strip with dual-signal outputs for AFB1 quantification in corn samples.RuPEI@SiO_(2)@Au nanospheres were synthesized for bonding with anti-AFB1 antibody and then colorimetrical signal-reported on test line through the capillary flow at strips.Meanwhile,ECL imaging signal of the constructed carbon-ink-based working electrode on polyvinyl chloride substrate of strips was exported under an applied potential of 1.25 V.The whole ECL test strips not only endowed convenient colorimetric responses but guaranteed quick-witted ECL image distinguishment even at extremely low AFB1 content.The detection limit of this ECL imaging-integrated mode was 10-fold lower than that of only colorimetric mode.Furthermore,satisfactory selectivity,reliability and practicability of the as-proposed ECL test strips were demonstrated.This work offered a promising platform for on-site,accurate and sensitive detection of pollutants in foods. 展开更多
关键词 Electrochemiluminescence imaging Test strips Nanomaterials Dual-signal outputs Aflatoxin B1 Food safety
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Sensitivity of Commercial Enzyme Inhibition Colorimetric Pesticide Residue Rapid Test Kit to a Variety of Pesticides
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作者 Junxia LUO Qianqian ZHAO +4 位作者 Lumei DUAN Yanzhen LI Huifang QIAO Zhipei DOU Jianbo ZHAO 《Asian Agricultural Research》 2024年第5期29-32,共4页
[Objectives]To fully understand the quality of commercial enzyme inhibition-colorimetric pesticide residue rapid detection kits,so that they can play a greater role in the detection and supervision of agricultural pro... [Objectives]To fully understand the quality of commercial enzyme inhibition-colorimetric pesticide residue rapid detection kits,so that they can play a greater role in the detection and supervision of agricultural products.[Methods]The sensitivity of 28 kinds of pesticides was determined by using the commercially available enzyme inhibition colorimetric rapid detection kit with Hendu brand.[Results]There was a significant difference in the sensitivity of the kit to each pesticide,and the kit was more sensitive to dichlorvos among the 28 pesticides tested.The sensitivity to methyl isosalifos,dimethoate,isocarbophos,fenthion and phorate was poor,and the sensitivity to quinalphos was different between 3.0 and 2.5 mL.[Conclusions]The large difference of the sensitivity of the enzyme inhibition-colorimetric rapid detection kit for pesticide residues to different kits is a reason for the false positive and false negative test results of the kit,which needs to be considered by relevant personnel. 展开更多
关键词 Enzyme inhibition-colorimetry Reagent kit PESTICIDE Inhibition rate Sensitivity
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Fracture mechanism of inclusions in thick plate center under tensile loading
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作者 Lei Hu Li-qin Zhang +2 位作者 Feng Hu Guo-hong Zhang Kuan Zheng 《Journal of Iron and Steel Research International》 SCIE EI CAS CSCD 2024年第5期1196-1209,共14页
Segregation of solute atoms in the center of thick plates of the tempered steel can cause an inhomogeneous structural transformation and generate micron-sized inclusions,which leads to lamellar tearing of thick plate ... Segregation of solute atoms in the center of thick plates of the tempered steel can cause an inhomogeneous structural transformation and generate micron-sized inclusions,which leads to lamellar tearing of thick plate and decreases the plasticity and toughness.The formation and fragmentation mechanisms of micron-sized inclusions,like MnS and(Nb,Ti)C,in the center of thick plates were investigated by using thermodynamic calculations,finite element simulations,and electron backscatter diffraction characterization techniques.The results show that micron-sized inclusions nucleate and grow in the liquid phase,and under tensile loading,they exhibit three fragmentation mechanisms.The local stress during the fragmentation of inclusions is lower than the critical fracture stress of adjacent grains,and phase boundaries can effectively impede crack propagation into the matrix.The existence of a low proportion of high-angle grain boundaries(58.1%)and high Kernel average misorientation value(0.534°)in the segregation band promotes inclusions fragmentation and crack propagation.The difference in crack initiation and propagation direction caused by the morphology of inclusions and physical properties,as well as different matrix arrest abilities,is the main reasons for the diversity of inclusion fragmentation. 展开更多
关键词 Thick plate INCLUSION Finite element simulation Critical fracture stress Fracture mechanism
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Using Small Punch Test to Investigate the Mechanical Properties of X42 Exposed to Gaseous Hydrogen:Effect of Pressure,Pre-charge Time,Punch Velocity and Oxygen Content
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作者 Hu-Yue Wang Hong-Liang Ming +3 位作者 Dong-Ceng Hou Jian-Qiu Wang Wei Ke En-Hou Han 《Acta Metallurgica Sinica(English Letters)》 SCIE EI CAS CSCD 2024年第11期1961-1983,共23页
This study investigated the effect of pressure,pre-charge time,punch velocity and oxygen content on the mechanical properties of X42 pipeline steel in gaseous hydrogen environment by using small punch test.When expose... This study investigated the effect of pressure,pre-charge time,punch velocity and oxygen content on the mechanical properties of X42 pipeline steel in gaseous hydrogen environment by using small punch test.When exposed to nitrogen,the fracture mode of X42 pipeline steel undergoes ductile fracture,but in the presence of hydrogen,it shifts to brittle fracture.Moreover,an increase in hydrogen pressure or a decrease in punch velocity is found to enhance the hydrogen embrittlement susceptibility of X42 pipeline steel,as evidenced by the decrease of maximal load,displacement at failure onset and small punch energy.But the effect of pre-charge time on the hydrogen embrittlement susceptibility of X42 pipeline steel is not very obvious.Meanwhile,the presence of oxygen has been found to effectively inhibit hydrogen embrittlement.As the oxygen content in hydrogen increases,the hydrogen embrittlement susceptibility of X42 pipeline steel decreases. 展开更多
关键词 X42 pipeline steel Hydrogen embrittlement Mechanical properties Scanning electron microscopy(SEM) Small punch test
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Limit Test and pH Determination of 5-Hydroxymethylfurfural in Jiulongteng Honey
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作者 Beiqiao YIN Yanyan CHEN +3 位作者 Lili LIU Shenggao YIN Yanxia CEN Shiman CHEN 《Medicinal Plant》 2024年第3期23-25,29,共4页
[Objectives]To explore the effect of storage time on pH and 5-hydroxymethylfurfural content in Jiulongteng honey.[Methods]The pH of Jiulongteng honey was determined by neutralization titration with sodium hydroxide st... [Objectives]To explore the effect of storage time on pH and 5-hydroxymethylfurfural content in Jiulongteng honey.[Methods]The pH of Jiulongteng honey was determined by neutralization titration with sodium hydroxide standard solution.The content of 5-hydroxymethylfurfural in Jiulongteng honey was determined by HPLC.Chromatographic conditions:ZORBAX SB-C 18 column(250 mm×4.6 mm,5μm)from Agilent Co.,Ltd.,acetonitrile-0.1%formic acid solution(5:95)as mobile phase,flow rate of 0.8 mL/min,5-hydroxymethylfurfural detection wavelength of 284 nm,guanosine detection wavelength of 254 nm.[Results]The pH of 12 batches of Jiulongteng honey was 3.70-3.84 in the new honey stage,3.92-4.05 in the old honey stage 1,and 4.25-4.53 in the old honey stage 2;5-hydroxymethylfurfural was not detected in the new honey stage,5-hydroxymethylfurfural was detected in FM-001 in the old honey stage 1,and 5-hydroxymethylfurfural was detected in most samples in the old honey stage 2.[Conclusions]The pH and 5-hydroxymethylfurfural content of 12 batches of Jiulongteng honey met the requirements within 3 years of storage.There was no 5-hydroxymethylfurfural in Jiulongteng honey,but with the extension of storage time,the detection amount of 5-hydroxymethylfurfural increased significantly even if Jiulongteng honey was stored at low temperature.Therefore,5-hydroxymethylfurfural can be used as an important indicator of honey freshness. 展开更多
关键词 Jiulongteng HONEY 5-HYDROXYMETHYLFURFURAL PH HPLC
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通过式固相萃取-超高效液相色谱-串联质谱法测定沉积物中草铵膦、草甘膦及其代谢物 被引量:1
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作者 杨霄 谢仲桂 +3 位作者 李小玲 索纹纹 陈相艺 万译文 《色谱》 北大核心 2025年第2期155-163,共9页
建立了通过式固相萃取-超高效液相色谱-串联质谱法测定沉积物中草铵膦、草甘膦及其6种代谢物(3-甲基磷酸亚基丙酸、N-乙酰草铵膦、氨甲基膦酸、N-乙酰氨甲基膦酸、N-乙酰草甘膦、N-甲基草甘膦)的方法。样品采用4%(体积分数)氨水溶液提取... 建立了通过式固相萃取-超高效液相色谱-串联质谱法测定沉积物中草铵膦、草甘膦及其6种代谢物(3-甲基磷酸亚基丙酸、N-乙酰草铵膦、氨甲基膦酸、N-乙酰氨甲基膦酸、N-乙酰草甘膦、N-甲基草甘膦)的方法。样品采用4%(体积分数)氨水溶液提取,提取液经PRiME HLB固相萃取柱净化,过0.22μm聚醚砜滤膜后供超高效液相色谱-串联质谱测定。目标化合物使用Metrosep A Supp 5阴离子色谱柱(150 mm×4.0 mm,5μm)分离,以水和200 mmol/L碳酸氢铵溶液(含0.05%(v/v)氨水)作为流动相进行梯度洗脱,在电喷雾离子源(ESI)、负离子扫描和多反应监测(MRM)模式下进行测定,基质匹配外标法定量。结果表明,草铵膦、草甘膦及其代谢物在15 min内即可完成色谱分离,色谱峰形良好,响应值高,目标化合物在2.0~200.0μg/L范围内线性关系良好,相关系数均大于0.995。草铵膦、3-甲基磷酸亚基丙酸、N-乙酰草铵膦、N-乙酰氨甲基膦酸、N-乙酰草甘膦、N-甲基草甘膦的检出限为5μg/kg,定量限为20μg/kg;草甘膦、氨甲基膦酸的检出限为10μg/kg,定量限为30μg/kg。以空白沉积物为基质样品,在3个加标水平(定量限、5倍定量限和10倍定量限)下,低有机质含量的沉积物中目标化合物的平均回收率为78.5%~107%,相对标准偏差为1.32%~14.7%(n=6);高有机质含量的沉积物中目标化合物的平均回收率为76.4%~113%,相对标准偏差为2.60%~11.2%(n=6)。采用本方法对池塘、湖泊、水库、河流等不同类型的沉积物样品进行测定,结果显示,湖泊、水库、河流沉积物样品中未检出草铵膦、草甘膦及其代谢物,1个池塘沉积物样品中检出草甘膦和氨甲基膦酸,检出含量分别为31.7μg/kg和52.3μg/kg。本研究建立的方法具有简单、快速、绿色环保、准确度和灵敏度高、重复性好等优势,适用于沉积物中草铵膦、草甘膦及其代谢物的快速检测,为研究其在沉积物中的残留特征和环境行为提供了技术支持。 展开更多
关键词 超高效液相色谱-串联质谱 通过式固相萃取 草铵膦 草甘膦 代谢物 沉积物 非衍生化
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Animal Safety Test of Bacillus thuringiensis BT Protein
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作者 Weimeng NING Dingkuo LIU +6 位作者 Fang LIU Yuan LI Xiaowei YANG Zhenguo GUAN Guijun YANG Bo ZHANG Pengcheng HU 《Asian Agricultural Research》 2024年第2期31-32,35,共3页
[Objectives]To determine the biological safety of BT protein from Bacillus thuringiensis(Bt)fermentation broth to mammals at high doses.[Methods]Healthy mice were randomly divided into 4 groups with 10 mice in each gr... [Objectives]To determine the biological safety of BT protein from Bacillus thuringiensis(Bt)fermentation broth to mammals at high doses.[Methods]Healthy mice were randomly divided into 4 groups with 10 mice in each group.The experimental groups were fed with Bt fermentation supernatant at 0.2,0.6 and 1.0 mL/kg,respectively,once a day for 7 consecutive days.The blank control group was fed normally without intragastric administration.[Results]There was no significant difference in blood routine and blood biochemical analysis between the experimental group and the control group.After intragastric administration,the mice were dissected,and no obvious pathological changes were found;the heart,liver,spleen,lung and kidney were taken to make tissue sections,and no pathological changes were found by microscopic observation.[Conclusions]Mice can tolerate high doses of BT protein from B.thuringiensis fermentation broth. 展开更多
关键词 Bacillus thuringiensis(Bt) BT protein Biological safety
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发芽辣木籽凝乳酶在鲜食干酪加工中的应用 被引量:2
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作者 杨妍 张瑞 +2 位作者 丁井杰 张璐 王雪峰 《现代食品科技》 北大核心 2025年第1期65-73,共9页
以商用小牛皱胃酶为对照,用发芽辣木籽凝乳酶加工鲜食干酪,分别通过感官、营养成分、功能特性(拉伸性、融化性、油脂析出性)、总色差、游离脂肪酸等指标进行比较分析,结果表明:两者所加工干酪在感官、得率、蛋白含量、总色差ΔE值上无... 以商用小牛皱胃酶为对照,用发芽辣木籽凝乳酶加工鲜食干酪,分别通过感官、营养成分、功能特性(拉伸性、融化性、油脂析出性)、总色差、游离脂肪酸等指标进行比较分析,结果表明:两者所加工干酪在感官、得率、蛋白含量、总色差ΔE值上无显著差异(P>0.05),发芽辣木籽凝乳酶加工干酪脂肪质量分数为17.71%,显著低于小牛皱胃酶加工干酪(P<0.05);发芽辣木籽凝乳酶加工干酪的功能特性中融化性和拉伸长度为14.50 mm和30.40 cm,显著优于小牛皱胃酶加工干酪(P<0.05)。发芽辣木籽凝乳酶加工干酪游离脂肪酸总含量与小牛皱胃酶加工干酪无显著性差异(P>0.05),发芽辣木籽凝乳酶加工干酪组分中的亚油酸质量分数为1.68%,显著高于小牛皱胃酶加工干酪。该研究表明发芽辣木籽凝乳酶在一定程度上可替代小牛皱胃酶应用于鲜食干酪的加工制作,为发芽辣木籽凝乳酶在干酪加工中的应用提供了重要参考价值。 展开更多
关键词 发芽辣木籽凝乳酶 小牛皱胃酶 鲜食干酪 功能特性 游离脂肪酸
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沙棘百香果复合饮料发酵工艺优化及抗疲劳特性研究 被引量:2
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作者 马勇 慕永利 +1 位作者 周硕 冉军舰 《中国酿造》 北大核心 2025年第1期141-147,共7页
以沙棘和百香果为原料,酿酒酵母(Saccharomyces cerevisiae)和植物乳植杆菌(Lactiplantibacillus plantarum)(1∶1)为发酵菌种,制备沙棘百香果复合饮料。以感官评分和小鼠力竭跑步时间为评价指标,采用单因素和响应面试验优化其发酵工艺... 以沙棘和百香果为原料,酿酒酵母(Saccharomyces cerevisiae)和植物乳植杆菌(Lactiplantibacillus plantarum)(1∶1)为发酵菌种,制备沙棘百香果复合饮料。以感官评分和小鼠力竭跑步时间为评价指标,采用单因素和响应面试验优化其发酵工艺,并探讨沙棘百香果复合饮料对小鼠抗疲劳特性的影响。结果表明,最佳发酵工艺条件为发酵温度34℃,发酵时间14 h,混菌接种量5%,沙棘果汁与百香果汁体积比1∶1,木糖醇添加量6%。在此优化条件下,沙棘百香果复合饮料的感官评分和小鼠力竭跑步时间分别为(87.65±3.12)分和(138.1±3.5)s。相比对照组,沙棘百香果复合饮料喂食力竭跑步小鼠,肌糖原和肝糖原含量分别显著提高了58.7%和43.1%(P<0.05),乳酸脱氢酶、超氧化物歧化酶、过氧化氢酶、谷胱甘肽过氧化物酶活性均显著提高了50%以上(P<0.05),肌酸激酶活性显著降低了48.8%(P<0.05)。结果显示,沙棘百香果复合饮料对力竭跑步小鼠具有较好的抗疲劳特性。 展开更多
关键词 沙棘 百香果 混菌发酵 发酵工艺优化 抗疲劳
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基于表面增强拉曼光谱免疫层析法的卷烟纸中重金属元素快速检测 被引量:1
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作者 董浩 胡兴锋 +6 位作者 白文龙 郑帅 黄治 刘华 王澍 周明珠 邢军 《中国造纸》 北大核心 2025年第1期92-100,共9页
为实现卷烟纸中重金属的高敏、定量及快速检测,本研究提出了一种基于表面增强拉曼散射(SERS)信号的新型免疫层析技术。SERS免疫层析法使用一种树莓状的SERS标签Fe_(3)O_(4)@树莓状金磁性纳米颗粒(Fe@RAu)捕获样本中的金属残留物,Fe@RAu... 为实现卷烟纸中重金属的高敏、定量及快速检测,本研究提出了一种基于表面增强拉曼散射(SERS)信号的新型免疫层析技术。SERS免疫层析法使用一种树莓状的SERS标签Fe_(3)O_(4)@树莓状金磁性纳米颗粒(Fe@RAu)捕获样本中的金属残留物,Fe@RAu表面的Au壳能够产生拉曼热点效应以增强其表面修饰的5,5'-二硫代双(2-硝基苯甲酸)(DTNB)分子的拉曼信号,且其Fe_(3)O_(4)内核可被外加磁力吸附以富集样本中的靶标。基于这些特性,SERS免疫层析法具有超高的检测灵敏度和定量能力。结果表明,该方法同时检测卷烟纸燃烧灰烬中镉(Cd^(2+))、铬(Cr^(3+))、铅(Pb^(2+)),3种重金属离子的灵敏度分别达1.424、0.937和1.568 ng/kg,检测实际卷烟纸标准样品的加标回收率>90%,相对标准偏差(RSD)<10%,检测时间(包含预处理)<30 min。 展开更多
关键词 卷烟纸 重金属 快速检测 表面增强拉曼光谱 免疫层析
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Analysis of Safety Assessment and Testing of Heavy Traffic Vehicles on Old Bridges Without Data
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作者 Qing Yang Jiang Feng 《Journal of World Architecture》 2024年第1期35-39,共5页
This article presents a real-life project that aimed to evaluate the safety of traffic vehicles on old bridges without any prior data.The project involved various safety inspections,including conventional,static,and d... This article presents a real-life project that aimed to evaluate the safety of traffic vehicles on old bridges without any prior data.The project involved various safety inspections,including conventional,static,and dynamic load inspections and safety assessments.After conducting these tests,it was concluded that the structure of the old bridge is relatively safe,with only a few bumps.The bridge could function normally following appropriate treatment.The analysis provides valuable insights into the assessment of the quality and safety of such bridges to ensure the safe driving of heavy vehicles. 展开更多
关键词 Old bridge Absence of data Heavy vehicles Safety inspection Safety assessment
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Analysis of the Application of Static Load Test in Bridge Bearing Capacity Testing
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作者 Wei Fu Bo Liu 《Journal of Architectural Research and Development》 2024年第3期36-41,共6页
This article uses real engineering projects as examples to analyze how static load test technology is applied in testing the bridge-bearing capacity.The analysis covers aspects such as testing section layout,test load... This article uses real engineering projects as examples to analyze how static load test technology is applied in testing the bridge-bearing capacity.The analysis covers aspects such as testing section layout,test load and efficiency coefficient,loading plan,evaluation optimization,test result modification,and result evaluation.The aim is to support the accurate detection and evaluation of bridge-bearing capacity. 展开更多
关键词 Bridge engineering Bearing capacity Static load test Loading plan Test evaluation
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Acoustic Non-Destructive Testing Technology in Concrete Bridge Inspection and Pile Foundation Detection
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作者 Wei Fu 《Journal of Architectural Research and Development》 2024年第1期20-25,共6页
This article takes the actual construction project of a certain concrete bridge project as an example to analyze the application of acoustic non-destructive testing technology in its detection.It includes an overview ... This article takes the actual construction project of a certain concrete bridge project as an example to analyze the application of acoustic non-destructive testing technology in its detection.It includes an overview of a certain bridge construction project studied and acoustic non-destructive testing technology and the application of acoustic non-destructive testing technology in actual testing.This analysis hopes to provide some guidelines for acoustic non-destructive testing of modern concrete bridge projects. 展开更多
关键词 Concrete bridge Bridge detection Acoustic detection Non-destructive testing technology
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碳材料在聚乳酸立构复合结晶中的应用研究进展 被引量:1
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作者 常伟伟 荣卫锋 彭辉 《复合材料学报》 北大核心 2025年第4期1812-1823,共12页
聚乳酸是一种原料广泛、可生物降解的绿色高分子材料,具有力学性能好、热塑性强等优点,在替代石油基塑料方面具有极大潜力。然而,聚乳酸结晶速率慢、结晶度低、耐热性能差等问题,严重限制着其应用和发展。立构复合结晶(SC)已被证实是提... 聚乳酸是一种原料广泛、可生物降解的绿色高分子材料,具有力学性能好、热塑性强等优点,在替代石油基塑料方面具有极大潜力。然而,聚乳酸结晶速率慢、结晶度低、耐热性能差等问题,严重限制着其应用和发展。立构复合结晶(SC)已被证实是提高聚乳酸各方面性能的有效方法。但是,在聚乳酸的实际生产与应用中SC晶体很难可控生成。碳材料作为一种绿色环保的成核剂,能够有效地调控SC生成。本文介绍了聚乳酸形成的同质晶体(HC)与SC的晶体结构,对近年来不同碳材料作为成核剂促进聚乳酸SC结晶的研究成果进行了综述,并探讨了碳材料成核剂促进聚乳酸SC结晶可能的机制,最后进行了总结与展望,指出目前存在的挑战并为未来的发展提供了思路。 展开更多
关键词 碳材料 聚乳酸 立构复合结晶 成核剂 机制
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直接甲酯化法测定特膳食品中脂肪酸含量 被引量:2
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作者 张协光 岑干君 +5 位作者 张柳青 林宇豪 杨华瑞 蓝雄 滕明攀 甘旺 《分析科学学报》 北大核心 2025年第1期65-72,共8页
针对特殊膳食用食品,研究并改进了乙酰氯-甲醇法,实现了对特膳食品中脂肪酸的快速、准确测定。样品加入十一碳酸甘油三酯(C11:0 TAG)内标溶液后,在5%乙酰氯-甲醇溶液和70℃水浴的条件下衍生90 min,然后使用6%碳酸钠溶液中和余酸,离心取... 针对特殊膳食用食品,研究并改进了乙酰氯-甲醇法,实现了对特膳食品中脂肪酸的快速、准确测定。样品加入十一碳酸甘油三酯(C11:0 TAG)内标溶液后,在5%乙酰氯-甲醇溶液和70℃水浴的条件下衍生90 min,然后使用6%碳酸钠溶液中和余酸,离心取上清液,经气相色谱仪分析,采用内标法定量。结果表明,各脂肪酸在一定浓度范围内线性关系良好,相关系数均大于0.999,方法检出限为0.0005 g/100g,定量限为0.002 g/100g。在不同基质的样品中进行了低、中、高浓度的加标实验,3个加标水平下的回收率在90.0%~110%之间,相对标准偏差(RSD)均小于10%。将该方法应用于6种不同基质的特殊膳食用食品脂肪酸的检测,测定结果与国标方法一致,RSD均小于10%。该方法简单快速,精密度和准确度高,样品量消耗少,适用于特殊膳食用食品中脂肪酸的检测。 展开更多
关键词 特殊膳食用食品 脂肪酸 乙酰氯-甲醇法 气相色谱 内标法
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基于安全视角下仪器共享平台管理模式的探析 被引量:3
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作者 陈晓丽 刘世君 +1 位作者 陈佩丽 苏秋成 《实验科学与技术》 2025年第1期149-155,共7页
仪器共享平台是依托高校、科研院所建立的集大型仪器设备共享、科研任务、仪器功能和方法开发于一体的特色平台,平台的安全运行是管理工作中的关键。该文从安全角度分析了仪器共享平台运行现状和主要安全隐患,分别从平台监督控制管理、... 仪器共享平台是依托高校、科研院所建立的集大型仪器设备共享、科研任务、仪器功能和方法开发于一体的特色平台,平台的安全运行是管理工作中的关键。该文从安全角度分析了仪器共享平台运行现状和主要安全隐患,分别从平台监督控制管理、仪器共享管理、实验室安全管理、化学试剂管理、安全教育管理和突发事件应急管理等方面初步探讨管理模式,旨在建立完善的仪器共享管理平台的安全管理体系,为仪器共享平台管理提供新的思路。 展开更多
关键词 仪器共享平台 安全管理 仪器设备
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