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Hydrogen storage properties of Mg-TiO_2 composite powder prepared by arc plasma method 被引量:5
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作者 潘银成 邹建新 +1 位作者 曾小勤 丁文江 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2014年第12期3834-3839,共6页
Mg-based Mg-TiO2 composite powder was prepared by arc plasma evaporation of the Mg+5%TiO2 mixture followed by passivation in air. ICP, XRD and SEM techniques were used to characterize the composition, phase component... Mg-based Mg-TiO2 composite powder was prepared by arc plasma evaporation of the Mg+5%TiO2 mixture followed by passivation in air. ICP, XRD and SEM techniques were used to characterize the composition, phase components and microstructure of the composite powder. The hydrogen sorption properties of the composite powder were investigated by DSC and PCT techniques. According to the data from PCT measurements, the hydrogenation enthalpy and entropy changes of the composite powder are calculated to be-71.5 kJ/mol and-130.1 J/(K·mol), respectively. Besides, the hydrogenation activation energy is determined to be 77.2 kJ/ mol. The results indicate that TiO2 added into Mg by arc plasma method can act as a catalyst to improve the hydrogen sorption kinetic properties of Mg. 展开更多
关键词 nanostructured composite Mg TIO2 hydrogen storage arc plasma method
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Decomposition of gaseous CF_2CIBr by cold plasma method 被引量:1
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作者 Deng Guohong Zhang Yue Yu Yong Zou Daozhong Hou Huiqi Li Changlin Environmental Science Institute,Fudan University,Shanghai 200433,China 《Journal of Environmental Sciences》 SCIE EI CAS CSCD 1997年第1期11-19,共9页
The paper presented the results regarding the decomposition of gaseous CF_2ClB_r by cold plasma method.After two minutes discharge,the maximum decomposition rate of 2660 Pa CF_2ClB_r pure and 2660 Pa CF_2ClBr plus 798... The paper presented the results regarding the decomposition of gaseous CF_2ClB_r by cold plasma method.After two minutes discharge,the maximum decomposition rate of 2660 Pa CF_2ClB_r pure and 2660 Pa CF_2ClBr plus 7980 Pa O_2 reached 60% and 80%,respectively.The pa- per also studied the cold plasma gas phase chemistry reaction mechanism of CF_2ClBr at low pres- sure,and the pressure effects of CF_2ClBr and added gas(He,N_2,O_2 and dry air)on the CF_2ClBr decomposition respectively by cold plasma method.These studies will be helpful to application of cold plasma method in the treatment of hazardous gaseous wastes. 展开更多
关键词 DECOMPOSITION gaseous CF_2ClBr cold plasma method.
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STUDIES ON THE SYNTHESIS OF Ti_3O_5 BY MICROWAVE INDUCED PLASMA METHOD
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作者 Ai Min YU Wen Guo XU +1 位作者 Wen Jun YANG Quan Zhong LI and Qin Han JIN (Department of Chemistry, Jinn University, Changchun 130023) 《Chinese Chemical Letters》 SCIE CAS CSCD 1994年第5期447-448,共2页
Using a low power microwave generator and a surfatron discharge cavity, Ti3O5 was synthesized via the hydrogenation of TiO2 in surface wave induced microwave plasma. Besides, the chemical behavior of hydrogen in the p... Using a low power microwave generator and a surfatron discharge cavity, Ti3O5 was synthesized via the hydrogenation of TiO2 in surface wave induced microwave plasma. Besides, the chemical behavior of hydrogen in the plasma and its influence on the formation of Ti3O5 were preliminarily studied. 展开更多
关键词 TI STUDIES ON THE SYNTHESIS OF Ti3O5 BY MICROWAVE INDUCED plasma method
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SILICON NITRIDE POWDER SYNTHESIZED BY THERMAL PLASMA METHOD 被引量:1
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作者 Liang Shuquan Huang Baiyun Zheng Ziqiao(Central South University of Technology, Changsha 410083)Szepvolgyi J (Research Laboratory for inorganic Chemistry of Hungarian Academy of Sciences,H-1502, Budapest, Hungary) 《中国有色金属学会会刊:英文版》 CSCD 1996年第3期103-107,共5页
SILICONNITRIDEPOWDERSYNTHESIZEDBYTHERMALPLASMAMETHOD¥LiangShuquan;HuangBaiyun;ZhengZiqiao(CentralSouthUniver... SILICONNITRIDEPOWDERSYNTHESIZEDBYTHERMALPLASMAMETHOD¥LiangShuquan;HuangBaiyun;ZhengZiqiao(CentralSouthUniversityofTechnology,... 展开更多
关键词 Si3N4 NANOSIZED POWDER thermal plasma method
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Synthesis and characterization of Fe_3Al intermetallic nanopowder by hydrogen arc plasma method (HP)
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作者 尹衍生 董丽华 范春华 《中国有色金属学会会刊:英文版》 CSCD 2005年第S3期43-47,共5页
Nanostructured Fe3Al intermetallic compounds were produced by using hydrogen arc plasma method(HP). The microstructures of the nano Fe3Al were characterized by means of XRD, DSC-TG and TEM. The results shows that th... Nanostructured Fe3Al intermetallic compounds were produced by using hydrogen arc plasma method(HP). The microstructures of the nano Fe3Al were characterized by means of XRD, DSC-TG and TEM. The results shows that the intermetallic compounds have ordered B2 structure and the average particle of the as synthesized is about 45nm. The B2 structure changes to highly ordered DO3 structure after annealing in vaccum at 480℃. The temperature of phase transformation is 545.3℃. 展开更多
关键词 nanointermetallic HYDROGEN ARC plasma method phase structure
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The determination of 52 elements in marine geological samples by an inductively coupled plasma optical emission spectrometry and an inductively coupled plasma mass spectrometry with a high-pressure closed digestion method 被引量:16
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作者 GAO Jingjing LIU Jihua +3 位作者 LI Xianguo YAN Quanshu WANG Xiaojing WANG Hongmin 《Acta Oceanologica Sinica》 SCIE CAS CSCD 2017年第1期109-117,共9页
An improved analytical method to determine the content of 52 major, minor and trace elements in marine geological samples, using a HF-HCl-HNO_3 acid system with a high-pressure closed digestion method(HPCD), is stud... An improved analytical method to determine the content of 52 major, minor and trace elements in marine geological samples, using a HF-HCl-HNO_3 acid system with a high-pressure closed digestion method(HPCD), is studied by an inductively coupled plasma optical emission spectrometry(ICP-OES) and an inductively coupled plasma mass spectrometry(ICP-MS). The operating parameters of the instruments are optimized, and the optimal analytical parameters are determined. The influences of optical spectrum and mass spectrum interferences, digestion methods and acid systems on the analytical results are investigated. The optimal spectral lines and isotopes are chosen, and internal standard element of rhodium is selected to compensate for matrix effects and analytical signals drifting. Compared with the methods of an electric heating plate digestion and a microwave digestion, a high-pressure closed digestion method is optimized with less acid, complete digestion,less damage for digestion process. The marine geological samples are dissolved completely by a HF-HCl-HNO_3 system, the relative error(RE) for the analytical results are all less than 6.0%. The method detection limits are 2–40μg/g by the ICP-OES, and 6–80 ng/g by ICP-MS. The methods are used to determine the marine sediment reference materials(GBW07309, GBW07311, GBW07313), rock reference materials(GBW07103, GBW07104,GBW07105), and cobalt-rich crust reference materials(GBW07337, GBW07338, GBW07339), the obtained analytical results are in agreement with the certified values, and both of the relative standard deviation(RSD) and the relative error(RE) are less than 6.0%. The analytical method meets the requirements for determining 52 elements contents of bulk marine geological samples. 展开更多
关键词 marine geological sample high-pressure closed digestion method inductively coupled plasma optical emission spectrometry inductively coupled plasma mass spectrometry major element minor element trace element
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Plasma shape optimization for EAST tokamak using orthogonal method
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作者 Yuan-Yang Chen Xiao-Hua Bao +1 位作者 Peng Fu Ge Gao 《Chinese Physics B》 SCIE EI CAS CSCD 2019年第1期453-459,共7页
It is necessary to reduce the currents of poloidal field(PF) coils as small as possible, during the static equilibrium design procedure of Experimental Advanced Superconductive Tokamak(EAST). The quasi-snowflake(QSF) ... It is necessary to reduce the currents of poloidal field(PF) coils as small as possible, during the static equilibrium design procedure of Experimental Advanced Superconductive Tokamak(EAST). The quasi-snowflake(QSF) divertor configuration is studied in this paper. Starting from a standard QSF plasma equilibrium, a new QSF equilibrium with 300 kA total plasma current is designed. In order to reduce the currents of PF6 and PF14, the influence of plasma shape on PF coil current distribution is analyzed. A fixed boundary equilibrium solver based on a non-rigid plasma model is used to calculate the flux distribution and PF coil current distribution. Then the plasma shape parameters are studied by the orthogonal method. According to the result, the plasma shape is redefined, and the calculated equilibrium shows that the currents of PF6 and PF14 are reduced by 3.592 kA and 2.773 kA, respectively. 展开更多
关键词 EAST plasma SHAPE ORTHOGONAL method plasma EQUILIBRIUM CALCULATION
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Critical Study on a Method for the Determination of Plasma Lipid Peroxides with Report of Normal Plasma Value in Healthy Adults
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作者 谭委民 朱雯 《The Journal of Biomedical Research》 CAS 1994年第1期19-21,共3页
Using TBA(thiobarbituric acid) method for lipid peroxides (LPO)of normal unhemolyzedand hemolyzed plasma was determined in 62 healthy blood donors,aging 28-42. In 46 normalunhemolyzed plasma, The normal range of LPO i... Using TBA(thiobarbituric acid) method for lipid peroxides (LPO)of normal unhemolyzedand hemolyzed plasma was determined in 62 healthy blood donors,aging 28-42. In 46 normalunhemolyzed plasma, The normal range of LPO is 5.56 ± 1.14,with 95% and 99% confidence regingwith in 5.221-5.889 and 5.108-6.012 respectively.There is a significant increase in the level of LPO(10.12 ± 3.84) in 16 hemolyzed plasma (P< 0-00 1).The results show that hemolyzed blood plasma sampleis unsuitable for analysis.We also fount that the blood plasma LPO value is not influenced by sex andblood group (P>0.05). 展开更多
关键词 TBA method plasma LPO value SEX blood group
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Study on Free Surface and Channel Flow Induced by Low Temperature Plasma via Lattice Boltzmann Method 被引量:1
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作者 弯港 金涌 +1 位作者 李海元 栗保明 《Plasma Science and Technology》 SCIE EI CAS CSCD 2016年第3期331-336,共6页
Active boundary layer flow control and boundary layer manipulation in the channel flow that was based on low temperature plasma were studied by means of a lattice Boltzmann method. Two plasma actuators were placed in ... Active boundary layer flow control and boundary layer manipulation in the channel flow that was based on low temperature plasma were studied by means of a lattice Boltzmann method. Two plasma actuators were placed in a row to obtain the influence rule of their separation distance on the velocity profile at three locations and maximum velocity in the flow field. Two plasma actuators were placed symmetrically inside a channel to examine the effect of channel height and voltage on the velocity profile and flow rate. It was found that the channel height controls the distribution of flow velocity, which affected the flow rate and its direction. Increasing plasma voltage had a negative effect on the flow rate due to the generation of a larger and stronger flow vortex. 展开更多
关键词 lattice Boltzmann method (LBM) low-temperature plasma induced flow
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Correlation Method of Average Plasma Velocity Measurement in Hall-Effect Thrusters
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作者 宁中喜 李鸿 于达仁 《Plasma Science and Technology》 SCIE EI CAS CSCD 2009年第6期709-713,共5页
A new method to measure the average plasma velocity in a Hall-effect thruster is presented. The method is brought forward in virtue of the characteristics of low frequency oscillation induced by the propellant ionizat... A new method to measure the average plasma velocity in a Hall-effect thruster is presented. The method is brought forward in virtue of the characteristics of low frequency oscillation induced by the propellant ionization in the channel and the oriented movement feature of the plasma density out of the channel. The method, equivalent to the correlation method generally used in the signal processing field, provides a solution to the problem of specific impulse measurement on a timescale of hundreds of microseconds and makes the time evolution of average plasma velocity clear. The comparison between the measured value and the calibrated value shows that the relative error is about 3%. 展开更多
关键词 Hall-effect thruster average plasma velocity correlation method
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Approximation analytical solutions for a unified plasma sheath model by double decomposition method
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作者 Fang Jin-Qing (China Institute of Atomic Energy Beijing 102413) 《Nuclear Science and Techniques》 SCIE CAS CSCD 1998年第4期193-197,共5页
A anified plasma sheath model and its potential equation are proposed. Any higher-ordor-approximation analytical solutions for the unified plasma sheath potential equa tiop are derived by double decomposition method.
关键词 等离子体 屏蔽模型 双分解方法 近似分析
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Piecewise linear recursive convolution FDTD method for magnetized plasmas 被引量:4
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作者 Liu Song Zhong Shuangying Liu Shaobin 《Journal of Systems Engineering and Electronics》 SCIE EI CSCD 2006年第2期290-295,共6页
The piecewise linear recursive convolution (PLRC) finite-different time-domain (FDTD) method greatly improves accuracy over the original recursive convolution (RC) FDTD approach but retains its speed and efficie... The piecewise linear recursive convolution (PLRC) finite-different time-domain (FDTD) method greatly improves accuracy over the original recursive convolution (RC) FDTD approach but retains its speed and efficiency advantages. A PLRC-FDTD formulation for magnetized plasma which incorporates both anisotropy and frequency dispersion at the same time is presented, enabled the transient analysis of magnetized plasma media. The technique is illustrated by numerical simulations the reflection and transmission coefficients through a magnetized plasma layer. The results show that the PLRC-FDTD method has significantly improved the accuracy over the original RC method. 展开更多
关键词 electromagnetic wave FDTD methods piecewise linear recursive convolution magnetized plasma.
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Separation Method in the Problem of a Beam-Plasma Interaction in a Cylindrical Warm Plasma Waveguide
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作者 Khaled H. El-Shorbagy Abdelrahman S. Al-Fhaid Mohamed A. Al-Ghamdi 《Journal of Modern Physics》 2011年第10期1104-1108,共5页
The stabilization effect of a strong HF electric field on beam-plasma instability in a cylindrical warm plasma waveguide is discussed. A mathematical technique “separation method” applied to the two-fluid plasma mod... The stabilization effect of a strong HF electric field on beam-plasma instability in a cylindrical warm plasma waveguide is discussed. A mathematical technique “separation method” applied to the two-fluid plasma model to separate the equations, which describe the system, into two parts, temporal and space parts. Plasma electrons are considered to have a thermal velocity. It is shown that a HF electric field has no essential influence on dispersion characteristics of unstable surface waves excited in a warm plasma waveguide by a low-density electron beam. The region of instability only slightly narrowing and the growth rate decreases by a small parameter and this result has been reduced compared to cold plasma. Also, it is found that the plasma electrons have not affected the solution of the space part of the problem. 展开更多
关键词 SEPARATION method Beam-plasma Interaction WARM plasma WAVEGUIDE
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Laser-induced plasma electron number density:Stark broadening method versus the Saha-Boltzmann equation 被引量:2
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作者 Arnab SARKAR Manjeet SINGH 《Plasma Science and Technology》 SCIE EI CAS CSCD 2017年第2期43-51,共9页
We report spectroscopic studies on plasma electron number density of laser-induced plasma produced by ns-Nd:YAG laser light pulses on an aluminum sample in air at atmospheric pressure. The effect of different laser e... We report spectroscopic studies on plasma electron number density of laser-induced plasma produced by ns-Nd:YAG laser light pulses on an aluminum sample in air at atmospheric pressure. The effect of different laser energy and the effect of different laser wavelengths were compared. The experimentally observed line profiles of neutral aluminum have been used to extract the excitation temperature using the Boltzmann plot method, whereas the electron number density has been determined from the Stark broadened as well as using the Saha-Boltzmann equation (SBE). Each approach was also carried out by using the AI emission line and Mg emission lines. It was observed that the,SBE method generated a little higher electron number density value than the Stark broadening, method, but within the experimental uncertainty range. Comparisons of Ne determined by the two methods show the presence of a linear relation which is independent of laser energy or laser wavelength. These results show the applicability of the SBE method for Are determination, especially when the system does not have any pure emission lines whose electron impact factor is known, Also use of Mg lines gives superior results than Al lines. 展开更多
关键词 plasma parameter laser induced plasma plasma electron density Saha-Boltzmannmethod Stark broadening method
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A Revised Piecewise Linear Recursive Convolution FDTD Method for Magnetized Plasmas 被引量:1
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作者 刘崧 钟双英 刘少斌 《Plasma Science and Technology》 SCIE EI CAS CSCD 2005年第6期3122-3126,共5页
The piecewise linear recursive convolution (PLRC) finite-different time-domain (FDTD) method improves accuracy over the original recursive convolution (RC) FDTD approach and current density convolution (JEC) b... The piecewise linear recursive convolution (PLRC) finite-different time-domain (FDTD) method improves accuracy over the original recursive convolution (RC) FDTD approach and current density convolution (JEC) but retains their advantages in speed and efficiency. This paper describes a revised piecewise linear recursive convolution PLRC-FDTD formulation for magnetized plasma which incorporates both anisotropy and frequency dispersion at the same time, enabling the transient analysis of magnetized plasma media. The technique is illustrated by numerical simulations of the reflection and transmission coefficients through a magnetized plasma layer. The results show that the revised PLRC-FDTD method has improved the accuracy over the original RC FDTD method and JEC FDTD method. 展开更多
关键词 Electromagnetic wave finite-different time-domain (FDTD) methods piecewise linear recursive convolution magnetized plasma
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Transmissivity of electromagnetic wave propagating in magnetized plasma sheath using variational method
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作者 Jianyi CHEN Chengxun YUAN +1 位作者 Xiudong SUN Lei HUO 《Plasma Science and Technology》 SCIE EI CAS CSCD 2019年第12期1-5,共5页
A variational method is introduced to analyze the transmissivity of an electromagnetic wave propagating in the magnetized plasma sheath. The plasma density is modeled by two parabolic inhomogeneous regions separated b... A variational method is introduced to analyze the transmissivity of an electromagnetic wave propagating in the magnetized plasma sheath. The plasma density is modeled by two parabolic inhomogeneous regions separated by one homogeneous region. The Lagrangian density of the system is constructed based on the fluid energy density and the electromagnetic energy density.The total variation of the Lagrangian density is derived. The fluid and electromagnetic fields are numerically solved by expansion in piecewise polynomial function space. We investigate the effect of an external magnetic field on the transmissivity of the electromagnetic wave. It is found that the transmissivity is increased when an external magnetic field is applied. The dependence of transmissivity on the collision frequency between the electrons and the neutral particles has also been studied. We also show that the external magnetic field causes a shift in the critical frequency of the plasma sheath. 展开更多
关键词 electromagnetic WAVE PROPAGATION variational method WAVE theory WAVE PROPAGATION plasma sheath
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Modeling OH transport phenomena in cold plasma discharges using the level set method
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作者 Wei HAN K N YU 《Plasma Science and Technology》 SCIE EI CAS CSCD 2019年第5期121-131,共11页
Cold atmospheric plasmas(CAPs)have attracted considerable interest in the field of plasma medicine.Generated reactive species such as hydroxyl(OH)species play an important role in applications of CAPs.Transportation o... Cold atmospheric plasmas(CAPs)have attracted considerable interest in the field of plasma medicine.Generated reactive species such as hydroxyl(OH)species play an important role in applications of CAPs.Transportation of OH species towards the target and distribution of these OH species in the plasma plume play an important role in the applications of plasma medicine.In the present work,a computational model was built to simulate the transportation and distribution of OH species in CAP discharges,which was based on the level set method to dynamically track the propagation of plasma carrier gas in air.A reaction term was incorporated for the OH species.The OH species tended to diffuse around the main stream of the carrier gas,and thus covered larger radial and axial distances.A CAP discharge onto a skin layer led to the largest accumulation of OH species at the central part of the exposed area.The distribution of OH species on the skin was asymmetric,which agreed with experiments.The computational model itself and the obtained results would be useful for future development of plasma medicine. 展开更多
关键词 cold atmospheric plasmas plasma medicine two-phase flow DIFFUSION level set method
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DBD等离子体辅助煤炭燃烧放电特性的影响因素研究 被引量:1
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作者 胡海波 《电工技术》 2025年第5期8-11,16,共5页
为了研究影响DBD等离子体辅助煤炭燃烧放电特性因素主次,并得出改善放电特性的最佳因素水平组合方案,采用平板型结构的DBD反应器用于助燃,共选择了3个因素3个水平,通过正交实验法将实验次数由27次减少至9次。实验结果表明:电压等级和电... 为了研究影响DBD等离子体辅助煤炭燃烧放电特性因素主次,并得出改善放电特性的最佳因素水平组合方案,采用平板型结构的DBD反应器用于助燃,共选择了3个因素3个水平,通过正交实验法将实验次数由27次减少至9次。实验结果表明:电压等级和电极间距是影响放电功率和传输电荷量较为显著的因素,而提高放电功率和传输电荷量的最佳因素水平组合方案为A_(3)B_(3)C_(1)和A_(3)B_(3)C_(2)。研究结果可为DBD等离子体助燃反应器的优化提供一定的参考价值。 展开更多
关键词 等离子体 介质阻挡放电 正交实验法 平板型
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等离子体刻蚀对聚苯乙烯微球尺寸缩减的工艺优化研究
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作者 孙士阳 黄胜保 +4 位作者 钱远近 刘东昆 李嘉彬 任元 张文兴 《材料保护》 2025年第7期58-65,共8页
利用感应耦合等离子体刻蚀技术(Inductively Coupled Plasma, ICP)以及聚苯乙烯(PS)微球作为掩膜的刻蚀技术在硅纳米阵列的制备中应用广泛,但是PS微球的尺寸缩减过程中刻蚀往往伴随着表面质量下降的问题,同时PS微球的形貌受到多种工艺... 利用感应耦合等离子体刻蚀技术(Inductively Coupled Plasma, ICP)以及聚苯乙烯(PS)微球作为掩膜的刻蚀技术在硅纳米阵列的制备中应用广泛,但是PS微球的尺寸缩减过程中刻蚀往往伴随着表面质量下降的问题,同时PS微球的形貌受到多种工艺参数共同的影响,研究困难。为了解决这些问题,采用正交实验法对ICP工艺在粒径为10μm的PS微球尺寸缩减过程中的工艺影响进行了深入研究。结果显示:气体成分对刻蚀效果有显著影响,射频功率与微球尺寸缩减、表面粗糙度均为正相关,压强与微球表面粗糙度呈负相关,流量基本无影响。基于上述结论,最终确定最优工艺参数为:在O_(2)中添加20%的CF_(4),射频功率200 W-100 W(感应功率-直流偏置功率),压强3.0 Pa,气体流量50 mL/min(O_(2)∶CF_(4)流量比为4∶1)的工艺参数下,在不影响PS微球的刻蚀缩减效果的情况下表面粗糙度最低。采用此优化模板制备得到了高度线性化且外表面光滑的硅纳米阵列。 展开更多
关键词 等离子体刻蚀 聚苯乙烯微球 正交实验法 表面形貌
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水中碘化物测定ICP-MS法与分光光度法的比较及应用
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作者 桂婷婷 田鑫 +1 位作者 沈宇琦 岳中慧 《广东化工》 2025年第11期123-126,共4页
分析ICP-MS法与分光光度法测定水中碘化物的数据对比,推广ICP-MS法作为新方法在基层实验室水碘检测中的应用。优化质谱条件,对两种方法检测限、线性范围、精密度、准确度、批量样品检测等数据进行配对t检验统计学分析。实验证明ICP-MS... 分析ICP-MS法与分光光度法测定水中碘化物的数据对比,推广ICP-MS法作为新方法在基层实验室水碘检测中的应用。优化质谱条件,对两种方法检测限、线性范围、精密度、准确度、批量样品检测等数据进行配对t检验统计学分析。实验证明ICP-MS法线性范围更广、灵敏度更低,在测定低浓度样品上优势明显,准确度、回收率均优于分光光度法;分光光度法不需要仪器记忆效应,对于高浓度水样检测准确度优于ICP-MS法。两种方法对实际样品检测结果的差异无统计学意义。 展开更多
关键词 ICP-MS法 分光光度法 水碘 STD模式 KED模式
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