To develop a suitable production process for fiber reinforced investment casting shell mold,three methods were studied:the traditional method(M_(1)),the method of adding fiber into silica sol with mechanical stirring ...To develop a suitable production process for fiber reinforced investment casting shell mold,three methods were studied:the traditional method(M_(1)),the method of adding fiber into silica sol with mechanical stirring and ultrasonic agitation(M_(2)),and the method of adding fiber into slurry with mechanical stirring and ultrasonic agitation for durations of 3,15,30,and 45 min(M_(3)).The bending strength,high-temperature self-load deformation,and thermal conductivity of the shell molds were investigated.The results reveal that the enhancement of fiber dispersion through ultrasonic agitation improves the comprehensive performance of the shell molds.The maximum green bending strength of the shell mold by M_(2) reaches 3.29 MPa,which is 29% higher than that of the shell mold prepared by M_(1).Moreover,the high-temperature self-load deformation of the shell mold is reduced from 0.62% to 0.44%.In addition,simultaneous ultrasonic agitation and mechanical stirring effectively shorten the slurry preparation time while maintaining comparable levels of fiber dispersion.With the process M_(3)-45 min,the fillers are uniformly dispersed in the slurry,and the fired bending strength and the high-temperature self-load deformation reach 6.25 MPa and 0.41%,respectively.Therefore,the proposed ultrasonic agitation route is promising for the fabrication of fiber-reinforced shell molds with excellent fibers dispersion.展开更多
The latest generation of aero engines has set higher standards for thrust-to-weight ratio and energy conversion efficiency,making it imperative to address the challenge of efficiently and accurately machining film coo...The latest generation of aero engines has set higher standards for thrust-to-weight ratio and energy conversion efficiency,making it imperative to address the challenge of efficiently and accurately machining film cooling holes.It has been demonstrated that conventional long-pulse lasers are incapable of meeting the elevated quality surface finish requirements for these holes,a consequence of the severe thermal defects.The employment of backside water-assisted laser drilling technology confers a number of distinct advantages in terms of mitigating laser thermal damage,thus representing a highly promising solution to this challenge.However,significant accumulation of bubbles and machining products during the backside water-assisted laser drilling process has been demonstrated to have a detrimental effect on laser transmission and machining stability,thereby reducing machining quality.In order to surmount these challenges,a novel method has been proposed,namely an ultrasonic shock water flow-assisted picosecond laser drilling technique.Numerical models for ultrasonic acoustic streaming and particle tracking for machining product transport have been established to investigate the mechanism.The simulation results demonstrated that the majority of the machining products could rapidly move away from the machining area because of the action of acoustic streaming,thereby avoiding the accumulation of bubbles and products.Subsequent analysis,comparing the process performance in micro-hole machining,confirmed that the ultrasonic field could effectively eliminate bubble and chip accumulation,thus significantly improving micro-hole quality.Furthermore,the impact of ultrasonic and laser parameters on micro-hole quality under varying machining methods was thoroughly investigated.The findings demonstrated that the novel methodology outlined in this study yielded superior-quality micro-holes at elevated ultrasonic and laser power levels,in conjunction with reduced laser frequency and scanning velocity.The taper of the micro-holes produced by the new method was reduced by more than 25%compared with the other conventional methods.展开更多
Pipelines are extensively used in environments such as nuclear power plants,chemical factories,and medical devices to transport gases and liquids.These tubular environments often feature complex geometries,confined sp...Pipelines are extensively used in environments such as nuclear power plants,chemical factories,and medical devices to transport gases and liquids.These tubular environments often feature complex geometries,confined spaces,and millimeter-scale height restrictions,presenting significant challenges to conventional inspection methods.Here,we present an ultrasonic microrobot(weight,80 mg;dimensions,24 mm×7 mm;thickness,210μm)to realize agile and bidirectional navigation in narrow pipelines.The ultrathin structural design of the robot is achieved through a high-performance piezoelectric composite film microstructure based on MEMS technology.The robot exhibits various vibration modes when driven by ultrasonic frequency signals,its motion speed reaches81 cm s-1 at 54.8 k Hz,exceeding that of the fastest piezoelectric microrobots,and its forward and backward motion direction is controllable through frequency modulation,while the minimum driving voltage for initial movement can be as low as 3 VP-P.Additionally,the robot can effortlessly climb slopes up to 24.25°and carry loads more than 36 times its weight.The robot is capable of agile navigation through curved L-shaped pipes,pipes made of various materials(acrylic,stainless steel,and polyvinyl chloride),and even over water.To further demonstrate its inspection capabilities,a micro-endoscope camera is integrated into the robot,enabling real-time image capture inside glass pipes.展开更多
P91 steel is an important bearing material used in nuclear power plants. The study of its mechanical degradation behavior is important for ensuring safe operation. The relationship between the dislocation density of P...P91 steel is an important bearing material used in nuclear power plants. The study of its mechanical degradation behavior is important for ensuring safe operation. The relationship between the dislocation density of P91 steel under different strains and the corresponding nonlinear ultrasonic parameter β was studied. The dislocation density of strained samples was estimated by X-ray diffraction. Nonlinear ultrasonic testing was conducted to evaluate β, showing that this value increased with increasing dislocation density induced by different tensile elongations. It was shown that the ultrasonic secondharmonic generation technique can effectively evaluate the degradation behavior of metallic materials, and the prediction of the residual life of bearing parts in service can be made based on β and the dislocation density.展开更多
The coupling effects of ultrasonic excitation and high-strain-rate deformation are the core factors for weld formation during ultrasonic welding.However,interfacial deformation behavior still shrouds in uncer-tainty b...The coupling effects of ultrasonic excitation and high-strain-rate deformation are the core factors for weld formation during ultrasonic welding.However,interfacial deformation behavior still shrouds in uncer-tainty because of the contradictory features between mutual dislocation retardation caused by severely frictional deformation and ultrasonic-accelerated dislocation motion.[101]and[111]-oriented Cu single crystals which tended to form geometrically necessary boundaries(GNBs)were selected as the welding substrates to trace the uniquely acoustoplastic effects in the interfacial region under the ultrasonically excited high-strain-rate deformation.It was indicated that for a low energy input,micro-welds localized at the specific interface region,and equiaxed dislocation cells substituting for GNBs dominated in the ini-tial single crystal rotation region.As the welding energy increased,continuous shear deformation drove the dynamic recrystallization region covered by equiaxed grains to spread progressively.Limited discrete dislocations inside the recrystallized grains and nascent dislocation cells at the grain boundaries were ob-served in[101]and[111]joints simultaneously,suggesting that the ultrasonic excitation promoted motion of intragranular dislocation and pile-up along the sub-grain boundaries.The interfacial morphology be-fore and after expansion of recrystallization region all exhibited the weakening of orientation constraint on dislocation motion,which was also confirmed by the similar micro-hardness in joint interface.The first-principle calculation and applied strain-rate analysis further revealed that ultrasonic excitation en-hanced dislocation slipping,and enabled dislocation motion to accommodate severe plastic deformation at a high-strain-rate.展开更多
This paper introduces part of the content in the association standard,T/CAAM0002–2020 Nomenclature and Location of Acupuncture Points for Laboratory Animals Part 3:Mouse.This standard was released by the China Associ...This paper introduces part of the content in the association standard,T/CAAM0002–2020 Nomenclature and Location of Acupuncture Points for Laboratory Animals Part 3:Mouse.This standard was released by the China Association of Acupuncture and Moxibustion on May 15,2020,implemented on October 31,2020,and published by Standards Press of China.The standard was drafted by the Institute of Acupuncture and Moxibustion,China Academy of Chinese Medical Sciences,and the Nanjing University of Chinese Medicine.Principal draftsmen:Xiang-hong JING and Xing-bang HUA.Participating draftsmen:Wan-zhu BAI,Bin XU,Dong-sheng XU,Yi GUO,Tie-ming MA,Xin-jun WANG,and Sheng-feng LU.展开更多
The remarkable ability of titanium alloys to preserve their superior physical and chemical characteristics when subjected to extreme conditions significantly enhances their importance in the aerospace,military,and med...The remarkable ability of titanium alloys to preserve their superior physical and chemical characteristics when subjected to extreme conditions significantly enhances their importance in the aerospace,military,and medical sectors.However,conventional machining of titanium alloys leads to elevated tool wear,development of surface defects,and reduced machining efficiency due to their low heat conductivity,and chemical affinity.These issues can be somewhat counteracted by integrating ultrasonic vibration in the conventional machining of titanium alloys and also enhance sustainability.This review article offers a holistic evaluation of the influence of ultrasonic vibration-assisted milling and turning on cutting forces,temperature,tool wear,and surface integrity,encompassing surface morphology,surface roughness,surface residual stress,surface hardness,and surface tribological properties during titanium alloys machining.Furthermore,it investigates the sustainability aspect that has not been previously examined.Studies on the performance of ultrasonic-assisted cutting revealed several advantages,including decreased cutting forces and cutting temperature,improved tool life,and a better-machined surface during machining.Consequently,the sustainability factor is improved due to minimized energy consumption and residual waste.In conclusion,the key challenges and future prospects in the ultrasonic-assisted cutting of titanium alloys are also discussed.This review article provides beneficial knowledge for manufactur-ers and researchers regarding ultrasonic vibration-assisted cutting of titanium alloy and will play an important role in achieving sustainability in the industry.展开更多
As light metals,aluminum and magnesium have been widely used in automotive manufacturing,but the welding of Al/Mg joints is facing challenges.However,it is difficult to obtain high-quality aluminum/magnesium joints wi...As light metals,aluminum and magnesium have been widely used in automotive manufacturing,but the welding of Al/Mg joints is facing challenges.However,it is difficult to obtain high-quality aluminum/magnesium joints with traditional arc welding methods.As a solid-phase welding technology,ultrasonic metal welding has the characteristics of high welding efficiency and less welded defects.It is also suitable for welding sound metal bonds.Aluminum and magnesium ultrasonic welding has become a research hotspot.Therefore,the evolution of microstructures and mechanical performance of Al/Mg and multi-layer Al/Mg ultrasonic welding,and the new study works,including the molecular dynamic simulation of Al/Mg ultrasonic welding and hybrid based on ultrasonic welding are summarized.Furthermore,several promising research directions are proposed to guide in-depth investigations into the ultrasonic welding of Al/Mg dissimilar joints.展开更多
The composite structures/components made by friction stir lap welding(FSLW)of Mg alloy sheet and Al alloy sheet are of wide application potentials in the manufacturing sector of transportation vehicles.To further impr...The composite structures/components made by friction stir lap welding(FSLW)of Mg alloy sheet and Al alloy sheet are of wide application potentials in the manufacturing sector of transportation vehicles.To further improve the joint quality,the ultrasonic vibration(UV)is exerted in FSLW,and the UV enhanced FSLW(UVeFSLW)was developed for making Mg-to-Al dissimilar joints.The numerical analysis and experimental investigation were combined to study the process mechanism in Mg/Al UVeFSLW.An equation related to the temperature and strain rate was derived to calculate the grain size at different locations of the weld nugget zone,and the effect of grain size distribution on the threshold thermal stress was included,so that the prediction accuracy of flow stress was further improved.With such modified constitutive equation,the numerical simulation was conducted to compare the heat generation,temperature profiles and material flow behaviors in Mg/Al UVeFSLW/FSLW processes.It was found that the exerted UV decreased the temperature at two checking points on the tool/workpiece interface from 707/671 K in FSLW to 689/660 K in UVeFSLW,which suppressed the IMCs thickness at Mg-Al interface from 1.7μm in FSLW to 1.1μm in UVeFSLW.The exerted UV increased the horizontal materials flow ability,and decreased the upward flow ability,which resulted in the increase of effective sheet thickness/effective lap width from 2.01/3.70 mm in FSLW to 2.04/4.84 mm in UVeFSLW.Therefore,the ultrasonic vibration improved the tensile shear strength of Mg-to-Al lap joints by 18%.展开更多
Superior strength and high-temperature performance make γ-TiAl vital for lightweight aero-engines. However, its inherent brittleness poses machining problems. This study employed Elliptical Ultrasonic Vibration Milli...Superior strength and high-temperature performance make γ-TiAl vital for lightweight aero-engines. However, its inherent brittleness poses machining problems. This study employed Elliptical Ultrasonic Vibration Milling (EUVM) to address these problems. Considering the influence of machining parameters on vibration patterns of EUVM, a separation time model was established to analyze the vibration evolutionary process, thereby instructing the cutting mechanism. On this basis, deep discussions regarding chip formation, cutting force, edge breakage, and subsurface layer deformation were conducted for EUVM and Conventional Milling (CM). Chip morphology showed the chip formation was rooted in the periodic brittle fracture. Local dimples proved that the thermal effect of high-speed cutting improved the plasticity of γ-TiAl. EUVM achieved a maximum 18.17% reduction in cutting force compared with CM. The force variation mechanism differed with changes in the cutting speed or the vibration amplitude, and its correlation with thermal softening, strain hardening, and vibratory cutting effects was analyzed. EUVM attained desirable edge breakage by achieving smaller fracture lengths. The fracture mechanisms of different phases were distinct, causing a surge in edge fracture size of γ-TiAl under microstructural differences. In terms of subsurface deformation, EUVM also showed strengthening effects. Noteworthy, the lamellar deformation patterns under the cutting removal state differed from the quasi-static, which was categorized by the orientation angles. Additionally, the electron backscattering diffraction provided details of the influence of microstructural difference on the orientation and the deformation of grains in the subsurface layer. The results demonstrate that EUVM is a promising machining method for γ-TiAl and guide further research and development of EUVM γ-TiAl.展开更多
The purpose of this study is to analyze the application of ultrasonic non-destructive testing technology in bridge engineering.During the research phase,based on literature collection and reading,as well as the analys...The purpose of this study is to analyze the application of ultrasonic non-destructive testing technology in bridge engineering.During the research phase,based on literature collection and reading,as well as the analysis of bridge inspection materials,the principle of ultrasonic non-destructive testing technology and its adaptability to bridge engineering are elaborated.Subsequently,starting from the preparation work before inspection until damage assessment,the entire process of ultrasonic non-destructive testing is studied,and finally,a technical system of ultrasonic non-destructive testing for bridge engineering that runs through the entire process is formed.It is hoped that this article can provide technical reference value for relevant units in China,and promote the high-quality development of China’s bridge engineering from a macro perspective.展开更多
This paper introduces part of the content in the association standard,T/CAAM0002–2020 Nomenclature and Location of Acupuncture Points for Laboratory Animals Part 2:Rat.This standard was released by the China Associat...This paper introduces part of the content in the association standard,T/CAAM0002–2020 Nomenclature and Location of Acupuncture Points for Laboratory Animals Part 2:Rat.This standard was released by the China Association of Acupuncture and Moxibustion on May 15,2020,implemented on October 31,2020,and published by Standards Press of China.The standard was drafted by the Institute of Acupuncture and Moxibustion,China Academy of Chinese Medical Sciences,and the Nanjing University of Chinese Medicine.Principal draftsmen:Xiang-hong JING and Xing-bang HUA.Participating draftsmen:Wan-Zhu BAI,Bin XU,Dong-sheng XU,Yi GUO,Tie-ming MA,Xin-jun WANG,and Sheng-feng LU.展开更多
In general,the rapid growth of α-Fe clusters is a challenge in high Fe-content Fe-based amorphous alloys,negatively affecting their physical properties.Herein,we introduce an efficient and rapid post-treatment techni...In general,the rapid growth of α-Fe clusters is a challenge in high Fe-content Fe-based amorphous alloys,negatively affecting their physical properties.Herein,we introduce an efficient and rapid post-treatment technique known as ultrasonic vibration rapid processing(UVRP),which enables the formation of high-density strong magnetic α-Fe clusters,thereby enhancing the soft magnetic properties of Fe_(78)Si(13)B_(9) amorphous alloy ribbon.展开更多
The loaded rock experiences multiple stages of deformation.It starts with the formation of microcracks at low stresses(crack initiation,CI)and then transitions into unstable crack propagation(crack damage,CD)near the ...The loaded rock experiences multiple stages of deformation.It starts with the formation of microcracks at low stresses(crack initiation,CI)and then transitions into unstable crack propagation(crack damage,CD)near the ultimate strength.In this study,both the acoustic emission method(AEM)and the ultrasonic testing method(UTM)were used to examine the characteristics of AE parameters(b-value,peak frequency,frequency-band energy ratio,and fractal dimension)and ultrasonic(ULT)properties(velocity,amplitude,energy attenuation,and scattering attenuation)of bedded shale at CI,CD,and ultimate strength.The comparison involved analyzing the strain-based method(SBM),AEM,and UTM to determine the thresholds for damage stress.A fuzzy comprehensive evaluation model(FCEM)was created to describe the damage thresholds and hazard assessment.The results indicate that the optimal AE and ULT parameters for identifying CI and CD stress are ringing count,ultrasonic amplitude,energy attenuation,and scattering attenuation of the S-wave.Besides,damage thresholds were detected earlier by AE monitoring,ranging from 3 MPa to 10 MPa.CI and CD identified by UTM occurred later than SBM and AEM,and were in the range of 12 MPa.The b-value,peak frequency,energy ratio in the low-frequency band(0e62.5 kHz),correlation dimension,and sandbox dimension showed low values at the peak stress,while the energy ratio in a moderate-frequency band(187.5e281.25 kHz)and amplitude showed high values.The successful application of FCEM to laboratory testing of shales has demonstrated its ability to quantitatively identify AE/ULT precursors of seismic hazards associated with rock failure.展开更多
BiVO_(4)porous spheres modified by ZnO were designed and synthesized using a facile two-step method.The resulting ZnO/BiVO_(4)composite catalysts have shown remarkable efficiency as piezoelectric catalysts for degradi...BiVO_(4)porous spheres modified by ZnO were designed and synthesized using a facile two-step method.The resulting ZnO/BiVO_(4)composite catalysts have shown remarkable efficiency as piezoelectric catalysts for degrading Rhodamine B(RhB)unde mechanical vibrations,they exhibit superior activity compared to pure ZnO.The 40wt%ZnO/BiVO_(4)heterojunction composite displayed the highest activity,along with good stability and recyclability.The enhanced piezoelectric catalytic activity can be attributed to the form ation of an I-scheme heterojunction structure,which can effectively inhibit the electron-hole recombination.Furthermore,hole(h+)and superoxide radical(·O_(2)^(-))are proved to be the primary active species.Therefore,ZnO/BiVO_(4)stands as an efficient and stable piezoelectric catalyst with broad potential application in the field of environmental water pollution treatment.展开更多
Conductor materials with good mechanical performance as well as high electrical and thermal conductivities are particularly important to break through the current bottle-neck limit(~ 100 T) of pulsed magnets. Here, we...Conductor materials with good mechanical performance as well as high electrical and thermal conductivities are particularly important to break through the current bottle-neck limit(~ 100 T) of pulsed magnets. Here, we perform systematic studies on the elastic properties of the Cu–6wt% Ag alloy wire, which is a promising candidate material for the new-generation pulsed magnets, by employing two independent ultrasonic techniques, i.e., resonant ultrasound spectroscopy(RUS) and ultrasound pulse-echo experiments. Our RUS measurements manifest that the elastic properties of the Cu–6wt% Ag alloy wires can be improved by an electroplastic drawing procedure as compared with the conventional cold drawing. We also take this opportunity to test the availability of our newly-built ultrasound pulse-echo facility at the Wuhan National High Magnetic Field Center(WHMFC, China), and the results suggest that the elastic performance of the electroplastically-drawn Cu–6wt% Ag alloy wire remains excellent without anomalous softening under extreme conditions,e.g., in ultra-high magnetic field up to 50 T and nitrogen or helium cryogenic liquids.展开更多
Stainless steel parts with complex shape can be fabricated using additive manufacturing,which do not rely on molds and dies.However,coarse dendrites induced by repeated heating of additive manufacturing result in weak...Stainless steel parts with complex shape can be fabricated using additive manufacturing,which do not rely on molds and dies.However,coarse dendrites induced by repeated heating of additive manufacturing result in weak properties,which limits its application.In this study,an in-situ ultrasonic rolling(UR)device was developed to assist the laser directed energy deposition(LDED)process.The microstructural characteristics,as well as the microhardness and wear behavior,were studied for the 316L stainless steel manufactured by in-situ ultrasonic rolling assisted LDED.It is found that austenite,ferrite,and small Si oxides are the main constituents of both the LDED and LDED-UR alloy samples.Under the severe plastic deformation of ultrasonic rolling,the long-branched ferrites by LDED are transformed into the rod-like phases by LDED-UR.Meanwhile,the ferrite is more uniformly distributed in the LDED-UR alloy sample compared with that in LDED alloy sample.Columnar grains with the size of 97.85μm appear in the LDED alloy sample,which is larger than the fully equiaxed grains(22.35μm)of the LDED-UR alloy.The hardness of the LDED-UR alloy sample is about 266.13±13.62 HV_(0.2),which is larger than that of the LDED alloy sample(212.93±12.85 HV_(0.2)).Meanwhile,the wear resistance is also greatly enhanced by applying the assisted in-situ ultrasonic rolling.The achieved high wear resistance can be ascribed to the uniformly distributed hard matter(ferrites)and the impedance of dislocations by high fraction of grain boundaries.Abrasive wear and adhesive wear are identified as the primary wear mechanisms of the studied alloy.Gaining an in-depth understanding of the relationship between wear mechanisms and microstructures offers an effective approach in manufacturing high wear resistant alloys suitable for use in harsh working environments.展开更多
A low rare-earth containing ZEK100-O magnesium alloy was welded to AA1230-clad high-strength AA2024-T3 aluminum alloy via solidstate ultrasonic spot welding(USW)to evaluate the microstructure,tensile lap shear strengt...A low rare-earth containing ZEK100-O magnesium alloy was welded to AA1230-clad high-strength AA2024-T3 aluminum alloy via solidstate ultrasonic spot welding(USW)to evaluate the microstructure,tensile lap shear strength,and fatigue properties.The tensile strength increased with increasing welding energy,peaked at a welding energy of 1000 J,and then decreased due to the formation of an increasingly thick diffusion layer mainly containing Al12Mg17intermetallic compound at higher energy levels.The peak tensile lap shear strength attained at 1000 J was attributed to the optimal inter-diffusion between the magnesium alloy and softer AA1230-clad Al layer along with the presence of‘fishhook'-like mechanical interlocks at the weld interface and the formation of an indistinguishable intermetallic layer.The dissimilar joints welded at 1000 J also exhibited a longer fatigue life than other Mg-Al dissimilar joints,suggesting the beneficial role of the softer clad layer with a better intermingling capacity during USW.While the transverse-through-thickness(TTT)failure mode prevailed at lower cyclic loading levels,interfacial failure was the predominant mode of fatigue failure at higher cyclic loads,where distinctive fatigue striations were also observed on the fracture surface of the softer clad Al layer.This was associated with the presence of opening stress and bending moment near the nugget edge despite the tension-tension lap shear cyclic loading applied.展开更多
Under the laser directed energy deposition(LDED)process,the rapid melting and solidification usually lead to the emergence of pores and coarse columnar dendrites,which in turn compromise the properties of the deposite...Under the laser directed energy deposition(LDED)process,the rapid melting and solidification usually lead to the emergence of pores and coarse columnar dendrites,which in turn compromise the properties of the deposited alloys.This study introduced in-situ ultrasonic rolling(UR)as an innovative method to enhance the corrosion resistance of LDED specimens,and the microstructural characteristics and their correlation with corrosion resistance were deeply investigated.The findings reveal that the LDED-UR specimen exhibits a reduction in both the fraction and size of pores.Under the influence of severe plastic deformation generated by LDED-UR process,fully equiaxed grains appear with a reduced average size of 28.61μm(compared to63.98μm for the LDED specimen with columnar grains).The electrochemical corrosion resistance of the LDED-UR specimen is significantly enhanced compared to the LDED specimen.This enhanced corrosion resistance can be attributed to the low fraction of small-sized pores,the fine and uniformly distributed Cr-enriched ferrite phase,and the formation of a compact and thick passive film due to dense grain boundaries.The insight of the correlation between microstructure and corrosion behavior opens up a new pathway to enhance the corrosion resistance of LDED specimens.展开更多
The Mg-9Li-1Zn(LZ91)alloy was subjected to an ultrasonic surface rolling process(USRP)with varying passes for the purpose of modifying its surface state.The USRP transformed surface residual stress from initial tensil...The Mg-9Li-1Zn(LZ91)alloy was subjected to an ultrasonic surface rolling process(USRP)with varying passes for the purpose of modifying its surface state.The USRP transformed surface residual stress from initial tensile stress to compressive stress,decreasing the surface roughness and increasing the ratio of the β-Li phase.The USRPed LZ91 sample(3 passes)showed superior corrosion resistance,with the corrosion current density changing from 57.11 to 24.70μA cm^(-2),and the polarization resistance increasing from 576.3 to 1146.1Ωcm^(2).According to the corrosion procedure evaluations,in situ observation revealed that the LZ91 alloy initially experiences pitting,which subsequently develops into cracking.The substantial area coverage of the β-Li phase facilitates the formation of a protective film on the surface,effectively delaying localized corrosion.展开更多
基金supported by the National Natural Science Foundation of China (Grant No. 5186504)the University Science Foundation for Young Science and Technology Talents in Inner Mongolia Autonomous Region of China (Grant No. NJYT22078)+2 种基金the Basic Scientific Research Expenses Program of Universities directly under Inner Mongolia Autonomous Region (Grant No. JY20220059)the Inner Mongolia Autonomous Region ‘Grassland Talent’ project Young Innovative Talent Training Program Level ⅠBasic Research Expenses of Universities directly under the Inner Mongolia Autonomous Region (Grant No. ZTY2023040)。
文摘To develop a suitable production process for fiber reinforced investment casting shell mold,three methods were studied:the traditional method(M_(1)),the method of adding fiber into silica sol with mechanical stirring and ultrasonic agitation(M_(2)),and the method of adding fiber into slurry with mechanical stirring and ultrasonic agitation for durations of 3,15,30,and 45 min(M_(3)).The bending strength,high-temperature self-load deformation,and thermal conductivity of the shell molds were investigated.The results reveal that the enhancement of fiber dispersion through ultrasonic agitation improves the comprehensive performance of the shell molds.The maximum green bending strength of the shell mold by M_(2) reaches 3.29 MPa,which is 29% higher than that of the shell mold prepared by M_(1).Moreover,the high-temperature self-load deformation of the shell mold is reduced from 0.62% to 0.44%.In addition,simultaneous ultrasonic agitation and mechanical stirring effectively shorten the slurry preparation time while maintaining comparable levels of fiber dispersion.With the process M_(3)-45 min,the fillers are uniformly dispersed in the slurry,and the fired bending strength and the high-temperature self-load deformation reach 6.25 MPa and 0.41%,respectively.Therefore,the proposed ultrasonic agitation route is promising for the fabrication of fiber-reinforced shell molds with excellent fibers dispersion.
基金supported by the National Natural Science Foundation of China(No.52205468,No.52275431,No.52375186)China Postdoctoral Science Foundation(No.2025M771349)Zhejiang Province Natural Science Foundation(No.LD22E050001)。
文摘The latest generation of aero engines has set higher standards for thrust-to-weight ratio and energy conversion efficiency,making it imperative to address the challenge of efficiently and accurately machining film cooling holes.It has been demonstrated that conventional long-pulse lasers are incapable of meeting the elevated quality surface finish requirements for these holes,a consequence of the severe thermal defects.The employment of backside water-assisted laser drilling technology confers a number of distinct advantages in terms of mitigating laser thermal damage,thus representing a highly promising solution to this challenge.However,significant accumulation of bubbles and machining products during the backside water-assisted laser drilling process has been demonstrated to have a detrimental effect on laser transmission and machining stability,thereby reducing machining quality.In order to surmount these challenges,a novel method has been proposed,namely an ultrasonic shock water flow-assisted picosecond laser drilling technique.Numerical models for ultrasonic acoustic streaming and particle tracking for machining product transport have been established to investigate the mechanism.The simulation results demonstrated that the majority of the machining products could rapidly move away from the machining area because of the action of acoustic streaming,thereby avoiding the accumulation of bubbles and products.Subsequent analysis,comparing the process performance in micro-hole machining,confirmed that the ultrasonic field could effectively eliminate bubble and chip accumulation,thus significantly improving micro-hole quality.Furthermore,the impact of ultrasonic and laser parameters on micro-hole quality under varying machining methods was thoroughly investigated.The findings demonstrated that the novel methodology outlined in this study yielded superior-quality micro-holes at elevated ultrasonic and laser power levels,in conjunction with reduced laser frequency and scanning velocity.The taper of the micro-holes produced by the new method was reduced by more than 25%compared with the other conventional methods.
基金supported by the National Key Research and Development Program of China(No.2024YFB3212901)National Natural Science Foundation of China(12072189)the Medicine and Engineering Interdisciplinary Research Fund of Shanghai Jiao Tong University(No.YG2025ZD05)。
文摘Pipelines are extensively used in environments such as nuclear power plants,chemical factories,and medical devices to transport gases and liquids.These tubular environments often feature complex geometries,confined spaces,and millimeter-scale height restrictions,presenting significant challenges to conventional inspection methods.Here,we present an ultrasonic microrobot(weight,80 mg;dimensions,24 mm×7 mm;thickness,210μm)to realize agile and bidirectional navigation in narrow pipelines.The ultrathin structural design of the robot is achieved through a high-performance piezoelectric composite film microstructure based on MEMS technology.The robot exhibits various vibration modes when driven by ultrasonic frequency signals,its motion speed reaches81 cm s-1 at 54.8 k Hz,exceeding that of the fastest piezoelectric microrobots,and its forward and backward motion direction is controllable through frequency modulation,while the minimum driving voltage for initial movement can be as low as 3 VP-P.Additionally,the robot can effortlessly climb slopes up to 24.25°and carry loads more than 36 times its weight.The robot is capable of agile navigation through curved L-shaped pipes,pipes made of various materials(acrylic,stainless steel,and polyvinyl chloride),and even over water.To further demonstrate its inspection capabilities,a micro-endoscope camera is integrated into the robot,enabling real-time image capture inside glass pipes.
基金Item Sponsored by National Natural Science Foundation of China(61171145,11274226)
文摘P91 steel is an important bearing material used in nuclear power plants. The study of its mechanical degradation behavior is important for ensuring safe operation. The relationship between the dislocation density of P91 steel under different strains and the corresponding nonlinear ultrasonic parameter β was studied. The dislocation density of strained samples was estimated by X-ray diffraction. Nonlinear ultrasonic testing was conducted to evaluate β, showing that this value increased with increasing dislocation density induced by different tensile elongations. It was shown that the ultrasonic secondharmonic generation technique can effectively evaluate the degradation behavior of metallic materials, and the prediction of the residual life of bearing parts in service can be made based on β and the dislocation density.
基金supported by the National Nat-ural Science Foundation of China(No.52175310)A part of the work was also supported by the National Science and Technology Major Project(No.2017-VI-0009-0080)+1 种基金the Guang-dong Province Key Research and Development Program(No.2019B010935001)and the Shenzhen Science and Technology Plan(No.GXWD20201230155427003-20200821172456002).
文摘The coupling effects of ultrasonic excitation and high-strain-rate deformation are the core factors for weld formation during ultrasonic welding.However,interfacial deformation behavior still shrouds in uncer-tainty because of the contradictory features between mutual dislocation retardation caused by severely frictional deformation and ultrasonic-accelerated dislocation motion.[101]and[111]-oriented Cu single crystals which tended to form geometrically necessary boundaries(GNBs)were selected as the welding substrates to trace the uniquely acoustoplastic effects in the interfacial region under the ultrasonically excited high-strain-rate deformation.It was indicated that for a low energy input,micro-welds localized at the specific interface region,and equiaxed dislocation cells substituting for GNBs dominated in the ini-tial single crystal rotation region.As the welding energy increased,continuous shear deformation drove the dynamic recrystallization region covered by equiaxed grains to spread progressively.Limited discrete dislocations inside the recrystallized grains and nascent dislocation cells at the grain boundaries were ob-served in[101]and[111]joints simultaneously,suggesting that the ultrasonic excitation promoted motion of intragranular dislocation and pile-up along the sub-grain boundaries.The interfacial morphology be-fore and after expansion of recrystallization region all exhibited the weakening of orientation constraint on dislocation motion,which was also confirmed by the similar micro-hardness in joint interface.The first-principle calculation and applied strain-rate analysis further revealed that ultrasonic excitation en-hanced dislocation slipping,and enabled dislocation motion to accommodate severe plastic deformation at a high-strain-rate.
文摘This paper introduces part of the content in the association standard,T/CAAM0002–2020 Nomenclature and Location of Acupuncture Points for Laboratory Animals Part 3:Mouse.This standard was released by the China Association of Acupuncture and Moxibustion on May 15,2020,implemented on October 31,2020,and published by Standards Press of China.The standard was drafted by the Institute of Acupuncture and Moxibustion,China Academy of Chinese Medical Sciences,and the Nanjing University of Chinese Medicine.Principal draftsmen:Xiang-hong JING and Xing-bang HUA.Participating draftsmen:Wan-zhu BAI,Bin XU,Dong-sheng XU,Yi GUO,Tie-ming MA,Xin-jun WANG,and Sheng-feng LU.
基金financially supported by the National Natural Science Foundation of China(Nos.92160301,92060203,52175415 and 52205475)the Science Center for Gas Turbine Project(No.P2023-B-IV-003-001)+1 种基金the Natural Science Foundation of Jiangsu Province(No.BK20210295)the Huaqiao University Engineering Research Center of Brittle Materials Machining(MOE,2023IME-001)。
文摘The remarkable ability of titanium alloys to preserve their superior physical and chemical characteristics when subjected to extreme conditions significantly enhances their importance in the aerospace,military,and medical sectors.However,conventional machining of titanium alloys leads to elevated tool wear,development of surface defects,and reduced machining efficiency due to their low heat conductivity,and chemical affinity.These issues can be somewhat counteracted by integrating ultrasonic vibration in the conventional machining of titanium alloys and also enhance sustainability.This review article offers a holistic evaluation of the influence of ultrasonic vibration-assisted milling and turning on cutting forces,temperature,tool wear,and surface integrity,encompassing surface morphology,surface roughness,surface residual stress,surface hardness,and surface tribological properties during titanium alloys machining.Furthermore,it investigates the sustainability aspect that has not been previously examined.Studies on the performance of ultrasonic-assisted cutting revealed several advantages,including decreased cutting forces and cutting temperature,improved tool life,and a better-machined surface during machining.Consequently,the sustainability factor is improved due to minimized energy consumption and residual waste.In conclusion,the key challenges and future prospects in the ultrasonic-assisted cutting of titanium alloys are also discussed.This review article provides beneficial knowledge for manufactur-ers and researchers regarding ultrasonic vibration-assisted cutting of titanium alloy and will play an important role in achieving sustainability in the industry.
基金supported by Key Projects of Science and Technology Research Plan of Hubei Provincial Department of Education(D20221306)the National Natural Science Foundation of China(51605103)Key Project of Hubei Provincial Science and Technology Department(2020BAB055).
文摘As light metals,aluminum and magnesium have been widely used in automotive manufacturing,but the welding of Al/Mg joints is facing challenges.However,it is difficult to obtain high-quality aluminum/magnesium joints with traditional arc welding methods.As a solid-phase welding technology,ultrasonic metal welding has the characteristics of high welding efficiency and less welded defects.It is also suitable for welding sound metal bonds.Aluminum and magnesium ultrasonic welding has become a research hotspot.Therefore,the evolution of microstructures and mechanical performance of Al/Mg and multi-layer Al/Mg ultrasonic welding,and the new study works,including the molecular dynamic simulation of Al/Mg ultrasonic welding and hybrid based on ultrasonic welding are summarized.Furthermore,several promising research directions are proposed to guide in-depth investigations into the ultrasonic welding of Al/Mg dissimilar joints.
基金supported by the National Natural Science Foundation of China(Grant No.52035005)the Key R&D Program of Shandong Province in China(Grant No.2021ZLGX01).
文摘The composite structures/components made by friction stir lap welding(FSLW)of Mg alloy sheet and Al alloy sheet are of wide application potentials in the manufacturing sector of transportation vehicles.To further improve the joint quality,the ultrasonic vibration(UV)is exerted in FSLW,and the UV enhanced FSLW(UVeFSLW)was developed for making Mg-to-Al dissimilar joints.The numerical analysis and experimental investigation were combined to study the process mechanism in Mg/Al UVeFSLW.An equation related to the temperature and strain rate was derived to calculate the grain size at different locations of the weld nugget zone,and the effect of grain size distribution on the threshold thermal stress was included,so that the prediction accuracy of flow stress was further improved.With such modified constitutive equation,the numerical simulation was conducted to compare the heat generation,temperature profiles and material flow behaviors in Mg/Al UVeFSLW/FSLW processes.It was found that the exerted UV decreased the temperature at two checking points on the tool/workpiece interface from 707/671 K in FSLW to 689/660 K in UVeFSLW,which suppressed the IMCs thickness at Mg-Al interface from 1.7μm in FSLW to 1.1μm in UVeFSLW.The exerted UV increased the horizontal materials flow ability,and decreased the upward flow ability,which resulted in the increase of effective sheet thickness/effective lap width from 2.01/3.70 mm in FSLW to 2.04/4.84 mm in UVeFSLW.Therefore,the ultrasonic vibration improved the tensile shear strength of Mg-to-Al lap joints by 18%.
基金co-supported by the Science Center for Gas Turbine Project, China(No. P2022-AB-IV-001-002)the National Natural Science Foundation of China (No. 91960203)+1 种基金the Fundamental Research Funds for the Central Universities (No. D5000230048)the Innovation Capability Support Program of Shaanxi (No. 2022TD-60)
文摘Superior strength and high-temperature performance make γ-TiAl vital for lightweight aero-engines. However, its inherent brittleness poses machining problems. This study employed Elliptical Ultrasonic Vibration Milling (EUVM) to address these problems. Considering the influence of machining parameters on vibration patterns of EUVM, a separation time model was established to analyze the vibration evolutionary process, thereby instructing the cutting mechanism. On this basis, deep discussions regarding chip formation, cutting force, edge breakage, and subsurface layer deformation were conducted for EUVM and Conventional Milling (CM). Chip morphology showed the chip formation was rooted in the periodic brittle fracture. Local dimples proved that the thermal effect of high-speed cutting improved the plasticity of γ-TiAl. EUVM achieved a maximum 18.17% reduction in cutting force compared with CM. The force variation mechanism differed with changes in the cutting speed or the vibration amplitude, and its correlation with thermal softening, strain hardening, and vibratory cutting effects was analyzed. EUVM attained desirable edge breakage by achieving smaller fracture lengths. The fracture mechanisms of different phases were distinct, causing a surge in edge fracture size of γ-TiAl under microstructural differences. In terms of subsurface deformation, EUVM also showed strengthening effects. Noteworthy, the lamellar deformation patterns under the cutting removal state differed from the quasi-static, which was categorized by the orientation angles. Additionally, the electron backscattering diffraction provided details of the influence of microstructural difference on the orientation and the deformation of grains in the subsurface layer. The results demonstrate that EUVM is a promising machining method for γ-TiAl and guide further research and development of EUVM γ-TiAl.
文摘The purpose of this study is to analyze the application of ultrasonic non-destructive testing technology in bridge engineering.During the research phase,based on literature collection and reading,as well as the analysis of bridge inspection materials,the principle of ultrasonic non-destructive testing technology and its adaptability to bridge engineering are elaborated.Subsequently,starting from the preparation work before inspection until damage assessment,the entire process of ultrasonic non-destructive testing is studied,and finally,a technical system of ultrasonic non-destructive testing for bridge engineering that runs through the entire process is formed.It is hoped that this article can provide technical reference value for relevant units in China,and promote the high-quality development of China’s bridge engineering from a macro perspective.
文摘This paper introduces part of the content in the association standard,T/CAAM0002–2020 Nomenclature and Location of Acupuncture Points for Laboratory Animals Part 2:Rat.This standard was released by the China Association of Acupuncture and Moxibustion on May 15,2020,implemented on October 31,2020,and published by Standards Press of China.The standard was drafted by the Institute of Acupuncture and Moxibustion,China Academy of Chinese Medical Sciences,and the Nanjing University of Chinese Medicine.Principal draftsmen:Xiang-hong JING and Xing-bang HUA.Participating draftsmen:Wan-Zhu BAI,Bin XU,Dong-sheng XU,Yi GUO,Tie-ming MA,Xin-jun WANG,and Sheng-feng LU.
基金supported by the Major Science and Technology Project of Zhongshan City(No.2022AJ004)the Key Basic and Applied Research Program of Guangdong Province(Nos.2019B030302010 and 2022B1515120082)Guangdong Science and Technology Innovation Project(No.2021TX06C111).
文摘In general,the rapid growth of α-Fe clusters is a challenge in high Fe-content Fe-based amorphous alloys,negatively affecting their physical properties.Herein,we introduce an efficient and rapid post-treatment technique known as ultrasonic vibration rapid processing(UVRP),which enables the formation of high-density strong magnetic α-Fe clusters,thereby enhancing the soft magnetic properties of Fe_(78)Si(13)B_(9) amorphous alloy ribbon.
基金financially supported by the National Natural Science Foundation of China(Grant Nos.U20A20266 and 12302503)Scientific and technological research projects in Sichuan province(Grant No.2024NSFSC0973).
文摘The loaded rock experiences multiple stages of deformation.It starts with the formation of microcracks at low stresses(crack initiation,CI)and then transitions into unstable crack propagation(crack damage,CD)near the ultimate strength.In this study,both the acoustic emission method(AEM)and the ultrasonic testing method(UTM)were used to examine the characteristics of AE parameters(b-value,peak frequency,frequency-band energy ratio,and fractal dimension)and ultrasonic(ULT)properties(velocity,amplitude,energy attenuation,and scattering attenuation)of bedded shale at CI,CD,and ultimate strength.The comparison involved analyzing the strain-based method(SBM),AEM,and UTM to determine the thresholds for damage stress.A fuzzy comprehensive evaluation model(FCEM)was created to describe the damage thresholds and hazard assessment.The results indicate that the optimal AE and ULT parameters for identifying CI and CD stress are ringing count,ultrasonic amplitude,energy attenuation,and scattering attenuation of the S-wave.Besides,damage thresholds were detected earlier by AE monitoring,ranging from 3 MPa to 10 MPa.CI and CD identified by UTM occurred later than SBM and AEM,and were in the range of 12 MPa.The b-value,peak frequency,energy ratio in the low-frequency band(0e62.5 kHz),correlation dimension,and sandbox dimension showed low values at the peak stress,while the energy ratio in a moderate-frequency band(187.5e281.25 kHz)and amplitude showed high values.The successful application of FCEM to laboratory testing of shales has demonstrated its ability to quantitatively identify AE/ULT precursors of seismic hazards associated with rock failure.
基金financially supported by the National Natural Science Foundation of China(No.22272151)Public Welfare Technology Application Research Project of Jinhua City,China(No.2023-4-022)。
文摘BiVO_(4)porous spheres modified by ZnO were designed and synthesized using a facile two-step method.The resulting ZnO/BiVO_(4)composite catalysts have shown remarkable efficiency as piezoelectric catalysts for degrading Rhodamine B(RhB)unde mechanical vibrations,they exhibit superior activity compared to pure ZnO.The 40wt%ZnO/BiVO_(4)heterojunction composite displayed the highest activity,along with good stability and recyclability.The enhanced piezoelectric catalytic activity can be attributed to the form ation of an I-scheme heterojunction structure,which can effectively inhibit the electron-hole recombination.Furthermore,hole(h+)and superoxide radical(·O_(2)^(-))are proved to be the primary active species.Therefore,ZnO/BiVO_(4)stands as an efficient and stable piezoelectric catalyst with broad potential application in the field of environmental water pollution treatment.
基金Project supported by the National Key R&D Program of China (Grant Nos. 2022YFA1602602 and 2023YFA1609600)the National Natural Science Foundation of China (Grant No. U23A20580)+3 种基金the open research fund of Songshan Lake Materials Laboratory (Grant No. 2022SLABFN27)Beijing National Laboratory for Condensed Matter Physics (Grant No. 2024BNLCMPKF004)Guangdong Basic and Applied Basic Research Foundation (Grant No. 2022B1515120020)the interdisciplinary program of Wuhan National High Magnetic Field Center at Huazhong University of Science and Technology (Grant No. WHMFC202132)。
文摘Conductor materials with good mechanical performance as well as high electrical and thermal conductivities are particularly important to break through the current bottle-neck limit(~ 100 T) of pulsed magnets. Here, we perform systematic studies on the elastic properties of the Cu–6wt% Ag alloy wire, which is a promising candidate material for the new-generation pulsed magnets, by employing two independent ultrasonic techniques, i.e., resonant ultrasound spectroscopy(RUS) and ultrasound pulse-echo experiments. Our RUS measurements manifest that the elastic properties of the Cu–6wt% Ag alloy wires can be improved by an electroplastic drawing procedure as compared with the conventional cold drawing. We also take this opportunity to test the availability of our newly-built ultrasound pulse-echo facility at the Wuhan National High Magnetic Field Center(WHMFC, China), and the results suggest that the elastic performance of the electroplastically-drawn Cu–6wt% Ag alloy wire remains excellent without anomalous softening under extreme conditions,e.g., in ultra-high magnetic field up to 50 T and nitrogen or helium cryogenic liquids.
基金supports from the National Natural Science Foundation of China(No.52305440)the Natural Science Foundation of Changsha City(Nos.kq2208272,kq2208274)+1 种基金the Tribology Science Fund of the State Key Laboratory of Tribology in Advanced Equipment(No.SKLTKF22B09)the National Key Research and Development Program of China(No.2022YFB3706902)were acknowledged.
文摘Stainless steel parts with complex shape can be fabricated using additive manufacturing,which do not rely on molds and dies.However,coarse dendrites induced by repeated heating of additive manufacturing result in weak properties,which limits its application.In this study,an in-situ ultrasonic rolling(UR)device was developed to assist the laser directed energy deposition(LDED)process.The microstructural characteristics,as well as the microhardness and wear behavior,were studied for the 316L stainless steel manufactured by in-situ ultrasonic rolling assisted LDED.It is found that austenite,ferrite,and small Si oxides are the main constituents of both the LDED and LDED-UR alloy samples.Under the severe plastic deformation of ultrasonic rolling,the long-branched ferrites by LDED are transformed into the rod-like phases by LDED-UR.Meanwhile,the ferrite is more uniformly distributed in the LDED-UR alloy sample compared with that in LDED alloy sample.Columnar grains with the size of 97.85μm appear in the LDED alloy sample,which is larger than the fully equiaxed grains(22.35μm)of the LDED-UR alloy.The hardness of the LDED-UR alloy sample is about 266.13±13.62 HV_(0.2),which is larger than that of the LDED alloy sample(212.93±12.85 HV_(0.2)).Meanwhile,the wear resistance is also greatly enhanced by applying the assisted in-situ ultrasonic rolling.The achieved high wear resistance can be ascribed to the uniformly distributed hard matter(ferrites)and the impedance of dislocations by high fraction of grain boundaries.Abrasive wear and adhesive wear are identified as the primary wear mechanisms of the studied alloy.Gaining an in-depth understanding of the relationship between wear mechanisms and microstructures offers an effective approach in manufacturing high wear resistant alloys suitable for use in harsh working environments.
基金the National Natural Science Foundation of China(Grant No.51971183)supported by OU(Osaka University,Japan)program for multilateral international collaboration research in joining and welding。
文摘A low rare-earth containing ZEK100-O magnesium alloy was welded to AA1230-clad high-strength AA2024-T3 aluminum alloy via solidstate ultrasonic spot welding(USW)to evaluate the microstructure,tensile lap shear strength,and fatigue properties.The tensile strength increased with increasing welding energy,peaked at a welding energy of 1000 J,and then decreased due to the formation of an increasingly thick diffusion layer mainly containing Al12Mg17intermetallic compound at higher energy levels.The peak tensile lap shear strength attained at 1000 J was attributed to the optimal inter-diffusion between the magnesium alloy and softer AA1230-clad Al layer along with the presence of‘fishhook'-like mechanical interlocks at the weld interface and the formation of an indistinguishable intermetallic layer.The dissimilar joints welded at 1000 J also exhibited a longer fatigue life than other Mg-Al dissimilar joints,suggesting the beneficial role of the softer clad layer with a better intermingling capacity during USW.While the transverse-through-thickness(TTT)failure mode prevailed at lower cyclic loading levels,interfacial failure was the predominant mode of fatigue failure at higher cyclic loads,where distinctive fatigue striations were also observed on the fracture surface of the softer clad Al layer.This was associated with the presence of opening stress and bending moment near the nugget edge despite the tension-tension lap shear cyclic loading applied.
基金financial supports from the National Natural Science Foundation of China (No.52305440)the Natural Science Foundation of Changsha City (Nos.kq2208272,kq2208274)+1 种基金the Tribology Science Fund of the State Key Laboratory of Tribology in Advanced Equipment (SKLTKF22B09)the National Key Research and Development Program of China (2022YFB3706902)。
文摘Under the laser directed energy deposition(LDED)process,the rapid melting and solidification usually lead to the emergence of pores and coarse columnar dendrites,which in turn compromise the properties of the deposited alloys.This study introduced in-situ ultrasonic rolling(UR)as an innovative method to enhance the corrosion resistance of LDED specimens,and the microstructural characteristics and their correlation with corrosion resistance were deeply investigated.The findings reveal that the LDED-UR specimen exhibits a reduction in both the fraction and size of pores.Under the influence of severe plastic deformation generated by LDED-UR process,fully equiaxed grains appear with a reduced average size of 28.61μm(compared to63.98μm for the LDED specimen with columnar grains).The electrochemical corrosion resistance of the LDED-UR specimen is significantly enhanced compared to the LDED specimen.This enhanced corrosion resistance can be attributed to the low fraction of small-sized pores,the fine and uniformly distributed Cr-enriched ferrite phase,and the formation of a compact and thick passive film due to dense grain boundaries.The insight of the correlation between microstructure and corrosion behavior opens up a new pathway to enhance the corrosion resistance of LDED specimens.
基金financially supported by the National Natural Science Foundation of China(No.52271091)the National Key Research and Development Program of China(No.2021YFB3701100)the Natural Science Foundation Project of Ningxia Province(No.2023AAC03324).
文摘The Mg-9Li-1Zn(LZ91)alloy was subjected to an ultrasonic surface rolling process(USRP)with varying passes for the purpose of modifying its surface state.The USRP transformed surface residual stress from initial tensile stress to compressive stress,decreasing the surface roughness and increasing the ratio of the β-Li phase.The USRPed LZ91 sample(3 passes)showed superior corrosion resistance,with the corrosion current density changing from 57.11 to 24.70μA cm^(-2),and the polarization resistance increasing from 576.3 to 1146.1Ωcm^(2).According to the corrosion procedure evaluations,in situ observation revealed that the LZ91 alloy initially experiences pitting,which subsequently develops into cracking.The substantial area coverage of the β-Li phase facilitates the formation of a protective film on the surface,effectively delaying localized corrosion.
