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Quantitative analysis of γ-oryzanol content in cold pressed rice bran oil by TLC-image analysis method 被引量:7
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作者 Apirak Sakunpak Jirapornchai Suksaeree +2 位作者 Chaowalit Monton Pathamaporn Pathompak Krisana Kraisintu 《Asian Pacific Journal of Tropical Biomedicine》 SCIE CAS 2014年第2期119-123,共5页
Objective:To develop and validate an image analysis method for quantitative analysis ofγ-oryzanol in cold pressed rice bran oil.Methods:TLC-densitometric and TLC-image analysis methods were developed,validated,and us... Objective:To develop and validate an image analysis method for quantitative analysis ofγ-oryzanol in cold pressed rice bran oil.Methods:TLC-densitometric and TLC-image analysis methods were developed,validated,and used for quantitative analysis of γ-oryzanol in cold pressed rice bran oil.The results obtained by these two different quantification methods were compared by paired t-test.Results:Both assays provided good linearity,accuracy,reproducibility and selectivity for determination of γ-oryzanol.Conclusions:The TLC-densitomelric and TLC-image analysis methods providett a similar reproducibility,accuracy and selectivity for the quantitative determination of γ-oryzanol in cold pressed rice bran oil.A statistical comparison of the quantitative determinations of γ-oryzanol in samples did not show any statistically significant difference between TLC-densitometric and TLC-image analysis methods.As both methods were found to be equal,they therefore can be used for the determination of γ-oryzanol in cold pressed rice bran oil. 展开更多
关键词 γ-Oryzanol TLC-densitometric method TLC-image analysis method Rice BRAN oil quantitative analysis
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Comparison of Calibration Curve Method and Partial Least Square Method in the Laser Induced Breakdown Spectroscopy Quantitative Analysis 被引量:1
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作者 Zhi-bo Cong Lan-xiang Sun +2 位作者 Yong Xin Yang Li Li-feng Qi 《Journal of Computer and Communications》 2013年第7期14-18,共5页
The Laser Induced Breakdown Spectroscopy (LIBS) is a fast, non-contact, no sample preparation analytic technology;it is very suitable for on-line analysis of alloy composition. In the copper smelting industry, analysi... The Laser Induced Breakdown Spectroscopy (LIBS) is a fast, non-contact, no sample preparation analytic technology;it is very suitable for on-line analysis of alloy composition. In the copper smelting industry, analysis and control of the copper alloy concentration affect the quality of the products greatly, so LIBS is an efficient quantitative analysis tech- nology in the copper smelting industry. But for the lead brass, the components of Pb, Al and Ni elements are very low and the atomic emission lines are easily submerged under copper complex characteristic spectral lines because of the matrix effects. So it is difficult to get the online quantitative result of these important elements. In this paper, both the partial least squares (PLS) method and the calibration curve (CC) method are used to quantitatively analyze the laser induced breakdown spectroscopy data which is obtained from the standard lead brass alloy samples. Both the major and trace elements were quantitatively analyzed. By comparing the two results of the different calibration method, some useful results were obtained: both for major and trace elements, the PLS method was better than the CC method in quantitative analysis. And the regression coefficient of PLS method is compared with the original spectral data with background interference to explain the advantage of the PLS method in the LIBS quantitative analysis. Results proved that the PLS method used in laser induced breakdown spectroscopy was suitable for simultaneous quantitative analysis of different content elements in copper smelting industry. 展开更多
关键词 LASER-INDUCED BREAKDOWN Spectroscopy (LIBS) PARTIAL Least SQUARE method (PLS) Matrix Effects quantitative analysis
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Simplified quantitative analysis method and its application in the insitu synthesized copper-based azide chips
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作者 Jie Ren Yunfeng Li +3 位作者 Mingyu Li Xingyu Wu Jiabao Wang Qingxuan Zeng 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2024年第2期309-316,共8页
Copper-based azide(Cu(N_(3))2 or CuN_(3),CA)chips synthesized by in-situ azide reaction and utilized in miniaturized explosive systems has become a hot research topic in recent years.However,the advantages of in-situ ... Copper-based azide(Cu(N_(3))2 or CuN_(3),CA)chips synthesized by in-situ azide reaction and utilized in miniaturized explosive systems has become a hot research topic in recent years.However,the advantages of in-situ synthesis method,including small size and low dosage,bring about difficulties in quantitative analysis and differences in ignition capabilities of CA chips.The aim of present work is to develop a simplified quantitative analysis method for accurate and safe analysis of components in CA chips to evaluate and investigate the corresponding ignition ability.In this work,Cu(N_(3))2 and CuN_(3)components in CA chips were separated through dissolution and distillation by utilizing the difference in solubility and corresponding content was obtained by measuring N_(3)-concentration through spectrophotometry.The spectrophotometry method was optimized by studying influencing factors and the recovery rate of different separation methods was studied,ensuring the accuracy and reproducibility of test results.The optimized method is linear in range from 1.0-25.0 mg/L,with a correlation coefficient R^(2)=0.9998,which meets the requirements of CA chips with a milligram-level content test.Compared with the existing ICP method,component analysis results of CA chips obtained by spectrophotometry are closer to real component content in samples and have satisfactory accuracy.Moreover,as its application in miniaturized explosive systems,the ignition ability of CA chips with different component contents for direct ink writing CL-20 and the corresponding mechanism was studied.This study provided a basis and idea for the design and performance evaluation of CA chips in miniaturized explosive systems. 展开更多
关键词 Copper-based azide chips SPECTROPHOTOMETRY Separation method quantitative analysis Ignition ability
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QUANTITATIVE ANALYSIS OF VERY WEAK ACID AND BASE BY pH-FIXED TITRATION METHOD
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作者 Gang XU Ping WEI Yu Cheng XIE Xing Dong YU(Jiangsu Institute of Chemical Technology,Changzhou,213016) 《Chinese Chemical Letters》 SCIE CAS CSCD 1990年第1期81-84,共4页
pH-fixed titration method for the determination of weak acids and bases has been studied in this paper.It is not necessary to know the ionization constant of weak acid or base and the concentration of titrant. This me... pH-fixed titration method for the determination of weak acids and bases has been studied in this paper.It is not necessary to know the ionization constant of weak acid or base and the concentration of titrant. This method had been applied to determine phenol,4-aminoantipyrine and glycine,whose ionization constants range from 10^(-10)to 10^(-12).The results were satisfactory. 展开更多
关键词 AATP ACID quantitative analysis OF VERY WEAK ACID AND BASE BY pH-FIXED TITRATION method ACID pH
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Improvement of quantitative analysis of molybdenum element using PLS-based approaches for laser-induced breakdown spectroscopy in various pressure environments 被引量:3
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作者 Jiamin LIU Ding WU +4 位作者 Cailong FU Ran HAI Xiao YU Liying SUN Hongbin DING 《Plasma Science and Technology》 SCIE EI CAS CSCD 2019年第3期140-147,共8页
An experimental setup has been designed and realized in order to optimize the characteristics of laser-induced breakdown spectroscopy system working in various pressure environments. An approach combined the normaliza... An experimental setup has been designed and realized in order to optimize the characteristics of laser-induced breakdown spectroscopy system working in various pressure environments. An approach combined the normalization methods with the partial least squares(PLS) method are developed for quantitative analysis of molybdenum(Mo) element in the multi-component alloy,which is the first wall material in the Experimental Advanced Superconducting Tokamak. In this study, the different spectral normalization methods(total spectral area normalization,background normalization, and reference line normalization) are investigated for reducing the uncertainty and improving the accuracy of spectral measurement. The results indicates that the approach of PLS based on inter-element interference is significantly better than the conventional PLS methods as well as the univariate linear methods in the various pressure for molybdenum element analysis. 展开更多
关键词 laser induced BREAKDOWN spectroscopy MOLYBDENUM VACUUM NORMALIZATION partial least SQUARES method quantitative analysis
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Quantitative analysis modeling for the Chem Cam spectral data based on laser-induced breakdown spectroscopy using convolutional neural network 被引量:2
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作者 Xueqiang CAO Li ZHANG +3 位作者 Zhongchen WU Zongcheng LING Jialun LI Kaichen GUO 《Plasma Science and Technology》 SCIE EI CAS CSCD 2020年第11期81-90,共10页
Laser-induced breakdown spectroscopy(LIBS)has been applied to many fields for the quantitative analysis of diverse materials.Improving the prediction accuracy of LIBS regression models is still of great significance f... Laser-induced breakdown spectroscopy(LIBS)has been applied to many fields for the quantitative analysis of diverse materials.Improving the prediction accuracy of LIBS regression models is still of great significance for the Mars exploration in the near future.In this study,we explored the quantitative analysis of LIBS for the one-dimensional Chem Cam(an instrument containing a LIBS spectrometer and a Remote Micro-Imager)spectral data whose spectra are produced by the Chem Cam team using LIBS under the Mars-like atmospheric conditions.We constructed a convolutional neural network(CNN)regression model with unified parameters for all oxides,which is efficient and concise.CNN that has the excellent capability of feature extraction can effectively overcome the chemical matrix effects that impede the prediction accuracy of regression models.Firstly,we explored the effects of four activation functions on the performance of the CNN model.The results show that the CNN model with the hyperbolic tangent(tanh)function outperforms the CNN models with the other activation functions(the rectified linear unit function,the linear function and the Sigmoid function).Secondly,we compared the performance among the CNN models using different optimization methods.The CNN model with the stochastic gradient descent optimization and the initial learning rate?=?0.0005 achieves satisfactory performance compared to the other CNN models.Finally,we compared the performance of the CNN model,the model based on support vector regression(SVR)and the model based on partial least square regression(PLSR).The results exhibit the CNN model is superior to the SVR model and the PLSR model for all oxides.Based on the above analysis,we conclude the CNN regression model can effectively improve the prediction accuracy of LIBS. 展开更多
关键词 laser-induced breakdown spectroscopy convolutional neural network activation function optimization method quantitative analysis
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Quantitative Phase Analysis of the Calcium Silicate Slag as the Residue of Extracting Alumina from High-Alumina Fly Ash
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作者 黄冬波 宗燕兵 +2 位作者 刘晓明 彭丹丹 杨志杰 《Journal of Shanghai Jiaotong university(Science)》 EI 2016年第6期729-736,共8页
Calcium silicate slag is the residue of process of pre-desilication alkali lime sintering applied in the high-alumina fly ash to extract the alumina.The quantitative phase analysis(QPA) of the calcium silicate slag ha... Calcium silicate slag is the residue of process of pre-desilication alkali lime sintering applied in the high-alumina fly ash to extract the alumina.The quantitative phase analysis(QPA) of the calcium silicate slag has been performed by the Rietveld method based on the powder X-ray diffraction(XRD) with the aid of noncommercial software GSAS-EXPGUI.A known weight of crystalline internal standard(10% CaF_2) was added to the calcium silicate slag to calculate the fraction of amorphous phase and other crystalline phases on an absolute basis.Besides,the calcium silicate slag was characterized by X-ray fluorescence(XRF) and thermo gravimetric(TG) differential scanning calorimetry(DSC) to test the QPA results and investigate its other characters.Finally,the results show that the amorphous fraction is 17.5%(hereinafter,the percentages refer to the mass fraction),and the major crystalline phases detected in the calcium silicate slag consist of 23.5% Beta-Ca_2 SiO_4,10.0% bredigite,10.3% Ca_3Al_2O_6(C_3A) and 21.6% CaCO_3. 展开更多
关键词 calcium silicate slag X-ray diffraction(XRD) quantitative phase analysis(QPA) Rietveld method
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A quantitative BP neural network analysis of the relationships between ΣREE content and impact factors in the Beibu Gulf
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作者 ZHANG Wen-li HU Hao +2 位作者 LONG Jiang-ping XU Dong ZHOU Meng-jia 《Marine Science Bulletin》 CAS 2017年第1期52-66,共15页
The distribution characteristics of rare earth elements (REE) in bottomsediments are influenced by many factors. Hence, conducting a quantitative analysis isdifficult. A qualitative analysis of the relationships bet... The distribution characteristics of rare earth elements (REE) in bottomsediments are influenced by many factors. Hence, conducting a quantitative analysis isdifficult. A qualitative analysis of the relationships between ΣREE content andprovenance, hydrodynamics, grain size and mineral distribution in the Beibu Gulf showsthat terrestrial rocks control the ΣREE composition. Both weaker hydrodynamics andfiner grain size lead to a higher ΣREE content. Relative curves revealing therelationships between individual impact factors and ΣREE content were obtained fromthe combination of qualitative and quantitative analyses of the BP neural network,which trained the position of samples, gravel content, sand content, silt content, claycontent and clay mineral content. The results are consistent with those of thequantitative analysis. The self-learning algorithm is automatically determined andcalculated quantitatively. The impact of each factor on REEs and how each factorcontrols the ΣREE distribution is identified. Thus, environmental changes and thegeological evolution of the region can be inferred based on curve variation and the geological evolution of the region can be inferred based on curve variation and theactual situation. This method also provides useful theoretical guidance for the analysisof REE enrichment and dispersion. 展开更多
关键词 REE impact factors quantitative analysis BP neural network controlvariable method
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Quantitative Analysis法在木兰溪水质模型选择中的应用
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作者 林平 《太原师范学院学报(自然科学版)》 2009年第1期134-136,144,共4页
木兰溪是闽中最大的溪流,为福建省八条主要水系之一.对木兰溪水质模型进行选择可以根据Quantitative Analysis法,由Pe(Peclet Number)的范围来判断污染物在河流三维上的混合情况.通过将木兰溪划分为四个计算(控制)单元,对控制单元4的Pe... 木兰溪是闽中最大的溪流,为福建省八条主要水系之一.对木兰溪水质模型进行选择可以根据Quantitative Analysis法,由Pe(Peclet Number)的范围来判断污染物在河流三维上的混合情况.通过将木兰溪划分为四个计算(控制)单元,对控制单元4的Pe值进行计算,快速准确地确定了适合木兰溪的简单实用的水质数学模型. 展开更多
关键词 quantitative analysis 水质模型 一维水质模型
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Application of the Quantitative Descriptive Analysis in Cosmetics Sensory Evaluation
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作者 Jiang Ligang He Yanjie +1 位作者 Chen Bin Huang Jiefang 《China Detergent & Cosmetics》 2018年第3期52-58,共7页
The sensory evaluation method was introduced so late in China, and a complete system of this method has not built yet in cosmetics industry. In this article, the application of the Quantitative Descriptive Analysis me... The sensory evaluation method was introduced so late in China, and a complete system of this method has not built yet in cosmetics industry. In this article, the application of the Quantitative Descriptive Analysis method in the evaluation of the sensory assessment items are studied. With the SPSS reliability analysis, it was found that the Quantitative Descriptive Analysis method is not suitable for some sensory assessment items. 展开更多
关键词 COSMETICS sensory evaluation quantitative descriptive analysis method
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Leveraging Bayesian methods for addressing multi-uncertainty in data-driven seismic liquefaction assessment
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作者 Zhihui Wang Roberto Cudmani +2 位作者 Andrés Alfonso Peña Olarte Chaozhe Zhang Pan Zhou 《Journal of Rock Mechanics and Geotechnical Engineering》 2025年第4期2474-2491,共18页
When assessing seismic liquefaction potential with data-driven models,addressing the uncertainties of establishing models,interpreting cone penetration tests(CPT)data and decision threshold is crucial for avoiding bia... When assessing seismic liquefaction potential with data-driven models,addressing the uncertainties of establishing models,interpreting cone penetration tests(CPT)data and decision threshold is crucial for avoiding biased data selection,ameliorating overconfident models,and being flexible to varying practical objectives,especially when the training and testing data are not identically distributed.A workflow characterized by leveraging Bayesian methodology was proposed to address these issues.Employing a Multi-Layer Perceptron(MLP)as the foundational model,this approach was benchmarked against empirical methods and advanced algorithms for its efficacy in simplicity,accuracy,and resistance to overfitting.The analysis revealed that,while MLP models optimized via maximum a posteriori algorithm suffices for straightforward scenarios,Bayesian neural networks showed great potential for preventing overfitting.Additionally,integrating decision thresholds through various evaluative principles offers insights for challenging decisions.Two case studies demonstrate the framework's capacity for nuanced interpretation of in situ data,employing a model committee for a detailed evaluation of liquefaction potential via Monte Carlo simulations and basic statistics.Overall,the proposed step-by-step workflow for analyzing seismic liquefaction incorporates multifold testing and real-world data validation,showing improved robustness against overfitting and greater versatility in addressing practical challenges.This research contributes to the seismic liquefaction assessment field by providing a structured,adaptable methodology for accurate and reliable analysis. 展开更多
关键词 data-driven method Bayes analysis Seismic liquefaction UNCERTAINTY Neural network
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The Analysis of the Untwisting and Retwisting Methods in Determining the Twist of OE Yarn
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作者 贾立锋 饶惠珍 李汝勤 《Journal of China Textile University(English Edition)》 EI CAS 1998年第3期92-94,共3页
The twists of twelve kinds of the cotton OE yarns in different machine twists and different yarn linear density have been determined by one time back twisting and twisting method, triple twisting method and double twi... The twists of twelve kinds of the cotton OE yarns in different machine twists and different yarn linear density have been determined by one time back twisting and twisting method, triple twisting method and double twisting method. The quantitative analysis of the measurement principles of all the untwisting and retwisting methods has been made by the writers. It is theoretically and practically concluded that for twelve kinds of the cotton OE yarns the difference between the twist determined by triple twisting method and machine twist is the lowest and there is measuring method error in determining the twist of OE yarn by all the untwisting and retwisting methods. 展开更多
关键词 untwisting and retwisting method quantitative analysis measuring method error .
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A New Approach to Investigate Students’ Behavior by Using Cluster Analysis as an Unsupervised Methodology in the Field of Education
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作者 Onofrio Rosario Battaglia Benedetto Di Paola Claudio Fazio 《Applied Mathematics》 2016年第15期1649-1673,共25页
The problem of taking a set of data and separating it into subgroups where the elements of each subgroup are more similar to each other than they are to elements not in the subgroup has been extensively studied throug... The problem of taking a set of data and separating it into subgroups where the elements of each subgroup are more similar to each other than they are to elements not in the subgroup has been extensively studied through the statistical method of cluster analysis. In this paper we want to discuss the application of this method to the field of education: particularly, we want to present the use of cluster analysis to separate students into groups that can be recognized and characterized by common traits in their answers to a questionnaire, without any prior knowledge of what form those groups would take (unsupervised classification). We start from a detailed study of the data processing needed by cluster analysis. Then two methods commonly used in cluster analysis are before described only from a theoretical point a view and after in the Section 4 through an example of application to data coming from an open-ended questionnaire administered to a sample of university students. In particular we describe and criticize the variables and parameters used to show the results of the cluster analysis methods. 展开更多
关键词 EDUCATION Unsupervised methods Hierarchical Clustering Not-Hierarchical Clustering quantitative analysis
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Numerical Analysis on Lorentz Force Field in φ160 Billet Under Harmonic Magnetic Field
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作者 BAI Yun-feng 《Journal of Iron and Steel Research International》 SCIE EI CAS CSCD 2012年第S1期118-122,共5页
A method was developed to quantitatively describe the time-varying Lorentz force field induced in billet under harmonic magnetic field.Based on the numerical analysis of the Lorentz force,the numeral features were con... A method was developed to quantitatively describe the time-varying Lorentz force field induced in billet under harmonic magnetic field.Based on the numerical analysis of the Lorentz force,the numeral features were concluded, which comprised of the mean force,the maximum force,the long axis,short axis and rotation direction of ellipse,the phase difference index,and so on.Using this method,the Lorentz force field in φ160 billet under 3 Hz harmonic magnetic field were analyzed. 展开更多
关键词 Lorentz force field quantitative description method numerical analysis harmonic magnetic field φ160 billet
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An analytical method for quantitative estimation of the cytotoxicity of dental alloys using MTT assay,ICP analysis and effective cytotoxicity calculation
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作者 Lü Xiao Ying and H.F.Kappert 《Chinese Medical Journal》 SCIE CAS CSCD 1997年第12期47-47,共1页
The two most important criteria for dental materials are their biofunctional and biocompatible endurance within the anticipated life-span of the dental restoration in the mouth. Biocompatibility relates mainly to the ... The two most important criteria for dental materials are their biofunctional and biocompatible endurance within the anticipated life-span of the dental restoration in the mouth. Biocompatibility relates mainly to the allergenicity and the toxicity of the material. To test the non-specific toxicity of dental materials, in vitro cell culture assays have been developed. For in vitro screening, such tests are recommended to check the cytotoxicity of dental materials (ISO 10993 5). Various studies have already been performed to quantitatively determine the cytotoxicity level of dental alloys. However, as long as only dental alloys and the cell culture technique are applied, it is not possible to determine which of the alloying elements cause the cytotoxicity. Therefore, an analytical method is needed. Wataha et al determined in 1991 the TC50 values of 9 metal cations of various dental casting alloys, using cell culture methods. Kapert et al reported in 1994 a complex in vitro test concept, where the ICP analysis (inductively coupled plasma emission spectroscopy) was introduced to measure the trace elements extracted from various alloys. Experimentelle Zahnheilkunde, Universitts ZMK Klinik Freiburg, Germany (Lü XY and Kappert HF) The aim of the present study was to find a relation between the ICP results, the TC50 value of metal cations, and the cytotoxicity of dental alloys. The cytotoxicity levels of various dental alloys and the TC50 values of 10 metal cations were established using the MTT assay, an effective cell culture of method. Then, the concentrations of the corrosively soluted metal cations in the extracts of the alloys were measured using the ICP method. From all these experimental results it was found that the relation between the effective cytotoxicity Z eff of an alloy, the concentrations C i of i th trace element and the TC50 values T Ci of the i th metal cation can approximately be expressed by Z eff =∑iC i2·T Ci . Two significant applications of this expression are a) The cytotoxicity of an alloy can be estimated by ICP analysis of the extract if the TC50 values of the trace elements are know. b) The cytotoxicity of a new-developed-alloy can be estimated in advance, according to the alloying components. 展开更多
关键词 MTT ICP An analytical method for quantitative estimation of the cytotoxicity of dental alloys using MTT assay ICP analysis and effective cytotoxicity calculation
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地顶孢霉培养物中麦角甾醇定量分析方法的建立与验证
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作者 徐娟娟 李俊辉 +4 位作者 刘发全 周群 潘瀚文 吴昊 徐自奥 《安徽农学通报》 2026年第2期92-96,共5页
为建立一种准确、可靠的地顶孢霉培养物中麦角甾醇定量分析方法,研究基于常规高效液相色谱法,分别对检测波长、提取时间(15、25、35、45、55 min)、提取溶剂(甲醇、无水乙醇、95%乙醇)、流动相比例(甲醇∶水,100∶0、98∶2、95∶5、90∶... 为建立一种准确、可靠的地顶孢霉培养物中麦角甾醇定量分析方法,研究基于常规高效液相色谱法,分别对检测波长、提取时间(15、25、35、45、55 min)、提取溶剂(甲醇、无水乙醇、95%乙醇)、流动相比例(甲醇∶水,100∶0、98∶2、95∶5、90∶10)、流速(0.6、0.8、1.0、1.2、1.4 mL/min)等进行优化,并对优化方法进行专属性、线性、精密度、准确度、检测限和定量限分析,利用10批地顶孢霉培养物进行方法的应用验证。结果表明,建立的高效液相色谱法的检测条件为检测波长281 nm,浸提溶液为95%乙醇、浸提时间45 min,流动相比例100∶0(甲醇∶水),流速1.0 mL/min。该方法能够有效分离地顶孢霉培养物中麦角甾醇和其他成分,且对麦角甾醇测定结果无影响;麦角甾醇在0.5~40.0µg/mL范围内线性关系良好(R^(2)=0.9992),精密度RSD小于3%,回收率在90.45%~99.41%,定量限为0.50µg/mL,检测限为0.15µg/mL;同一批次的地顶孢霉培养物样品重复性较好,稳定且可操作性强。综合表明,本文建立的高效液相色谱法方法具有测定范围宽、线性好、准确性高等优点,能够对地顶孢霉培养物中麦角甾醇进行准确定量。 展开更多
关键词 地顶孢霉培养物 麦角甾醇 高效液相色谱法 定量分析 方法验证
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专利视角下宝鸡市科技创新能力提升研究
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作者 张蕴 党建华 +2 位作者 任静 杨宏伟 王静 《技术与创新管理》 2026年第1期36-42,126,共8页
专利是衡量地区科技创新能力的重要指标。采用定量分析法,从专利申请趋势、创新主体构成、技术领域分布、专利类型结构、维持状况以及跨省合作等维度,对宝鸡市2014—2024年间的专利数据进行全面统计与深入分析,揭示了宝鸡市科技创新能... 专利是衡量地区科技创新能力的重要指标。采用定量分析法,从专利申请趋势、创新主体构成、技术领域分布、专利类型结构、维持状况以及跨省合作等维度,对宝鸡市2014—2024年间的专利数据进行全面统计与深入分析,揭示了宝鸡市科技创新能力的发展现状并提出对策建议,为政策制定、创新资源配置等提供科学依据。结果表明:专利申请和授权数量总体呈上升趋势,但发明专利占比(29%)低于全国平均水平;创新资源集中度高,前3%的申请主体贡献了29%的专利申请量,域内高校和国企是主要创新主体,创新技术领域主要集中在B部(作业、运输);发明专利维持率显著高于实用新型专利和外观设计专利,企业专利维持率高于高校;跨省合作专利、PCT国际专利申请数量少,区域创新协同能力和技术国际化程度有较大提升空间;创新成果转化渠道总体畅通。建议通过提升公众知识产权保护意识、培育高价值专利、推动技术领域的多元化、构建产学研融合生态环境、加速专利的国际化布局等相关举措,全面推进宝鸡市在专利创造、运用、保护与管理方面的能力,为宝鸡市科技创新能力提升及地方区域社会经济高质量发展提供坚实保障。 展开更多
关键词 知识产权 科技创新能力 定量分析法 专利 技术领域 专利权转移 专利合作条约
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X射线荧光光谱定量方法在文物分析中的应用
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作者 杜维莎 董佩 +2 位作者 景博文 王伟锋 杨莹 《理化检验(物理分册)》 2026年第2期27-33,共7页
X射线荧光光谱(XRF)分析技术是一种无损、便捷、高效的分析方法,可同时获取待测物的元素组成及其含量信息,已在文物产地溯源、工艺研究及病害识别等方面得到广泛应用。介绍了XRF定量方法及其影响因素,综述了其在陶瓷、金属及彩绘类文物... X射线荧光光谱(XRF)分析技术是一种无损、便捷、高效的分析方法,可同时获取待测物的元素组成及其含量信息,已在文物产地溯源、工艺研究及病害识别等方面得到广泛应用。介绍了XRF定量方法及其影响因素,综述了其在陶瓷、金属及彩绘类文物中的应用情况,并剖析了其在标准试样及行业标准方面存在的局限与问题,认为XRF技术在文物定量分析中极具潜力,具体使用时应根据检测需求,对待测试样进行充分评估,选择适宜的标准试样及测试方法,以获取更为科学、准确的数据。 展开更多
关键词 X射线荧光光谱分析 定量方法 文物分析 标准试样 无损检测
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基于人工智能的动物毛混纺纤维含量定量分析研究
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作者 颜刚华 黄宇斌 +7 位作者 刘卓钦 谢飞 杨二涛 黄海敏 兰丽丽 袁志磊 费静 王文 《分析测试学报》 北大核心 2026年第2期358-365,共8页
与GB/T 16988-2013《特种动物纤维与绵羊毛混合物含量的测定》标准采用人工方法分辨和测量动物毛及其混纺产品纤维含量不同,基于人工智能的分析技术,利用显微镜自动扫描捕集动物纤维图像,通过集成图像识别、图像处理等先进方法,建立纤... 与GB/T 16988-2013《特种动物纤维与绵羊毛混合物含量的测定》标准采用人工方法分辨和测量动物毛及其混纺产品纤维含量不同,基于人工智能的分析技术,利用显微镜自动扫描捕集动物纤维图像,通过集成图像识别、图像处理等先进方法,建立纤维分类模型,进而完成纤维含量的自动定量分析。该文介绍了基于人工智能的动物毛纤维成分定量分析方法的原理,设计了一个包含8个实验室、4个种类各3个质量水平动物毛混纺纤维的平衡均匀水平试验,并对人工智能定量分析方法进行方法确认,评价方法的正确度和精密度。结果表明,人工智能定量分析方法的正确度可信、精密度满足检测应用要求,可等效替代GB/T 16988-2013标准检测方法,并提供更高效、更稳定的定量检测结果,具有广阔的应用前景。 展开更多
关键词 毛混纺纤维 人工智能 定量分析 方法确认
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液质联用与气质联用测定物品表面增塑剂的对比实验研究
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作者 殷子扬 陆艳荣 +2 位作者 王星 范子文 冯嘉靖 《广州化工》 2026年第2期186-190,共5页
对比研究了液质联用法和气质联用法检测邻苯二甲酸酯类(PAEs)增塑剂的性能差异,发现气质联用法对PAEs具有更好的分离能力和检出能力。基于气质联用法建立了物品表面14种PAEs的分析方法,方法在0.05~10μg/g范围内具有良好的线性,回收率可... 对比研究了液质联用法和气质联用法检测邻苯二甲酸酯类(PAEs)增塑剂的性能差异,发现气质联用法对PAEs具有更好的分离能力和检出能力。基于气质联用法建立了物品表面14种PAEs的分析方法,方法在0.05~10μg/g范围内具有良好的线性,回收率可达90.3%~104.9%,相对标准偏差在5.0%~9.6%,定量限在0.1~6.0 ng/g,能够实现PAEs的痕量分析。通过实际样品分析,发现鼠标表面有5种PAEs高频检出,PAEs的总浓度在147.7~775.6 ng/g。该实验简单高效,可扩展应用到食品、皮肤以及多类物品表面增塑剂的测定,实验设计贴近工作生活,有利于激发学生的科研兴趣,同时实验涵盖多个知识点,有利于培养学生的科研技能和探索能力。 展开更多
关键词 邻苯二甲酸酯 对比研究法 质谱法 定性定量分析 仪器分析实验
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