A comprehensive understanding of shale’s bedding anisotropy is crucial for shale-related engineering activities,such as hydraulic fracturing,drilling and underground excavation.In this study,seven Brazilian tests wer...A comprehensive understanding of shale’s bedding anisotropy is crucial for shale-related engineering activities,such as hydraulic fracturing,drilling and underground excavation.In this study,seven Brazilian tests were conducted on shale samples at different bedding orientations with respect to the loading direction(0°,45°and 90°)and the disc end face(0°,45°and 90°).An acoustic emission(AE)system was employed to capture the evolution of damage and the temporal-spatial distribution of microcracks under splitting-tensile stress.The results show that the Brazilian tensile strength decreases with increasing bedding inclination with respect to the disc end face,while it increases with the angle between bedding and loading directions.Increasing the bedding inclination with respect to the end face facilitates the reduction in b value and enhances the shale’s resistance to microcrack growth during the loading process.Misalignment between the bedding orientation and the end face suppresses the growth of mixed tensile-shear microcracks,while reducing the bedding angle relative to the loading direction is beneficial for creating mixed tensile-shear and tensile cracks.The observed microscopic failure characteristics are attributed to the competing effects of bedding activation and breakage of shale matrix at different bedding inclinations.The temporal-spatial distribution of microcracks,characterized by AE statistics including the correlation dimension and spatial correlation length,illustrates that the fractal evolution of microcracks is independent of bedding anisotropy,whereas the spatial distribution shows a stronger correlation.The evolution features of correlation dimension and spatial correlation length could be potentially used as precursors for shale splitting failure.These findings may be useful for predicting rock mass instability and analyzing the causes of catastrophic rupture.展开更多
In this paper,Brazilian test was performed on disk samples of analogue materials with defined structural planes.The surface strain evolution process of the disk samples during loading was analyzed via digital image co...In this paper,Brazilian test was performed on disk samples of analogue materials with defined structural planes.The surface strain evolution process of the disk samples during loading was analyzed via digital image correlation.The damage evolution process was explored from a microscopic perspective by combining discrete element numerical simulation technology.The criterion of the failure mode of the disc specimen in the split state was theoretically deduced.The influence of structural surface roughness and loading inclination angle on the stress state at the center of the specimen was explored.The results showed that the failure modes of the samples could be divided into three typical modes as matrix failure,structural plane failure and combination failure.The rough structural plane improves the failure strength of the specimen by limiting its lateral deformation,and the degree of improvement weakens continuously with the increase of the inclination angle of the structural plane.As the inclination angle of the structural plane increases,the main type of microcracks in the structural plane changes from shear microcracks to tensile microcracks.This study contributes to a better understanding of macro-and meso-failure characteristics of rock masses with structural planes under a splitting state.展开更多
The presence of evangelicals in Brazil is a social and religious phenomenon that has aroused interest of many scholars due to its rapid and significant expansion in recent decades and its projection beyond national bo...The presence of evangelicals in Brazil is a social and religious phenomenon that has aroused interest of many scholars due to its rapid and significant expansion in recent decades and its projection beyond national borders.Among evangelical denominations that stand out in this scenario are Pentecostal churches,which have developed intense missionary activity in several countries,including Europe.In this article,we intend to analyze features and challenges of Brazilian evangelical churches:World Cathedral of Hope(CIME)(Catedral Mundial da Esperança-ICME)and Assembly of God Victory in Christ(ADVEC)(Assembleia de Deus Vitória em Cristo-ADVEC)that operate in Portugal,seeking to understand issues of identity and belonging of these communities,their models of transnationalization,its evangelization strategies and its adaptations to Portuguese context,in the period from 2000 to 2020.展开更多
Background: In low-income African countries, the demand and use of plastic surgery operations including abdominoplasty, liposuction and Brazilian butt lift (BBL) are increasing. The goal of this work is to present my ...Background: In low-income African countries, the demand and use of plastic surgery operations including abdominoplasty, liposuction and Brazilian butt lift (BBL) are increasing. The goal of this work is to present my experience and the challenges of this aesthetic plastic surgery among black African women. Material and Methods: A retrospective study was conducted about the abdominoplasties, liposuctions and Brazilian butt lift (BBL) which I operated in public and private hospitals at Kinshasa (Democratic Republic of Congo) in black African women. It covers a period of 13 years, going from December 1, 2010 to December 1, 2023. For this study, I had at least 6 months period (to Juin 1, 2024) to assess the occurrence of early and late postoperative complications. Results: I performed 84 abdominoplasties, 144 liposuctions and 23 Brazilian butt lifts (BBL). The average age at the time of abdominoplasty was 44 years with extremes ranging from 26 to 55 years and a concentration of cases (60.7%) in the age group of 40 to 49 years. The age group of 20 to 29 years old represented the lowest rate of requests for abdominoplasty (4.7%). Patients with a BMI of 30 to 2 were the majority (61.9%), followed by those between 25 to 2 (29.7%). 67.8% of patients were obese (BMI ≥ 30 kg/m2). The average age at the time of liposuction was 41 years with extremes ranging from 21 years to 69 years;and more than half of cases (68%) in the age group between 30 and 49 years. As for Brazilian butt lift (BBL), the average age was 33 years with extremes ranging from 24 to 42 years and a concentration of patients (91.3%) between 20 and 39 years. The immediate postoperative complications of abdominoplasties observed were: seroma in 7% of cases, hematoma and partial infection of the surgical site in 5% of cases. Pathological scars (hypertrophic, keloid) after abdominoplasties were observed in 9% of cases. The most common complication of liposuction was contour deformity. I observed 16 patients (11.1%) with soft-tissue depressions or elevations, skin panniculus or folds. For Brazalian Butt Lift (BBL), complications like asymmetry for 2 patients (8.9%), contour irregularities for 2 patients (8.9%), and excessive fat removal for 6 patients (26%), had observed. I have not recorded any cases of death or pulmonary embolism. Conclusion: I perform aesthetic plastic surgery procedures in black African women with a high socioeconomic standard of living compared to the average of the general population. The renunciation of planned surgery is motivated by the impossibility of paying the cost of the operation as well as by popular and religious perceptions regarding cosmetic surgery. The results of these aesthetic plastic surgery procedures carried out are very satisfactory for them. The challenges to overcome are mainly threefold: the unforeseeable complications of these cosmetic plastic surgery procedures, popular and religious perceptions of cosmetic surgery as well as the poverty of the population.展开更多
In this study,authors analyzed value,production and area used for producing Cerrado’s main agricultural products,and data on the farms located within this biome and registered in CAR up until April 2019,by microregio...In this study,authors analyzed value,production and area used for producing Cerrado’s main agricultural products,and data on the farms located within this biome and registered in CAR up until April 2019,by microregion.The territory considered here comprised all microregions with at least 25%of its area covered by the Cerrado biome.The production,agricultural production,and planted area values used were the averages of the 2015 to 2017 harvests,and are shown in graphs and tables,as are maps of planted areas and groups of main annual crops,semi-perennial and perennial crops.The areas designated for environmental preservation(ADPs)are the result of the sum of permanent preservation areas(APP),legal reserves(RL)and additional vegetation areas within the farms.Authors’study shows that most of Brazilian cotton,eucalyptus for charcoal,orange,sugarcane,maize and soybean are produced in Cerrado,that 28%of Cerrado are ADPs within farms,and that 16%are areas planted with cotton,eucalyptus,orange,sugarcane,maize,soybean,coffee,beans,and potatoes.The territory occupied by agricultural areas and ADPs required by the Brazilian Forest Code shows that agricultural production and environmental preservation do coexist,and gather the maintenance of essential ecosystem services provided by the ADPs together with the development of the country’s relevant agricultural production.展开更多
A discrete element method （DEM） called particle flow code （PFC2D） was used to construct a model for Brazilian disc splitting test in the present study. Based on the experimental results of intact Brazilian disc of...A discrete element method （DEM） called particle flow code （PFC2D） was used to construct a model for Brazilian disc splitting test in the present study. Based on the experimental results of intact Brazilian disc of rock-like material, a set of micro-parameters in PFC2D that reflected the macro-mechanical behavior of rock-like materials were obtained. And then PFC2D was used to simulate Brazilian splitting test for jointed rock mass specimens and specimen containing a central straight notch. The effect of joint angle and notch angle on the tensile strength and failure mode of jointed rock specimens was detailed analyzed. In order to reveal the meso-mechanical mechanism of crack coalescence, displacement trend lines were applied to analyze the displacement evolution during the crack initiation and propagation. The investigated conclusions can be described as follows. （1） The tensile strength of jointed rock mass disc specimen is dependent to the joint angle. As the joint angle increases, the tensile strength of jointed rock specimen takes on a nonlinear variance. （2） The tensile strength of jointed rock mass disc specimen containing a central straight notch distributes as a function of both joint angle and notch angle. （3） Three major failure modes, i.e., pure tensile failure, shear failure and mixed tension and shear failure mode are observed in jointed rock mass disc specimens under Brazilian test. （4） The notch angle roles on crack initiation and and joint angle play important propagation characteristics of jointed rock mass disc specimen containing a central straight notch under Brazilian test.展开更多
The experimental study in this paper focuses on the effects of the layer orientation and sample shape on failure strength and fracture pattern of samples tested under Brazilian test conditions(i.e.diametrical loading ...The experimental study in this paper focuses on the effects of the layer orientation and sample shape on failure strength and fracture pattern of samples tested under Brazilian test conditions(i.e.diametrical loading of cylindrical discs)for one particular layered sandstone which is from Modave in the south of Belgium.The variations of the strength in combination with the failure patterns are examined as a function of the inclination angle between the layer plane and the loading direction.The experimental,results clearly show that the induced fracture patterns are a combination of tensile and/or shear fractures.In shape effect experiments the layer thickness and the number of layer boundaries are investigated.Different blocks of Modave sandstone are used to prepare samples.The layer thickness is different among the various blocks,but the layer thickness in each studied rock block can be considered to be constant;hence,the number of layer boundaries changes according to the sample diameter for samples of the same block.The experimental study shows that the layer thickness plays a more important role than the number of layer boundaries per sample.展开更多
Tensile failure(spalling or slabbing)often occurs on the sidewall of deep tunnel,which is closely related to the coupled stress state of deep rock mass under high pre-static load and dynamic disturbance.To reveal the ...Tensile failure(spalling or slabbing)often occurs on the sidewall of deep tunnel,which is closely related to the coupled stress state of deep rock mass under high pre-static load and dynamic disturbance.To reveal the mechanism of rock tensile failure caused by this coupled stress mode,the Brazilian disc tests were carried on red sandstone under high pre-static load induced by dynamic disturbance.Based on the pure static tensile fracture load of red sandstone specimen,two static load levels(80%and 90%of the pure static tensile fracture load)were selected as the initial high pre-static loading state,and then the dynamic disturbance load was applied until the rock specimen was destroyed.The dynamic disturbance loading mode adopted a sinusoidal wave(sine-wave)load,and the loading wave amplitude was 20%and 10%of the pure static tensile fracture load,respectively.The dynamic disturbance frequencies were set to 1,10,20,30,40,and 50 Hz.The results show that the tensile failure strength and peak displacement of red sandstone specimens under coupled load actions are lower than those under pure static tensile load,and both parameters decrease significantly with the increase of dynamic disturbance frequency.With the increase of dynamic disturbance frequency,the decrease range of tensile strength of red sandstone increased from 3.3%to 9.4%when the pre-static load level is 80%.While when the pre-static load level is 90%,the decrease range will increase from 7.4%to 11.6%.This weakening effect of tensile strength shows that the deep surrounding rock is more likely to fail under the coupled load actions of pre-static load and dynamic disturbance.In this tensile failure mechanism of the deep surrounding rock,the stress environment of deep sidewall rock determines that the failure mode of rock is a tensile failure,the pre-static load level dominates the tensile failure strength of surrounding rock,and dynamic disturbance promotes the strength-weakening effect and affects the weakening range.展开更多
To reveal stress distribution and crack propagation of Brazilian discs under impact loads, dynamic tests were conducted with SHPB （split Hopkinson pressure bar） device. Stress states of specimens were monitored with...To reveal stress distribution and crack propagation of Brazilian discs under impact loads, dynamic tests were conducted with SHPB （split Hopkinson pressure bar） device. Stress states of specimens were monitored with strain gauges on specimen surface and SHPB bars. The failure process of specimen was recorded by ultra speed camera FASTCAM SAI.1 （675 000 fps）. Stress histories from strain gauges offer comprehensive information to evaluate the stress equilibrium of specimen in time and space. When a slowly rising load （with loading rates less than 1 200 N/s for d 50 mm bar） is applied, there is usually good stress equilibrium in specimen. The stress distribution after equilibrium is similar to its static counterpart. And the first crack initiates at the disc center and propagates along the load direction. But with the front of incident wave becoming steep, it is hard for specimens to get to stress equilibrium. The first crack may appear anywhere on the specimen together with multiple randomly distributed secondary cracks. For a valid dynamic Brazil test with stress equilibrium, the specimen will break into two halves neatly. While for tests with stress disequilibrium, missing strap may be found when broken halves of specimens are put together. For those specimens broken up neatly at center but having missing wedges at the loading areas, it is usually subjected to local buckling from SHPB bars.展开更多
A new specimen geometry-the double edge-cracked Brazilian disk and a relevant fracture analysis byweight function method are proposed for the investigation of rock fracture caused by compression-shear loading. Notonly...A new specimen geometry-the double edge-cracked Brazilian disk and a relevant fracture analysis byweight function method are proposed for the investigation of rock fracture caused by compression-shear loading. Notonly can the mixed mode fracture with any ratio of KⅠ/KⅡ be achieved, but also the pure mode Ⅱ crack extensioncan be obtained. The combined mode fracture analysis for this geometry shows that diametral compression in the far-field can induce a compression-shear stress state in the singular stress field ahead of crack tips. Experimental investi-gations conducted on marble specimens show that the pure mode Ⅱ crack extension can be obtained when the dimen-sionless crack length a＞0.7 and the inclined crack angle 5°≤ψ≤40°. Normalized mode Ⅰ and mode Ⅱ stress inten-sity factors decrease from -0.45 and 2.47 at ψ=5° to -1.65 and 1.52 at ψ=40°, respectively. The strains at threepoints of specimen are also measured in order to investigate the influence of stress singularity on initial crack exten-sion. The results show that the principal orientations of strain at three points are very stable in the loading process.The derived formulae are quite explicit, and the specimen geometry is easy to fabricate and convenient to achieve thepure mode Ⅱ crack extension. Therefore, it can hopefully be used to obtain mode Ⅱ fracture toughness of rock.展开更多
The general contact problem of a disc squeezed between jaws of arbitrary curvature is considered employing Muskhelishvili’s complex potentials.Taking advantage of the general solution introduced,the closed-form expre...The general contact problem of a disc squeezed between jaws of arbitrary curvature is considered employing Muskhelishvili’s complex potentials.Taking advantage of the general solution introduced,the closed-form expressions for the stresses along strategic loci(loaded rim,loaded diameter,disc’s center)are obtained,in terms of the ratio r of the disc’s to the jaw’s curvature.Then,the effect of r(as well as that of the relative stiffness of the disc’s and jaw’s materials dictating the contact arc)on the stress distribution along these loci is explored.It is concluded that,for both smooth contact(zero friction)and contact with friction,the role of the jaw’s curvature is significant not only along the disc-jaw contact arc(as it could be expected),but also all along the loaded diameter.On the other hand,it is indicated that the stress field at the disc’s center is more or less insensitive to the jaw’s curvature assuming that r lies within the range(0,0.67)or in other words within the limits defined by the two standardized suggestions,i.e.that of American Society for Testing and Materials(ASTM)(plane loading platens with r ? 0)and that of International Society for Rock Mechanics(ISRM)(curved jaws with r ? 0.67).The upper limit of this range is a kind of compromise between the need to make the stress field at the disc’s center independent of the boundary conditions while keeping at the same time the contact angle large enough to reduce the stress concentration and the risk for premature fracture initiation far from the disc’s center.For jaws with radius of curvature exceeded by that suggested by ISRM,the stress field at the disc’s center is significantly influenced.Especially for jaws with radius approaching that of the disc,the stress field at the disc’s center is dramatically distorted rendering Hondros’ formula inapplicable and the test results erroneous.展开更多
Cracked straight-through Brazilian disc(CSTBD) samples prepared using two rock materials were used for thermal treatment from room temperature to 700℃. Uniaxial splitting experiments were performed using an automatic...Cracked straight-through Brazilian disc(CSTBD) samples prepared using two rock materials were used for thermal treatment from room temperature to 700℃. Uniaxial splitting experiments were performed using an automatic electro-hydraulic servo press to study the evolution laws of physical and fracture properties of different deep rock materials under high-temperature geological conditions. The fracture characteristics were measured using an industrial camera and digital image correlation technology to analyze the effect of high temperature on fracture properties and failure modes of the CSTBD samples after different thermal treatments. The micro-damage properties of green sandstone and granite materials were obtained using a scanning electron microscope(SEM). The following conclusions were drawn from the test results:(1) With the increasing temperature, the fracture characteristics of green sandstone and granite change from brittle fracture to plasticity fracture, the longitudinal wave velocity of granite decreases sharply at 600℃, and the damage factor reaches 0.8748 at 700℃.(2) The fracture toughness of green sandstone and granite decreases with increasing temperature;however, the decreasing range of granite is larger than that of green sandstone.(3) As the temperature increases, the fracture morphologies of green sandstone and granite materials become rougher, whereas thermal damage cracks of granite and intergranular fractures inside sandstone as well as pores of sandstone increase.(4) The crack tip opening displacement and peak strain corresponding to peak load increase with the temperature.展开更多
Split Hopkinson pressure bar(SHPB)has been used to study the dynamic failure pattern of flattened mortar Brazilian disc under impact load.Each disc contains several prefabricated cracks paralleled to each other.Dynami...Split Hopkinson pressure bar(SHPB)has been used to study the dynamic failure pattern of flattened mortar Brazilian disc under impact load.Each disc contains several prefabricated cracks paralleled to each other.Dynamic FEM has also been adopted to simulate such failure behavior.The mechanism of crack initiation,propagation and cut-through have been scrutinized with both experimental and numerical approaches.Influence of the number of the prefabricated cracks on the specimen strength and acoustic emission(AE)performance can be observed and studied.The results show that the strength decreases and AE counts increases,when the number of the prefabricated cracks increases.展开更多
The Brazilian test is a widely used method for determining the tensile strength of rocks and for calibrating parameters in bondedparticle models（BPMs）. In previous studies, the Brazilian disc has typically been trim...The Brazilian test is a widely used method for determining the tensile strength of rocks and for calibrating parameters in bondedparticle models（BPMs）. In previous studies, the Brazilian disc has typically been trimmed from a compacted rectangular specimen. The present study shows that different tensile strength values are obtained depending on the compressive loading direction. Several measures are proposed to reduce the anisotropy of the disc. The results reveal that the anisotropy of the disc is significantly influenced by the compactibility of the specimen from which it is trimmed. A new method is proposed in which the Brazilian disc is directly generated with a particle boundary, effectively reducing the anisotropy. The stiffness（particle and bond） and strength（bond） of the boundary are set at less than and greater than those of the disc assembly, respectively,which significantly decreases the stress concentration at the boundary contacts and prevents breakage of the boundary particle bonds. This leads to a significant reduction in the anisotropy of the disc and the discreteness of the tensile strength. This method is more suitable for carrying out a realistic Brazilian test for homogeneous rock-like material in the BPM.展开更多
The center cracked Brazilian disk subjected to diametral compressive stress uniformly distributed along parts of its cylindrical surface is used to investigate combined mode fracture of brittle material. A fracture a...The center cracked Brazilian disk subjected to diametral compressive stress uniformly distributed along parts of its cylindrical surface is used to investigate combined mode fracture of brittle material. A fracture analysis is made of this specimen configuration. Explicit formulae for mode Ⅰ and mode Ⅱ stress intensity factor calculation are derived based on boundary integral equation method and related numerical solution given by Atkinson. The proposed formulae are valid in wide range of crack length a/R . This configuration can avoid splitting along load line usually occuring in Brazilian test and permit one to achieve easily pure mode Ⅱ crack growth (crack coplanar extension) and any combination of K Ⅰ and K Ⅱ by a simple alignment of crack orientation with respect to load line. SIF values from the present calculation and finite element solution are also given for comparison.展开更多
It is claimed that the formula used for calculating the tensile strength of a disk-shaped rock specimen in the Brazilian test is not accurate, because the formula is based on the 2-dimensional elastic theory and only ...It is claimed that the formula used for calculating the tensile strength of a disk-shaped rock specimen in the Brazilian test is not accurate, because the formula is based on the 2-dimensional elastic theory and only suitable for very long or very short cylinders. The Matlab software was used to obtain the 2-dimensional distribution of stress in the rock specimen for Brazilian test. Then the 2-dimensional stress distribution in Brazilian disk was analyzed by the Marc FEM software. It can be found that the results obtained by the two software packages can verify each other. Finally, the 3-dimensional elastic stress in the specimen was calculated. The results demonstrate that the distribution of stress on the cross section of the specimen is similar to that in 2-dimension. However, the value of the stress on the cross section varies along the thickness of the specimen and the stress is bigger when getting closer to the end of the specimen. For the specimen with a height-to-diameter ratio of 1 and a Poisson＇s ratio of 0.25, the tensile strength calculated with the classical 2-D formula is 23.3% smaller than the real strength. Therefore, the classical 2-D formula is too conservative.展开更多
Both experimental and numerical approaches were used to study dynamic failure properties and patterns of flattened Brazilian discs,containing two prefabricated cracks intersected at a varying angle.Mechanism of crack ...Both experimental and numerical approaches were used to study dynamic failure properties and patterns of flattened Brazilian discs,containing two prefabricated cracks intersected at a varying angle.Mechanism of crack initiation,propagation,and cut-through were scrutinized and influences of the intersection angle on specimen strength and acoustic emission performance were also studied.All primary cracks initialize near the middle or the tip points of the upper prefabricated crack,and they continue to develop along the load direction and finally cut through the specimen.The secondary cracks could be observed in directions almost horizontal or parallel to the directions of prefabricated cracks.Furthermore,it is found that stress intensity factor reaches its maximum for specimen with intersection angle of 0 degree.展开更多
Dynamic tensile failure is a common phenomenon in deep rock practices,and thus accurately evaluating the dynamic tensile responses of rocks under triaxial pressures is of great significance.The Brazilian disc(BD)test ...Dynamic tensile failure is a common phenomenon in deep rock practices,and thus accurately evaluating the dynamic tensile responses of rocks under triaxial pressures is of great significance.The Brazilian disc(BD)test is the suggested method by the International Society for Rock Mechanics and Rock Engineering(ISRM)for measuring both the static and dynamic tensile strengths of rock-like materials.However,due to the overload phenomenon and the complex preloading conditions,the dynamic tensile strengths of rocks measured by the BD tests tend to be overestimated.To address this issue,the dynamic BD tensile strength(BTS)of Fangshan marble(FM)under different preloading conditions were measured through a triaxial split Hopkinson pressure bar(SHPB).The fracture onset in BD specimen was captured through a strain gage around the disc center.The discrepancy between the traditional tensile strength(TTS,determined by the peak load P_(f) of the BD specimen)and the nominal tensile strength(NTS,obtained from the load P_(i) when the diametral fracture commences in the tested BD specimen)was applied to quantitatively evaluating the overload phenomenon.The Griffith criterion was used to rectify the calculation of the tensile stress at the disc center under triaxial stress states.The results demonstrate that the overload ratio(s)increases with the loading rate(σ)and decreases with the hydrostatic pressure(σ_(s)).The TTS corrected by the Griffith criterion is independent of theσ_(s)due to the overload phenomenon,while the NTS corrected by the Griffith criterion is sensitive to both the andσ.Therefore,it is essential to modify the tensile stress in dynamic confined BD tests using both the overload correction and the Griffith criterion rectification to obtain the accurate dynamic BTS of rocks.展开更多
The increasing demand for safe food without preservatives or pesticides residues has encouraged several studies on natural products with antifungal activity and low toxicity.In this study,ethanolic extracts from leave...The increasing demand for safe food without preservatives or pesticides residues has encouraged several studies on natural products with antifungal activity and low toxicity.In this study,ethanolic extracts from leaves and fruit residues(peel and seeds)of three Brazilian savanna species(Acrocomia aculeata,Campomanesia adamantium and Caryocar brasiliense)were evaluated against phytopathogenic fungi.Additionally,the most active extract was chemically characterized by ESI-MS and its oral acute toxicity was evaluated.Extracts from C.brasiliense(pequi)peel and leaves were active against Alternaria alternata,Alternaria solani and Venturia pirina with minimal inhibitory concentrations between 350 and 1000 lg/mL.When incorporated in solid media,these extracts extended the lag phase of A.alternata and A.solani and reduced the growth rate of A.solani.Pequi peel extract showed better antifungal activity and their ESI-MS analysis revealed the presence of substances widely reported as antifungal such as gallic acid,quinic acid,ellagic acid,glucogalin and corilagin.The oral acute toxicity was relatively low,being considered safe for use as a potential natural fungicide.展开更多
Brazil is the largest producer of sugarcane and its derivatives in the world, and one of the largest consumers of sugarcane derivatives. Sugar places a position of great prominence in Brazilian feed, either by direct ...Brazil is the largest producer of sugarcane and its derivatives in the world, and one of the largest consumers of sugarcane derivatives. Sugar places a position of great prominence in Brazilian feed, either by direct consumption or as a component of industrialized products, from increasing consumption in the country. Sugar samples taken from local market were analyzed as the quality of table sugar consumed in the state of Sao Paulo (Brazil). The analysis of the parameters and basic attributes of characterization of sugar was according to the methodology developed by ICUMSA (2005;2011) and ICUMSA modified by Copersucar (2002). Samples of sugar from this region showed that medium-low quality. It can be observed in fundamental aspects such as purity and insoluble residues, which were below the standard. In addition, it should be noted the difficulty of obtaining information about the limit values for each attribute, by virtue of Legislation not be assertive to the product and, also, the scientific studies have not been unified to present the specifics for each type of sugar.展开更多
基金supported by the National Natural Science Foundation of China (Grant No.52364004)the Basic Research Project of Guizhou University (Grant No.[2023]40)support by the Helmholtz Association’s Initiative and Networking Fund for the Helmholtz Young Investigator Group ARES (Contract No.VH-NG-1516).
文摘A comprehensive understanding of shale’s bedding anisotropy is crucial for shale-related engineering activities,such as hydraulic fracturing,drilling and underground excavation.In this study,seven Brazilian tests were conducted on shale samples at different bedding orientations with respect to the loading direction(0°,45°and 90°)and the disc end face(0°,45°and 90°).An acoustic emission(AE)system was employed to capture the evolution of damage and the temporal-spatial distribution of microcracks under splitting-tensile stress.The results show that the Brazilian tensile strength decreases with increasing bedding inclination with respect to the disc end face,while it increases with the angle between bedding and loading directions.Increasing the bedding inclination with respect to the end face facilitates the reduction in b value and enhances the shale’s resistance to microcrack growth during the loading process.Misalignment between the bedding orientation and the end face suppresses the growth of mixed tensile-shear microcracks,while reducing the bedding angle relative to the loading direction is beneficial for creating mixed tensile-shear and tensile cracks.The observed microscopic failure characteristics are attributed to the competing effects of bedding activation and breakage of shale matrix at different bedding inclinations.The temporal-spatial distribution of microcracks,characterized by AE statistics including the correlation dimension and spatial correlation length,illustrates that the fractal evolution of microcracks is independent of bedding anisotropy,whereas the spatial distribution shows a stronger correlation.The evolution features of correlation dimension and spatial correlation length could be potentially used as precursors for shale splitting failure.These findings may be useful for predicting rock mass instability and analyzing the causes of catastrophic rupture.
基金Project(52274148)supported by the National Natural Science Foundation of ChinaProject(2022XJLJ01)supported by the Fundamental Research Funds for the Central Universities,China。
文摘In this paper,Brazilian test was performed on disk samples of analogue materials with defined structural planes.The surface strain evolution process of the disk samples during loading was analyzed via digital image correlation.The damage evolution process was explored from a microscopic perspective by combining discrete element numerical simulation technology.The criterion of the failure mode of the disc specimen in the split state was theoretically deduced.The influence of structural surface roughness and loading inclination angle on the stress state at the center of the specimen was explored.The results showed that the failure modes of the samples could be divided into three typical modes as matrix failure,structural plane failure and combination failure.The rough structural plane improves the failure strength of the specimen by limiting its lateral deformation,and the degree of improvement weakens continuously with the increase of the inclination angle of the structural plane.As the inclination angle of the structural plane increases,the main type of microcracks in the structural plane changes from shear microcracks to tensile microcracks.This study contributes to a better understanding of macro-and meso-failure characteristics of rock masses with structural planes under a splitting state.
文摘The presence of evangelicals in Brazil is a social and religious phenomenon that has aroused interest of many scholars due to its rapid and significant expansion in recent decades and its projection beyond national borders.Among evangelical denominations that stand out in this scenario are Pentecostal churches,which have developed intense missionary activity in several countries,including Europe.In this article,we intend to analyze features and challenges of Brazilian evangelical churches:World Cathedral of Hope(CIME)(Catedral Mundial da Esperança-ICME)and Assembly of God Victory in Christ(ADVEC)(Assembleia de Deus Vitória em Cristo-ADVEC)that operate in Portugal,seeking to understand issues of identity and belonging of these communities,their models of transnationalization,its evangelization strategies and its adaptations to Portuguese context,in the period from 2000 to 2020.
文摘Background: In low-income African countries, the demand and use of plastic surgery operations including abdominoplasty, liposuction and Brazilian butt lift (BBL) are increasing. The goal of this work is to present my experience and the challenges of this aesthetic plastic surgery among black African women. Material and Methods: A retrospective study was conducted about the abdominoplasties, liposuctions and Brazilian butt lift (BBL) which I operated in public and private hospitals at Kinshasa (Democratic Republic of Congo) in black African women. It covers a period of 13 years, going from December 1, 2010 to December 1, 2023. For this study, I had at least 6 months period (to Juin 1, 2024) to assess the occurrence of early and late postoperative complications. Results: I performed 84 abdominoplasties, 144 liposuctions and 23 Brazilian butt lifts (BBL). The average age at the time of abdominoplasty was 44 years with extremes ranging from 26 to 55 years and a concentration of cases (60.7%) in the age group of 40 to 49 years. The age group of 20 to 29 years old represented the lowest rate of requests for abdominoplasty (4.7%). Patients with a BMI of 30 to 2 were the majority (61.9%), followed by those between 25 to 2 (29.7%). 67.8% of patients were obese (BMI ≥ 30 kg/m2). The average age at the time of liposuction was 41 years with extremes ranging from 21 years to 69 years;and more than half of cases (68%) in the age group between 30 and 49 years. As for Brazilian butt lift (BBL), the average age was 33 years with extremes ranging from 24 to 42 years and a concentration of patients (91.3%) between 20 and 39 years. The immediate postoperative complications of abdominoplasties observed were: seroma in 7% of cases, hematoma and partial infection of the surgical site in 5% of cases. Pathological scars (hypertrophic, keloid) after abdominoplasties were observed in 9% of cases. The most common complication of liposuction was contour deformity. I observed 16 patients (11.1%) with soft-tissue depressions or elevations, skin panniculus or folds. For Brazalian Butt Lift (BBL), complications like asymmetry for 2 patients (8.9%), contour irregularities for 2 patients (8.9%), and excessive fat removal for 6 patients (26%), had observed. I have not recorded any cases of death or pulmonary embolism. Conclusion: I perform aesthetic plastic surgery procedures in black African women with a high socioeconomic standard of living compared to the average of the general population. The renunciation of planned surgery is motivated by the impossibility of paying the cost of the operation as well as by popular and religious perceptions regarding cosmetic surgery. The results of these aesthetic plastic surgery procedures carried out are very satisfactory for them. The challenges to overcome are mainly threefold: the unforeseeable complications of these cosmetic plastic surgery procedures, popular and religious perceptions of cosmetic surgery as well as the poverty of the population.
文摘In this study,authors analyzed value,production and area used for producing Cerrado’s main agricultural products,and data on the farms located within this biome and registered in CAR up until April 2019,by microregion.The territory considered here comprised all microregions with at least 25%of its area covered by the Cerrado biome.The production,agricultural production,and planted area values used were the averages of the 2015 to 2017 harvests,and are shown in graphs and tables,as are maps of planted areas and groups of main annual crops,semi-perennial and perennial crops.The areas designated for environmental preservation(ADPs)are the result of the sum of permanent preservation areas(APP),legal reserves(RL)and additional vegetation areas within the farms.Authors’study shows that most of Brazilian cotton,eucalyptus for charcoal,orange,sugarcane,maize and soybean are produced in Cerrado,that 28%of Cerrado are ADPs within farms,and that 16%are areas planted with cotton,eucalyptus,orange,sugarcane,maize,soybean,coffee,beans,and potatoes.The territory occupied by agricultural areas and ADPs required by the Brazilian Forest Code shows that agricultural production and environmental preservation do coexist,and gather the maintenance of essential ecosystem services provided by the ADPs together with the development of the country’s relevant agricultural production.
基金supported by the National Basic Research Programof China(2014CB046905)the Fundamental Research Funds for the Central Universities(China University of Mining and Technology)(2014YC10)
文摘A discrete element method （DEM） called particle flow code （PFC2D） was used to construct a model for Brazilian disc splitting test in the present study. Based on the experimental results of intact Brazilian disc of rock-like material, a set of micro-parameters in PFC2D that reflected the macro-mechanical behavior of rock-like materials were obtained. And then PFC2D was used to simulate Brazilian splitting test for jointed rock mass specimens and specimen containing a central straight notch. The effect of joint angle and notch angle on the tensile strength and failure mode of jointed rock specimens was detailed analyzed. In order to reveal the meso-mechanical mechanism of crack coalescence, displacement trend lines were applied to analyze the displacement evolution during the crack initiation and propagation. The investigated conclusions can be described as follows. （1） The tensile strength of jointed rock mass disc specimen is dependent to the joint angle. As the joint angle increases, the tensile strength of jointed rock specimen takes on a nonlinear variance. （2） The tensile strength of jointed rock mass disc specimen containing a central straight notch distributes as a function of both joint angle and notch angle. （3） Three major failure modes, i.e., pure tensile failure, shear failure and mixed tension and shear failure mode are observed in jointed rock mass disc specimens under Brazilian test. （4） The notch angle roles on crack initiation and and joint angle play important propagation characteristics of jointed rock mass disc specimen containing a central straight notch under Brazilian test.
基金The fnancial support of the Research Council of the Katholieke Universiteit Leuven(OT-project OT/03/35)
文摘The experimental study in this paper focuses on the effects of the layer orientation and sample shape on failure strength and fracture pattern of samples tested under Brazilian test conditions(i.e.diametrical loading of cylindrical discs)for one particular layered sandstone which is from Modave in the south of Belgium.The variations of the strength in combination with the failure patterns are examined as a function of the inclination angle between the layer plane and the loading direction.The experimental,results clearly show that the induced fracture patterns are a combination of tensile and/or shear fractures.In shape effect experiments the layer thickness and the number of layer boundaries are investigated.Different blocks of Modave sandstone are used to prepare samples.The layer thickness is different among the various blocks,but the layer thickness in each studied rock block can be considered to be constant;hence,the number of layer boundaries changes according to the sample diameter for samples of the same block.The experimental study shows that the layer thickness plays a more important role than the number of layer boundaries per sample.
基金Projects(42077244,41877272,41472269)supported by the National Natural Science Foundation of ChinaProject(2242020R10023)supported by the Fundamental Research Funds for the Central Universities of Southeast University,China。
文摘Tensile failure(spalling or slabbing)often occurs on the sidewall of deep tunnel,which is closely related to the coupled stress state of deep rock mass under high pre-static load and dynamic disturbance.To reveal the mechanism of rock tensile failure caused by this coupled stress mode,the Brazilian disc tests were carried on red sandstone under high pre-static load induced by dynamic disturbance.Based on the pure static tensile fracture load of red sandstone specimen,two static load levels(80%and 90%of the pure static tensile fracture load)were selected as the initial high pre-static loading state,and then the dynamic disturbance load was applied until the rock specimen was destroyed.The dynamic disturbance loading mode adopted a sinusoidal wave(sine-wave)load,and the loading wave amplitude was 20%and 10%of the pure static tensile fracture load,respectively.The dynamic disturbance frequencies were set to 1,10,20,30,40,and 50 Hz.The results show that the tensile failure strength and peak displacement of red sandstone specimens under coupled load actions are lower than those under pure static tensile load,and both parameters decrease significantly with the increase of dynamic disturbance frequency.With the increase of dynamic disturbance frequency,the decrease range of tensile strength of red sandstone increased from 3.3%to 9.4%when the pre-static load level is 80%.While when the pre-static load level is 90%,the decrease range will increase from 7.4%to 11.6%.This weakening effect of tensile strength shows that the deep surrounding rock is more likely to fail under the coupled load actions of pre-static load and dynamic disturbance.In this tensile failure mechanism of the deep surrounding rock,the stress environment of deep sidewall rock determines that the failure mode of rock is a tensile failure,the pre-static load level dominates the tensile failure strength of surrounding rock,and dynamic disturbance promotes the strength-weakening effect and affects the weakening range.
基金Projects(50904079, 51274254, 50934006) supported by the National Natural Science Foundation of ChinaProject(2010CB732004) supported by the National Basic Research Program of ChinaProject(NCET-11-0528) supported by Program for New Century Excellent Talents in University of China
文摘To reveal stress distribution and crack propagation of Brazilian discs under impact loads, dynamic tests were conducted with SHPB （split Hopkinson pressure bar） device. Stress states of specimens were monitored with strain gauges on specimen surface and SHPB bars. The failure process of specimen was recorded by ultra speed camera FASTCAM SAI.1 （675 000 fps）. Stress histories from strain gauges offer comprehensive information to evaluate the stress equilibrium of specimen in time and space. When a slowly rising load （with loading rates less than 1 200 N/s for d 50 mm bar） is applied, there is usually good stress equilibrium in specimen. The stress distribution after equilibrium is similar to its static counterpart. And the first crack initiates at the disc center and propagates along the load direction. But with the front of incident wave becoming steep, it is hard for specimens to get to stress equilibrium. The first crack may appear anywhere on the specimen together with multiple randomly distributed secondary cracks. For a valid dynamic Brazil test with stress equilibrium, the specimen will break into two halves neatly. While for tests with stress disequilibrium, missing strap may be found when broken halves of specimens are put together. For those specimens broken up neatly at center but having missing wedges at the loading areas, it is usually subjected to local buckling from SHPB bars.
基金Project (50274074) supported by the National Natural Science Foundation of China
文摘A new specimen geometry-the double edge-cracked Brazilian disk and a relevant fracture analysis byweight function method are proposed for the investigation of rock fracture caused by compression-shear loading. Notonly can the mixed mode fracture with any ratio of KⅠ/KⅡ be achieved, but also the pure mode Ⅱ crack extensioncan be obtained. The combined mode fracture analysis for this geometry shows that diametral compression in the far-field can induce a compression-shear stress state in the singular stress field ahead of crack tips. Experimental investi-gations conducted on marble specimens show that the pure mode Ⅱ crack extension can be obtained when the dimen-sionless crack length a＞0.7 and the inclined crack angle 5°≤ψ≤40°. Normalized mode Ⅰ and mode Ⅱ stress inten-sity factors decrease from -0.45 and 2.47 at ψ=5° to -1.65 and 1.52 at ψ=40°, respectively. The strains at threepoints of specimen are also measured in order to investigate the influence of stress singularity on initial crack exten-sion. The results show that the principal orientations of strain at three points are very stable in the loading process.The derived formulae are quite explicit, and the specimen geometry is easy to fabricate and convenient to achieve thepure mode Ⅱ crack extension. Therefore, it can hopefully be used to obtain mode Ⅱ fracture toughness of rock.
基金co-financed by the EU(European Social Fund-ESF)Greek National Funds through the Operational Program "Education and Lifelong Learning" of the National Strategic Reference Framework(NSRF)-ResearchFunding Program:THALES:Reinforcement of the interdisciplinary and/or inter-institutional research and innovation
文摘The general contact problem of a disc squeezed between jaws of arbitrary curvature is considered employing Muskhelishvili’s complex potentials.Taking advantage of the general solution introduced,the closed-form expressions for the stresses along strategic loci(loaded rim,loaded diameter,disc’s center)are obtained,in terms of the ratio r of the disc’s to the jaw’s curvature.Then,the effect of r(as well as that of the relative stiffness of the disc’s and jaw’s materials dictating the contact arc)on the stress distribution along these loci is explored.It is concluded that,for both smooth contact(zero friction)and contact with friction,the role of the jaw’s curvature is significant not only along the disc-jaw contact arc(as it could be expected),but also all along the loaded diameter.On the other hand,it is indicated that the stress field at the disc’s center is more or less insensitive to the jaw’s curvature assuming that r lies within the range(0,0.67)or in other words within the limits defined by the two standardized suggestions,i.e.that of American Society for Testing and Materials(ASTM)(plane loading platens with r ? 0)and that of International Society for Rock Mechanics(ISRM)(curved jaws with r ? 0.67).The upper limit of this range is a kind of compromise between the need to make the stress field at the disc’s center independent of the boundary conditions while keeping at the same time the contact angle large enough to reduce the stress concentration and the risk for premature fracture initiation far from the disc’s center.For jaws with radius of curvature exceeded by that suggested by ISRM,the stress field at the disc’s center is significantly influenced.Especially for jaws with radius approaching that of the disc,the stress field at the disc’s center is dramatically distorted rendering Hondros’ formula inapplicable and the test results erroneous.
基金funding support from the Sichuan Science and Technology Program (Grant No. 2021YJ0511)the State Key Laboratory for Geo-Mechanics and Deep Underground Engineering,China University of Mining&Technology (Grant No.SKLGDUEK2111)the Key Laboratory of Rock Mechanics and Geohazards of Zhejiang Province (Grant No. ZJRMG-2020-01)。
文摘Cracked straight-through Brazilian disc(CSTBD) samples prepared using two rock materials were used for thermal treatment from room temperature to 700℃. Uniaxial splitting experiments were performed using an automatic electro-hydraulic servo press to study the evolution laws of physical and fracture properties of different deep rock materials under high-temperature geological conditions. The fracture characteristics were measured using an industrial camera and digital image correlation technology to analyze the effect of high temperature on fracture properties and failure modes of the CSTBD samples after different thermal treatments. The micro-damage properties of green sandstone and granite materials were obtained using a scanning electron microscope(SEM). The following conclusions were drawn from the test results:(1) With the increasing temperature, the fracture characteristics of green sandstone and granite change from brittle fracture to plasticity fracture, the longitudinal wave velocity of granite decreases sharply at 600℃, and the damage factor reaches 0.8748 at 700℃.(2) The fracture toughness of green sandstone and granite decreases with increasing temperature;however, the decreasing range of granite is larger than that of green sandstone.(3) As the temperature increases, the fracture morphologies of green sandstone and granite materials become rougher, whereas thermal damage cracks of granite and intergranular fractures inside sandstone as well as pores of sandstone increase.(4) The crack tip opening displacement and peak strain corresponding to peak load increase with the temperature.
基金Funded by the National Natural Science Foundation of China(Nos.51678170,51878190)。
文摘Split Hopkinson pressure bar(SHPB)has been used to study the dynamic failure pattern of flattened mortar Brazilian disc under impact load.Each disc contains several prefabricated cracks paralleled to each other.Dynamic FEM has also been adopted to simulate such failure behavior.The mechanism of crack initiation,propagation and cut-through have been scrutinized with both experimental and numerical approaches.Influence of the number of the prefabricated cracks on the specimen strength and acoustic emission(AE)performance can be observed and studied.The results show that the strength decreases and AE counts increases,when the number of the prefabricated cracks increases.
基金Support provided by the National Basic Research Program of China (2015CB258500, 2015CB058102, 2014CB046904)
文摘The Brazilian test is a widely used method for determining the tensile strength of rocks and for calibrating parameters in bondedparticle models（BPMs）. In previous studies, the Brazilian disc has typically been trimmed from a compacted rectangular specimen. The present study shows that different tensile strength values are obtained depending on the compressive loading direction. Several measures are proposed to reduce the anisotropy of the disc. The results reveal that the anisotropy of the disc is significantly influenced by the compactibility of the specimen from which it is trimmed. A new method is proposed in which the Brazilian disc is directly generated with a particle boundary, effectively reducing the anisotropy. The stiffness（particle and bond） and strength（bond） of the boundary are set at less than and greater than those of the disc assembly, respectively,which significantly decreases the stress concentration at the boundary contacts and prevents breakage of the boundary particle bonds. This leads to a significant reduction in the anisotropy of the disc and the discreteness of the tensile strength. This method is more suitable for carrying out a realistic Brazilian test for homogeneous rock-like material in the BPM.
文摘The center cracked Brazilian disk subjected to diametral compressive stress uniformly distributed along parts of its cylindrical surface is used to investigate combined mode fracture of brittle material. A fracture analysis is made of this specimen configuration. Explicit formulae for mode Ⅰ and mode Ⅱ stress intensity factor calculation are derived based on boundary integral equation method and related numerical solution given by Atkinson. The proposed formulae are valid in wide range of crack length a/R . This configuration can avoid splitting along load line usually occuring in Brazilian test and permit one to achieve easily pure mode Ⅱ crack growth (crack coplanar extension) and any combination of K Ⅰ and K Ⅱ by a simple alignment of crack orientation with respect to load line. SIF values from the present calculation and finite element solution are also given for comparison.
基金[This work was financially supported by the Fundamental Science Research Fund of Southwest Jiaotong University (No.2004B13).
文摘It is claimed that the formula used for calculating the tensile strength of a disk-shaped rock specimen in the Brazilian test is not accurate, because the formula is based on the 2-dimensional elastic theory and only suitable for very long or very short cylinders. The Matlab software was used to obtain the 2-dimensional distribution of stress in the rock specimen for Brazilian test. Then the 2-dimensional stress distribution in Brazilian disk was analyzed by the Marc FEM software. It can be found that the results obtained by the two software packages can verify each other. Finally, the 3-dimensional elastic stress in the specimen was calculated. The results demonstrate that the distribution of stress on the cross section of the specimen is similar to that in 2-dimension. However, the value of the stress on the cross section varies along the thickness of the specimen and the stress is bigger when getting closer to the end of the specimen. For the specimen with a height-to-diameter ratio of 1 and a Poisson＇s ratio of 0.25, the tensile strength calculated with the classical 2-D formula is 23.3% smaller than the real strength. Therefore, the classical 2-D formula is too conservative.
基金Funded by the National Natural Science Foundation of China(Nos.51878190 and 51678170)。
文摘Both experimental and numerical approaches were used to study dynamic failure properties and patterns of flattened Brazilian discs,containing two prefabricated cracks intersected at a varying angle.Mechanism of crack initiation,propagation,and cut-through were scrutinized and influences of the intersection angle on specimen strength and acoustic emission performance were also studied.All primary cracks initialize near the middle or the tip points of the upper prefabricated crack,and they continue to develop along the load direction and finally cut through the specimen.The secondary cracks could be observed in directions almost horizontal or parallel to the directions of prefabricated cracks.Furthermore,it is found that stress intensity factor reaches its maximum for specimen with intersection angle of 0 degree.
基金We acknowledge the funding support from the National Natural Science Foundation of China(Grant Nos.42141010,51879184 and 12172253).
文摘Dynamic tensile failure is a common phenomenon in deep rock practices,and thus accurately evaluating the dynamic tensile responses of rocks under triaxial pressures is of great significance.The Brazilian disc(BD)test is the suggested method by the International Society for Rock Mechanics and Rock Engineering(ISRM)for measuring both the static and dynamic tensile strengths of rock-like materials.However,due to the overload phenomenon and the complex preloading conditions,the dynamic tensile strengths of rocks measured by the BD tests tend to be overestimated.To address this issue,the dynamic BD tensile strength(BTS)of Fangshan marble(FM)under different preloading conditions were measured through a triaxial split Hopkinson pressure bar(SHPB).The fracture onset in BD specimen was captured through a strain gage around the disc center.The discrepancy between the traditional tensile strength(TTS,determined by the peak load P_(f) of the BD specimen)and the nominal tensile strength(NTS,obtained from the load P_(i) when the diametral fracture commences in the tested BD specimen)was applied to quantitatively evaluating the overload phenomenon.The Griffith criterion was used to rectify the calculation of the tensile stress at the disc center under triaxial stress states.The results demonstrate that the overload ratio(s)increases with the loading rate(σ)and decreases with the hydrostatic pressure(σ_(s)).The TTS corrected by the Griffith criterion is independent of theσ_(s)due to the overload phenomenon,while the NTS corrected by the Griffith criterion is sensitive to both the andσ.Therefore,it is essential to modify the tensile stress in dynamic confined BD tests using both the overload correction and the Griffith criterion rectification to obtain the accurate dynamic BTS of rocks.
基金We are grateful to SaōPaulo Research Foundation for the financial support of this research and for the fellowships awarded to C.A.B.(FAPESP No.2011/19057-7)G.A.B.(FAPESP No.2012/21395-0)to Study Group of Cerrado Agroindustrial Processes(GEPPAC)of the Federal University of Grande Dourados to provide laboratories for plant material processing step.
文摘The increasing demand for safe food without preservatives or pesticides residues has encouraged several studies on natural products with antifungal activity and low toxicity.In this study,ethanolic extracts from leaves and fruit residues(peel and seeds)of three Brazilian savanna species(Acrocomia aculeata,Campomanesia adamantium and Caryocar brasiliense)were evaluated against phytopathogenic fungi.Additionally,the most active extract was chemically characterized by ESI-MS and its oral acute toxicity was evaluated.Extracts from C.brasiliense(pequi)peel and leaves were active against Alternaria alternata,Alternaria solani and Venturia pirina with minimal inhibitory concentrations between 350 and 1000 lg/mL.When incorporated in solid media,these extracts extended the lag phase of A.alternata and A.solani and reduced the growth rate of A.solani.Pequi peel extract showed better antifungal activity and their ESI-MS analysis revealed the presence of substances widely reported as antifungal such as gallic acid,quinic acid,ellagic acid,glucogalin and corilagin.The oral acute toxicity was relatively low,being considered safe for use as a potential natural fungicide.
文摘Brazil is the largest producer of sugarcane and its derivatives in the world, and one of the largest consumers of sugarcane derivatives. Sugar places a position of great prominence in Brazilian feed, either by direct consumption or as a component of industrialized products, from increasing consumption in the country. Sugar samples taken from local market were analyzed as the quality of table sugar consumed in the state of Sao Paulo (Brazil). The analysis of the parameters and basic attributes of characterization of sugar was according to the methodology developed by ICUMSA (2005;2011) and ICUMSA modified by Copersucar (2002). Samples of sugar from this region showed that medium-low quality. It can be observed in fundamental aspects such as purity and insoluble residues, which were below the standard. In addition, it should be noted the difficulty of obtaining information about the limit values for each attribute, by virtue of Legislation not be assertive to the product and, also, the scientific studies have not been unified to present the specifics for each type of sugar.
