A series of oxygen deficient perovskite supported palladium catalysts were prepared by the “solid phase crystallization'(spc) method and investigated with XRD, TPR, TPD, TEM, XPS, BET analysis and CO oxidation. I...A series of oxygen deficient perovskite supported palladium catalysts were prepared by the “solid phase crystallization'(spc) method and investigated with XRD, TPR, TPD, TEM, XPS, BET analysis and CO oxidation. It was found that Pd/perovskite catalysts synthesized by the spc method were more active for CO oxidation than the calcined LaCo 0 95 Pd 0 05 O 3, where Pd dispersed in the solid solution. H 2 reducing treatment in the spc method could yield not only high dispersed fine Pd particles on the perovskite surface but also oxygen deficient structure. In these perovskite supported Pd catalysts, oxygen vacancies adsorbed, activated and supplied oxygen to the active Pd sites, where the oxidation occurred with adsorbed CO. The high activities were due to the cooperative action of Pd and oxygen vacancies.展开更多
本文在介绍用户程控交换机故障诊断基本原理的基础上,采用功能测试的方法,对不同的印刷电路板使用不同的等效黑盒进行测试。在完全不改变整机结构的情况下,仅增加一块诊断板,便可通过软件对各种印刷电路板及其单元电路进行测试和故障诊...本文在介绍用户程控交换机故障诊断基本原理的基础上,采用功能测试的方法,对不同的印刷电路板使用不同的等效黑盒进行测试。在完全不改变整机结构的情况下,仅增加一块诊断板,便可通过软件对各种印刷电路板及其单元电路进行测试和故障诊断。故障定位的准确度对单块印刷电路板,单元电路以及单个 IC 芯片分别为100%,80%以及和70%左右。展开更多
文摘A series of oxygen deficient perovskite supported palladium catalysts were prepared by the “solid phase crystallization'(spc) method and investigated with XRD, TPR, TPD, TEM, XPS, BET analysis and CO oxidation. It was found that Pd/perovskite catalysts synthesized by the spc method were more active for CO oxidation than the calcined LaCo 0 95 Pd 0 05 O 3, where Pd dispersed in the solid solution. H 2 reducing treatment in the spc method could yield not only high dispersed fine Pd particles on the perovskite surface but also oxygen deficient structure. In these perovskite supported Pd catalysts, oxygen vacancies adsorbed, activated and supplied oxygen to the active Pd sites, where the oxidation occurred with adsorbed CO. The high activities were due to the cooperative action of Pd and oxygen vacancies.
文摘本文在介绍用户程控交换机故障诊断基本原理的基础上,采用功能测试的方法,对不同的印刷电路板使用不同的等效黑盒进行测试。在完全不改变整机结构的情况下,仅增加一块诊断板,便可通过软件对各种印刷电路板及其单元电路进行测试和故障诊断。故障定位的准确度对单块印刷电路板,单元电路以及单个 IC 芯片分别为100%,80%以及和70%左右。
