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超声化学制备单分散金属纳米钯 被引量:17

Synthesis of Palladium Nanoparticles by A Sonochemical Method
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摘要 A simple sonochemical technique is used to synthesize palladium nanoparticles in a poly(ethylene glycol) (PEG) solvent at room temperature. The reaction based on chemical reduction of PdCl2 by ascorbic acid (AA). The as prepared Pd nanoparticles are highly dispersed and uniform in size (with average size of ~ 20nm). The products were characterized by X ray powder diffraction (XRD) and transmission electron microscopy (TEM). A simple sonochemical technique is used to synthesize palladium nanoparticles in a poly(ethylene glycol) (PEG) solvent at room temperature. The reaction based on chemical reduction of PdCl2 by ascorbic acid (AA). The as prepared Pd nanoparticles are highly dispersed and uniform in size (with average size of similar to 20nm). The products were characterized by X-ray powder diffraction (XRD) and transmission electron microscopy (TEM).
机构地区 南京大学化学系
出处 《无机化学学报》 SCIE CAS CSCD 北大核心 2003年第7期766-770,共5页 Chinese Journal of Inorganic Chemistry
基金 国家自然科学基金资助项目(No.50072006 90206037) 江苏高新计划资助项目(No.BG2001039)。
关键词 超声化学 制备 单分散 金属钯 聚乙二醇 纳米材料 sonochemistry nano palladium PEG
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