摘要
本文介绍了5—硝基糠叉二醋酸酯的制备方法。讨论了不同硝化体系对收率的影响,实验表明,发烟硝酸作为硝化剂收率最高。
The title compound was prepared by nitration of furfural with five kinds of nitration systems ( fuming HNO3, Ac2O; HNO3, Ac2O, SbSl3; HNO3, Ac2O, P-toluene-slfonic acid; H2SO4, NaIO3, NaNO3, Ac2O; HNO3) The highest gield was obtained in nitration with the fuming HNO3 system.
出处
《河北大学学报（自然科学版）》
CAS
1992年第3期78-80,共3页
Journal of Hebei University(Natural Science Edition)
关键词
醋酸酯
制备
糠醛
硝化
5-Nitrofurfurylidene diacetate, Preparation, Furfural, Nitration.
