摘要
邻苯二甲酸酯(PAEs)类塑化剂是一种环境污染物,具有生殖毒性,易致癌、致畸,植物油易受到PAEs污染。旨在为植物油中PAEs类塑化剂检测方法的开发提供参考,对植物油中PAEs类塑化剂检测技术的前处理方法和定量检测技术进行了综述,比较了各方法的优缺点,并对其发展趋势进行了展望。PAEs类塑化剂检测的前处理方法包括液-液萃取法、固相萃取法、凝胶渗透色谱法和QuEChERS法等;定量检测技术包括高效液相色谱法、气相色谱法、液相色谱-质谱联用法、气相色谱-质谱联用法等。未来联合前处理技术、在线净化、微萃取,以及三重四极杆气相色谱-质谱联用技术等将成为PAEs类塑化剂检测的发展方向。
Phthalate esters(PAEs)plasticizers are environmental pollutants associated with reproductive toxicity,cancer risks,and birth defects.Vegetable oils are prone to PAEs contamination.In order to provide a reference for advancing PAEs detection methods,the pre-treatment methods and quantitative detection technologies of PAEs detection were reviewed,and their advantages and disadvantages were compared.The development trends of detection technology of PAEs were prospected.The pre-treatment methods of PAEs detection includes liquid-liquid extraction,solid-phase extraction,gel permeation chromatography,and QuEChERS,etc.The quantitative detection technologies for PAEs in vegetable oils include high-performance liquid chromatography,gas chromatography,liquid chromatography-mass spectrometry,gas chromatography-mass spectrometry,etc.Future directions in PAEs detection technology are expected to focus on the integration of combined pre-treatment approaches,online purification,microextraction techniques,and gas chromatography-tandem triple-quadrupole mass spectrometry(GC-MS/MS).
作者
贺诗意
张蕊
周明慧
王松雪
朱琳
付湘晋
HE Shiyi;ZHANG Rui;ZHOU Minghui;WANG Songxue;ZHU Lin;FU Xiangjin(Academy of National Food and Strategic Reserves Administration,Beijing 100037,China;College of Food Science and Engineering,Central South University of Forestry and Technology,Changsha 410004,China)
出处
《中国油脂》
北大核心
2025年第9期33-39,共7页
China Oils and Fats
基金
“十四五”国家重点研发计划(2022YFF0710400,2022YFF0710404)
“十三五”国家重点研发计划(2019YFC1605200,2019YFC1605202)。
关键词
植物油
塑化剂
邻苯二甲酸酯
前处理方法
定量检测技术
vegetable oil
plasticizer
phthalate esters
pre-treatment method
quantitative detection technique
