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虾活性肽微胶囊的制备工艺优化及其理化性质

Optimization of Preparation Process and Physicochemical Properties of Shrimp Bioactive Peptide Microcapsules
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摘要 为提高虾活性肽的稳定性和作用效果,以阿拉伯胶和β-环糊精为壁材,采用喷雾干燥法制备虾活性肽微胶囊(shrimp bioactive peptide microcapsules,SBPM),实现虾活性肽的微胶囊化,并开展制备工艺优化和理化性质研究。试验结果表明:当壁材比(阿拉伯胶与β-环糊精的质量比)为3∶1、芯材与壁材质量比为1∶4、固形物含量为15%、单甘酯添加量为0.4%时,制备的SBPM为淡黄色类粉末,呈现类球体结构,无孔洞、开裂及不良气味,特征粒径D_(90)<10μm,流动性良好,虾活性肽包埋率为(90.11±0.23)%;虾活性肽与壁材之间的分子间相互作用促使二者形成微胶囊;微胶囊化可明显降低虾活性肽的吸湿性;SBPM经模拟胃肠液消化12 h的多肽累计释放量达89.82%,具有较好的缓释性能。 In order to improve the stability and efficacy of shrimp bioactive peptides,microencapsulation was carried out with Arabic gum andβ-cyclodextrin as wall materials through a spray-drying method,generating shrimp bioactive peptide microcapsules(SBPM).The preparation process was optimized,and the physico-chemical properties of SBPM were studied.The results showed that the prepared SBPM was a faint yellow pow-der with a spherical-like structure,no holes,cracks,or undesirable odors,a characteristic particle size of D90<10μm,and good flowability at the following conditions:wall material ratio(Arabic gum toβ-cyclodextrin mass ratio)of 3∶1,the core-to-wall ratio of 1∶4(mass ratio),the solid content of 15%,and the monoglyceride con-tent of 0.4%.The encapsulation efficiency of shrimp bioactive peptides reached(90.11±0.23)%.The intermo-lecular interactions between the shrimp bioactive peptides and the wall materials facilitated the formation of mi-crocapsules.Microencapsulation significantly reduced the hygroscopicity of the shrimp bioactive peptides.Af-ter 12 hours of digestion in simulated gastrointestinal fluid,the cumulative release of peptides from SBPM reached 89.82%,indicating good sustained-release performance.
作者 吴泽龙 白锴凯 何建林 洪碧红 WU Zelong;BAI Kaikai;HE Jianlin;HONG Bihong(Technical Innovation Center for Utilization of Marine Biological Resources,Third Institute of Oceanography,Ministry of Natural Resources,Xiamen 361005,Fujian,China;College of Food Science,Fujian Agriculture and Forestry University,Fuzhou 350002,Fujian,China)
出处 《食品研究与开发》 2025年第4期100-106,共7页 Food Research and Development
基金 福建省海洋经济发展专项资金项目(FJHJF-L-2022-6) 自然资源部第三海洋研究所基本科研业务费(2018013)。
关键词 南美白对虾 虾活性肽 微胶囊 喷雾干燥 工艺优化 Penaeus vannamei shrimp bioactive peptide microcapsules spray-drying process optimization
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