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5,11,17,23-四叔丁基-25,26,27,28-四[3-(甲氧基羰基)苄氧基]杯[4]芳烃包合性能的研究 被引量：4

Studies on the Inclusion Property of 5,11,17,23-Tetra-tert-butyl-25,26, 27,28-tetrakis[3-(methoxycarbonyl)benzyloxy]calixarene
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摘要 The synthesis of a novel host blocked in the cone conformation and bearing m-methoxycarbonylbenzyl groups at the lower rim is described. X-ray crystal structure analysis revealed that action of one molecule of compound upon one molecule of CH 3CN or one molecule of CH 3NO 2, forms an intramolecular inclusion complex, respectively, by CH 3-π interactions. The complex of L with tetrabutyl ammonium bromide(TBAB), L·TBAB, was obtained. The results of DTA-TG and XRD analysis of L·TBAB can also be considered as an intramolecular inclusion complex. The synthesis of a novel host blocked in the cone conformation and bearing m-methoxycarbonylbenzyl groups at the lower rim is described. X-ray crystal structure analysis revealed that action of one molecule of compound upon one molecule of CH 3CN or one molecule of CH 3NO 2, forms an intramolecular inclusion complex, respectively, by CH 3-π interactions. The complex of L with tetrabutyl ammonium bromide(TBAB), L·TBAB, was obtained. The results of DTA-TG and XRD analysis of L·TBAB can also be considered as an intramolecular inclusion complex.
作者 周稚仙 石雅琳 杜晨霞 邢彦军 吴养洁
机构地区 郑州大学化学系
出处 《高等学校化学学报》 SCIE EI CAS CSCD 北大核心 2002年第12期2281-2283,共3页 Chemical Journal of Chinese Universities
基金 国家自然科学基金 (批准号 :2 9872 0 34)资助
关键词 包合性能 5 11 17 23-四叔丁基-25 26 27 芳烃 超分子 晶体结构 季铵盐 包合物 Calixarene Crystal structure Quaternary ammonium cation Inclusion complex
分类号 O641.3 [理学—物理化学]
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  • 1周稚仙,石雅琳,杜晨霞,邢彦军,吴养洁.Studies on the Intramolecular Inclusion Complexes of Functionalized Calixarenes with CH_3X (X=CN, NO_2)[J].Chinese Journal of Chemistry,2002,20(11):1205-1211. 被引量：1
  • 2陈轶华,罗虹.杯芳烃受体的合成及其对氨基酸的识别[J].南华大学学报（自然科学版）,2005,19(F09):99-102. 被引量：3
  • 3GUILBAULT G G, DURST R A, FRANT M S, et al. Recommendations for nomenclature of ion-selective electrodes[J]. Pure & Appl Chem, 1976, 48(1) : 127- 132.
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  • 5MCKERVEY M A, SEWARD E M, FERGUSON G, et a]. Synthesis, x-ray crystal structures, and cation transfer properties of alkyl calixaryl acetates, a new series of molecular receptors[J]. J Chem Soc Chem Commun, 1985. 388 - 390.
  • 6DIAMOND D, SVEHLA G. A sodium ion-selective electrode based on methyl p-t-butylcalix[ 4]aryl acetate as the ionophore[J]. Anal Chim Acta, 1988, 204: 223-231.
  • 7BOHMER V. Calixarenes, macrocycles with(almost) unlimited possibilities[J]. Angew Chem Int Ed Engl, 1995, 34(7):713 - 745.
  • 8GUTSCHE C D. Calixarenes, monographs in supramolecular chemistry[M]. Cambridge: The Royal Society of Chemistry,1989.
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高等学校化学学报
2002年 第12期

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