摘要
采用双辉等离子技术在机械曲轴表面制备了SiC/Ta复合涂层,研究了合成温度对复合涂层显微形貌、物相组成、耐磨和耐腐蚀性能的影响。结果表明,当合成温度从750上升至900℃时,复合涂层表面形貌由花纹状逐渐演变成细小颗粒团簇状,截面形貌中可见不同合成温度下复合涂层厚度和内部质量存在一定差异,不同合成温度的复合涂层中都出现了SiC、Ta、Ta_(2)C和TaC衍射峰。机械曲轴基体的摩擦系数都高于不同合成温度下的复合涂层,合成温度800℃时复合涂层的摩擦系数最小且最为稳定;随着合成温度升高,磨痕深度、磨痕宽度、磨损体积和比磨损率都呈现先减小后增大的特征,在合成温度为800℃时磨损体积和比磨损率最小;极化曲线和电化学阻抗谱测试结果保持一致,即复合涂层的耐蚀性能都优于基体,且合成温度为800℃时复合涂层的耐蚀性能最好;机械曲轴表面适宜的复合涂层合成温度为800℃,此时复合涂层具有最佳的耐蚀和耐磨性能。
The surfaces of 4 Cr13 stainless steel, a crankshaft material, were modified and reconditioned with SiC/Ta coatings by double glow discharge plasma alloying.The influence of the surface alloying temperature and Ta-transition layer on the tribological behavior of the coatings was investigated with X-ray diffraction, scanning electron microscopy, conventional mechanical probes and electrochemistry work station.The results show that the alloying temperature had a major impact.To be specific, the Ta-transition layer considerably enhanced the interfacial adhesion and improved the toughness;as the alloying temperature increased from 750℃ to 900℃,the wear-resistance and corrosion-resistance changed in an increase-decrease mode, peaking at 800℃.Moreover, alloyed at 800℃,the coatings had the lowest friction coefficient, because of the refinement of texture and grain size.Abrasive wear was found to account for the wear mechanism.
作者
王波
徐颖梅
赵东宏
张崎静
WANG Bo;XU Yingmei;ZHAO Donghong;ZHANG Qijing(Yangzhou Polytechnic Institute,Yangzhou 225127,China;Nanjing University Of Aeronautics and Astronautics,college of materials science and technology,Nanjing 210016,China)
出处
《真空科学与技术学报》
CAS
CSCD
北大核心
2021年第3期241-247,共7页
Chinese Journal of Vacuum Science and Technology
基金
江苏省自然科学基金项目(BK20180495)
机械设计与制造行业骨干专业项目(XM-01)
江苏省教育科学“十二五”规划2015年度职成教重点资助课题(B-a/2015/03/008)
扬州市校合作资金项目(YZ2016271)
扬州工业职业技术学院重点科研课题(2016xjzk004)。
关键词
双辉等离子技术
机械曲轴
复合涂层
耐磨
耐蚀性能
Double glow plasma technology
Mechanical crankshaft
Composite coating
Wear resistance
Corrosion resistance
