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原位合成莫来石-碳化硅系复合材料 被引量:12

In situ Synthesis of Mullite Siliconcarbide Composite Materials
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摘要 以铝 硅系天然矿物 蜡石和天然石墨为原料,通过碳热还原法原位合成了莫来石 碳化硅系复合材料·并对合成复合材料的韧性、抗压强度和抗渣侵蚀性能进行了测定·研究结果表明,通过向蜡石中添加适量的天然石墨,并将蜡石和天然石墨的混合物在氩气气氛下加热到1550℃以上时,可以很容易地合成莫来石 碳化硅系复合材料;原位还原合成的碳化硅多呈球状,颗粒粒径在1μm左右且均匀地分布在生成的莫来石相中;与单一的莫来石材料相比较,合成的莫来石-碳化硅系复合材料的韧性、抗压强度和抗渣侵蚀性能明显提高· ?By using Aland Si containing natural pyrophyllite and natural graphite,mullitesiliconcarbide composite materials were synthesized with insitu carbothermal reduction reaction method. The toughness,strength and corrosion resistance of the synthesized mullitesiliconcarbide composite materials were investigated. The results show that the mullitesiliconcarbide composite materials can be easily manufactured by adding the natural graphite powder to the pyrophyllite and heating the admixtures in argon atmosphere over 1?550?℃. The microstructure observation shows that the siliconcarbide phase has spherical shape,and is welldistributed in the mullite matrix and the siliconcarbide particle size is around 1?μm. The toughness,strength and corrosion resistance of the mullitesiliconcarbide composite materials are all improved compared with the mullite material.
出处 《东北大学学报(自然科学版)》 EI CAS CSCD 北大核心 2002年第11期1070-1072,共3页 Journal of Northeastern University(Natural Science)
基金 教育部科学技术研究重点项目(重点01057) 教育部留学回国人员科研启动基金资助项目
关键词 复合材料 莫来石 碳化硅 原位合成 碳热还原 composite materials mullite siliconcarbide in situ synthesis carbothermal reduction reaction
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参考文献8

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