摘要
建立了顶空-固相微萃取/气相色谱-质谱(HSSPME/GC-MS)联用法分析不同烙铁温度对同一规格不同批次卷烟中试试样烟丝样品中致香物质的组成及含量的影响。结果表明:①两个批次的成品烟丝共检测出35种核心致香成分,其中批次X含30种,批次Y含34种;②3-甲基-3-丁烯-2-酮、2-己烯-1-醇、2-(丁氧基乙氧基)乙醇、棕榈酸甲酯、3,5-二甲基苯酚为批次X未检测出成分,3-甲基-1,2-环戊二酮为批次Y未检测出成分,1,2-丙二醇为含量最高的致香物质;③F检验表明X、Y两个批次样品中致香成分含量的差异是来自于烙铁温度,将烙铁温度控制在270℃更利于保留烟丝中的致香成分。
Head space solid-phase microextraction(HS-SPME)coupled with chromatography-mass spectrometry(GC-MS)method was developed to study the effects of different temperature of the heater on the composition and content of aroma components in the test samples of different batches of cigarettes.The results were as follows:① A total of 35 core aroma components were detected in two batches of finished cut tobacco,of which batches X and Y contained 30 and 34 kinds respectively;② 3-methyl-3-buten-2-one,2-hexene-1-alcohol,2-(butoxyethoxy)ethanol,Methyl palmitate and 3,5-dimethylphenol were unde-tected components in X,while 3-methyl-1,2-cyclopentadione was undetected components in Y.1,2-propanediol was the highest content of aroma substances;(3) F-test showed that the difference in the content of aroma components in X and Y was resulted in by the temperature of heater and the temperature set at 270 ℃was more conducive to retain aroma components in tobacco.
作者
李超
袁湘云
李达
葛文
王家寿
LI Chao;YUAN Xiang-yun;LI Da;GE Wen;WANG Jia-shou(Technology Center of China Tobacco Yunnan Industrial Co., Ltd., Kunming, Yunnan 650024, China;Hongyun Honghe Tobacco 〔Group〕 Co., Ltd., Kunming, Yunnan 650231, China)
出处
《食品与机械》
北大核心
2019年第8期27-31,36,共6页
Food and Machinery
基金
红云红河烟草(集团)有限责任公司科技项目(编号:HYHH2018XX03)
云南省应用基础研究计划项目(编号:2017FD048)
关键词
烙铁温度
烟丝
致香成分
顶空-固相微萃取
气相色谱-质谱
heater temperature
finished tobacco
aroma component
head space solid-phase microextraction
chromatography-mass spectrometry
