摘要
制备了带平台的DD403合金变截面单晶铸件,分析了不同抽拉速率下平台区域的枝晶生长和取向演化。结果表明,平台底面由3种类型的区间构成:叶身区、二次枝晶区、平台边缘枝晶的"回路式"生长区。在平台边缘枝晶的"回路式"生长区与二次枝晶区之间的枝晶汇聚界面上,两侧枝晶的取向差由一侧向另一侧逐渐增大。随着抽拉速率的增大,枝晶汇聚界面上的取向差增大,其成为大角度晶界的倾向性增强,且枝晶偏转是枝晶汇聚界面上大角度晶界形成的主要原因。与晶粒间大角度晶界和亚晶粒间小角度晶界上恒定的取向差不同,枝晶汇聚界面上大角度晶界与小角度晶界的取向差是变化的。
Ni-based single crystal(SX) superalloys are widely used in key hot section parts of advanced aero engine and industrial gas turbines(IGTs) because of their superior mechanical performance at high temperature.During directional solidification process of SX blades,high angle grain boundaries that degrade the creep and fatigue properties significantly might be highly likely to occur in the platform region,thus the analysis of multi-influencing factors,such as platform dimension,withdrawal rate and seed orientation,need to be studied.However,most of these works are conducted from the perspective of heterogeneous nucleation induced by the extreme concave shape of liquid-solid interface,and there is rare report concerning that whether dendrite deformation could also induce the high angle grain boundaries.Therefore,in the present work,the SX castings with three platforms were directionally solidified in a Bridgman-furnace,to investigate dendrite growth and the associated orientation evolution.It was observed that the whole platform consisted of three types of regions: blade body,secondary dendrite spread zone,and the "circuit-like" dendrite growth zone.The convergent boundaries of dendrite arms(CBDAs) were formed between secondary dendrite spread zone and the "circuit-like" dendrite growth zone.With increasing withdrawal rate,the area of "circuit-like" dendrite growth zone was increased,and the area of secondary dendrite spread zone was reduced.Moreover,the monotonically increased misorientation angle along CBDAs as a result of the dendrite deformation around platform edge was identified.As withdrawal rate increased,the misorientation angle along CBDAs was increased,and thus the tendency of high angle grain boundary formation on the CBDAs was enhanced.Unlike the nearly constant misorientation angle of the high angle grain boundary between grains and the low angle grain boundary between subgrains,the misorientation angle of the high angle grain boundary and low angle grain boundary formed on the CBDAs varied regularly.
作者
孙德建
刘林
黄太文
张家晨
曹凯莉
张军
苏海军
傅恒志
SUN Dejian;LIU Lin;HUANG Taiwen;ZHANG Jiachen;CAO Kaili;ZHANG Jun;SU Haijun;FU Hengzhi(State Key Laborotory of Solidification Processing,Northwestern Polytechnical University,Xi'an 710072,China)
出处
《金属学报》
SCIE
EI
CAS
CSCD
北大核心
2019年第5期619-626,共8页
Acta Metallurgica Sinica
基金
国家自然科学基金项目Nos.51331005
51631008
51690163和51771148
国家重点研发计划项目Nos.2016YFB0701400和2017YFB0702900~~
关键词
单晶高温合金
枝晶生长
枝晶偏转
取向演化
大角度晶界
single crystal superalloy
dendrite growth
dendrite deformation
orientation evolution
high angle grain boundary
