摘要
目的建立和完善广西壮药粪箕笃药材的质量标准。方法根据《中国药典》2015年版第四部中药品标准研究方法首次对粪箕笃药材进行水分、灰分、酸不溶灰分、浸出物及重金属的检测,并采用高效液相色谱法对粪箕笃药材中千金藤啶碱成分进行鉴定。结果粪箕笃药材水分不高于16.10%,总灰分不高于13.90%,酸不溶性灰分不高于1.28%,浸出物不低于9.29%,粪箕笃药材不含有千金藤啶碱成分。结论该方法可作为制定和完善粪箕笃药材质量标准的依据。
Objective： To construct the quality standards of Stephania longa Lour. from Zhuang medicine materials in Guangxi. Methods： The characters as moisture, total ash, acid insoluble ash, extract and heavy metal ofS. longa Lour. were detected based on pharmaceutical standard in 2015 version. Stepholidine in S. longa Lour. was determined by HPLC. Results： S. longa＇s Lour. moisture, total ash, acid insoluble ash were not over 16.10%, 13.90% and 1.28% respectively, the extract was not less than 9.29%, and it had no Stepholidine. Conclusion： The results can be used as to develop and perfect the basis ofS. longa Lour. quality standard.
作者
庞丹清
魏中璇
陈勇
阙祖亮
魏江存
张昕
庾延和
PANG Dan-qing, WEI Zhong-xuan, CHEN Yong, QUE Zu-liang, WEI Jiang-cun, ZHANG Xin, YU Yan-he(College of Charmaey, Guangxi University of Chinese Medicine, Nanning, Guangxi 530200, Chin)
出处
《井冈山大学学报（自然科学版）》
2018年第1期82-86,共5页
Journal of Jinggangshan University (Natural Science)
基金
国家自然科学基金项目(81260673
81660701)
广西中医药大学科研创新项目(JS201625)
广西高校中药提取纯化与质量分析重点实验室(桂教科研[2014]6号)
关键词
壮药
粪箕笃
干金藤啶碱:质量标准
Zhuang medicine
Stephania longa Lour.
stepholidine
quality standard
