摘要
以醋酸锌和葡萄糖为原料用行星式球磨法及热解前驱体制备纳米碳—氧化锌复合材料。采用X-射线衍射仪和扫描电子显微镜对产物进行了结构和相貌表征,研究了碳源、热处理温度和时间等因素对纳米碳—氧化锌复合材料的影响。研究表明,以葡萄糖为碳源,热处理温度为400℃,热处理时间为10 min时,得到的碳—氧化锌复合材料产率为96.8%。
The nano-composite materials of carbon-zinc oxide were prepared using zinc acetate and glucose by planetary ball-milling method and heat treatment of the precursor in this paper. The structure and morphologies of the product were characterized by scanning electron microscopy（ SEM） and X-ray diffraction（ XRD）. The effects of carbon source,heat treatment temperature and time for the nano-composite materials of carbon-zinc oxide were studied. The result showed the yield of products of carbon-zinc oxide composite materials was 96. 8 % when the heat treatment was under 400℃ for 10 min and glucose as carbon source.
出处
《武汉轻工大学学报》
2015年第4期21-23,共3页
Journal of Wuhan Polytechnic University
关键词
纳米材料
热处理
行星式球磨法
碳—氧化锌
nanomaterials
heat treatment
planetary ball-milling method
C-Zn O
