摘要
以质量分数64%的硫酸水解脱脂棉，制备纤维素晶须。探讨了反应温度、反应时间和固液比对晶须产率的影响。结果表明，最佳制备条件为：反应温度55℃，反应时间30 min，固液比1：12 g/mL，在此条件下，所得纤维素晶须尺寸分布较为均匀，长度1~10μm，长径比为1~10。
A discussion about influences of factors including temperature,time and solid-liquid ratio on the preparation of cellulose whiskers and an optimization of preparation conditions were made by hydrolyzing absorbent cotton with sulfuric acid（64%,mass fraction）. The result shows that the best preparation con-dition is 55 ℃,30 min and 1 ：12 g/mL,under this condition,the size of prepared cellulose whiskers has a uniform distribution,the overall length is 1~10 μm and the length-diameter ratios is from 1~10.
出处
《应用化工》
CAS
CSCD
2014年第11期2049-2051,2055,共4页
Applied Chemical Industry
关键词
纤维素晶须
制备
产率
优化
cellulose whiskers preparation yield optimization
