摘要
以多聚磷酸 (PPA)为催化剂和反应溶剂 ,肉桂酸为酰化剂 ,对二苯并 - 2 4-冠 - 8进行酰化 ,成功地合成了茚满酮型二苯并 - 2 4-冠 - 8.经由IR ,MS和元素分析对合成的新产物的结构进行了鉴定 .
Indanone dibenzo-24-crown-8 has been synthesized in the condition of polyphosphoric acid(PPA) catalyst and solvent and cinnamic acid as acylating agent and dibenzo-24-crown-8 being acylated.The products are characterized by IR,MS and elements analysis.
基金
陕西省教育厅自然科学基金资助课题 (91K0 5 3)