摘要
本文以β-溴丙酸甲酯和锡直接反应合成了双甲氧羰乙基二溴化锡,并通过熔点测定、红外光谱和~1HNMR谱确认了该化合物。
Bis(methoxycarbonylethyl)tin dibromide was prepared by direct reaction of tin powder with methyl β-bromopropionate. Its composition and structure have been identified by its melting point, IR and ~1HNMR spectrum. The compound has an octahedral configuration of intramolecular coordination between caxbonyl and tin.
关键词
二溴化锡
烷氧羰乙基
合成
Bis(β-alkoxycarbonylethyl)tin dibromide
Bis(methoxycarbonylethyl)tin dibromide
Synthesis
Spectra
