摘要
运用主成分分析法对自增韧氮化硅陶瓷显微结构与力学性能的表征进行了研究.确定了该材料的显微结构可以用其表征变量的第一主成分一综合结构指标代表.为了获得结构优良的自增韧Si3N4陶瓷,需要保证致密(基体晶粒直径d1小、材料相对密度ρ高)的基体、长径比 AR2大、直径均匀(Y2 × 100小)的增韧相·通过综合结构指标的计算证实了综合结构指标相近的材料具有相近的力学性能二材料的力学性能可以用表征变量的第一、二主成分代表,分别称它们为性能稳定性指标和平均性能指标.前者代表材料受显微结构彼动影响的力学性能-断裂韧性KIC和Weibull模量m,后者代表材料的平均力学性能一抗弯强度σf.
The microstructure and mechanical properties of in-situ toughened Si3N4 were studied by principal components analysis. The microstructure can be characterized by the first principal component of its characterization variables, which intitules complex microstructure index. Compact matrix with fine grains and uniform large grains with great aspect ration must be ensured in order to get in-situ toughened Si3N4 with excellent microstructure. It has been approved that materials with similar complex microstructure index possessing similar mechanical properties. The mechanical proper-ties can be characterized by the first and the second principal components of its characterization variables, which intitule mechanical properties stability index and average mechanical properties index. The former one reflects fracture toughness and Weibull modulus which are affected by the fluctuation of microstructure; the later one reflects the average mechanical property, namely strength.
出处
《无机材料学报》
SCIE
EI
CAS
CSCD
北大核心
2002年第1期105-110,共6页
Journal of Inorganic Materials
关键词
自增韧氮化硅
显微结构
力学性能
表征
陶瓷材料
in-situ toughened Si3N4
microstructure
characterization
mechanical property