摘要
对氯化螺磷进行了催化合成研究 .研究结果表明 ,采用 Al Cl3作催化剂 ,和已报道的专利相比 ,可使 POCl3:C( COH) 4( mol比 )从 5.5降到 4 ,时间节省 50 %以上 ,反应温度从 1 1 0℃降到 50℃ .
In this paper,the study of catalytic synthesis of dichloropentate is introduced.Results show that,with AlCl 3 used as the catalyst,the reaction time is reduced by 50% and the reaction temperature is dropped from 110℃ to 50℃,making the ratio of POCl 3 to C(COH) 4(mol ratio) decrease from 5.5 to 4.
出处
《内蒙古工业大学学报(自然科学版)》
2001年第1期14-18,共5页
Journal of Inner Mongolia University of Technology:Natural Science Edition