摘要
本文采用氯气与环己烷直接反应的方法 ,制得了一氯代环己烷 ,并着重讨论了温度、物料配比、不同光源对收率的影响 ,得出了适宜的反应条件 :温度为 40℃ ,环己烷与氯气摩尔比为 4∶1,光照采用蓝光 ,收率为 83 % ,纯度为 98%
A method for direct conversion of cyclohexane and chlorine to monochlorocyclohexane is described in the article.The influences of reaction temperature,mole ratio of matarials and different lights were investigated.The reaction suitable conditions are follows:reation temperature is 40℃,mole ratio of cyclohexane and chlorine is 4∶1,the light is blue,the yield is 98%.
出处
《化学工程师》
CAS
2001年第4期17-18,共2页
Chemical Engineer