摘要
建立了高效液相色谱法测定虫草灵芝圣酒中腺苷含量的方法。在SulpelcosilLC 18 DB色谱柱 (15 0mm× 4 6mmi d ,5 μm)上 ,以 V(乙腈 ) ∶V(水 ) =4 ∶ 96为流动相 ,检测波长2 60nm ,腺苷的检出限为 0 62 6ng。成功地测定了不同批号虫草灵芝圣酒中腺苷的含量 ,平均回收率为 10 1%。分析方法灵敏、准确 。
In this paper, an HPLC method for the determination of adenosine in Chongcao (Cordyceps sinensis) Lingchi (Ganoderma lucidum) liqueur was established The determination was performed on a supelcosil LC 18 DB column (150?mm×4 6?mm i d , 5μm) with acetonitrile water (4∶96, v/v) as mobile phase Set the determination wavelength at 260?nm The determination limit was 0 626?ng Adenosine contents in different batches of Chongcao Lingchi liqueur were determined successfully, the average recovery was 101% The proposed method was sensitive, accurate and precise
出处
《食品与发酵工业》
CAS
CSCD
北大核心
2001年第9期63-65,共3页
Food and Fermentation Industries
关键词
高效液相色谱法
虫草灵芝圣酒
腺苷含量
测定
药酒
high performance liquid chromatography, Chongcao Lingchi liqueur, adenosine
