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N-氯代丁二酰亚胺的合成工艺改进 被引量：1

Technological Study of N-Chloro-Succimide Synthesis
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摘要 Using succimide (NHS) and chlorine as the raw materials, N Chloro succimide was synthesized by the substitution reaction. The effects of catalyst, mole ratio of the raw materials and reaction temperature on the reaction were studied, and the optimal experimental conditions were obtained. Using succimide (NHS) and chlorine as the raw materials, N Chloro succimide was synthesized by the substitution reaction. The effects of catalyst, mole ratio of the raw materials and reaction temperature on the reaction were studied, and the optimal experimental conditions were obtained.
作者 杨锦飞 刘云山
机构地区 南京师范大学化学与环境科学学院
出处 《中国药科大学学报》 CAS CSCD 北大核心 2001年第5期396-397,共2页 Journal of China Pharmaceutical University
关键词 N-氯代丁二酰亚胺 合成 氯化剂 工艺改进 N Chloro succimide Synthesis
分类号 R914 [医药卫生—药物化学]
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参考文献4

  • 1彭卫红 成本诚.关于α-卤代羧酸的应用研究[J].湖南化工,1986,1:24-24.
  • 2中国商品大辞典编辑委员会.中国商品大辞典化学试剂分册[M].北京:中国商业出版社,1994.225.
  • 3中国商品大辞典编委会，中国商品大辞典化学试剂分册，1994年，225页
  • 4彭卫红，湖南化工，1986年，1卷，24页

同被引文献21

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  • 3Schlama T, Mioskowski A, et al. Tetraethylammonium trichloride: A vsertile reagent for chlorinations and oxidations[J]. Angew Chem Int Ed, 1997,36(21):2342.
  • 4Kabalka G W, Yang K. Bromination of alkynes with sodium perporate and sodium bromide[J].Synth Commun, 1998,28(20): 3807 - 3809.
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  • 6Masuda H S, Takasc K O, Niahio M, et al. A new synthetic method of preparing iodohydrin and bromohydrin derivatives through in situ generation of hypohalous acids from H5 IO6 and NaBrO3 in the presence of NaiSO3 [J]. J Org Chem, 1994,59(19):5550-5555.
  • 7Strzalko T, Seyden- penne J, Wartski L, et al. Effect of aggregation of nitrile anions on the 1,2 versus 1,4 regioselectivity towards benzylideneacetone [J]. Tetrahedron Letters, 1994,35(23) :3935 - 3936.
  • 8Kumaraswamy S, Selvik S, Swamy K C. Synthesis of new α-hydroxy-α-halogeno and vinylphosphonates derived from 5,5-dimethyl-1,3,2-dioxaphosphinan-2-one[J]. Synthesis, 1997, (2) :207 -212.
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  • 10Jiling Huang, Quiqian Huang, YangLong Qian. Chlorination of differentially ringsubstituted titanocene complex by SO2Cl2/SOCl2 and X-my structure of chlorinated product [ C5 H4 (C2H5) 2-C6H2-3-Cl-5-Cl-2-o] TiCl2[J].Polyhedron, 1998,17(15) :2523.

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中国药科大学学报
2001年 第5期

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