摘要
根据溶剂效应 ,选择合适的溶剂 ,合成了 2 ,4 ,8,1 0 -四氯 -1 2 H-双苯并 [d,g][1 ,3 ,2 ]-二氧磷杂硫代磷酰氯 ,首次合成并纯化得到了 2 ,4 ,8,1 0 -四氯 -1 2 H-双苯并 [d,g][1 ,3 ,2
On the basis of agent effects in chemical reactions the synthesis of 6 chloro 2,4,8,10 terachloro 12[WT5BX]H dibenzo[d,g][1,3,2]dioxaphosphocin 6 sulfide was achieved with high yields from 2,2′ methylene bis[3,5 dichloro phenol]([ST5HZ]1) and thiophlsphoryl chloride by adopting suitable agents; the cyclization product of [ST5HZ]1 with phosphorus oxychloride has been prepared and purified at the first time.
出处
《合成化学》
CAS
CSCD
2001年第3期277-279,共3页
Chinese Journal of Synthetic Chemistry
