摘要
介绍了标题化合物的合成方法。以乙酰乙酸乙酯为起始原料,经一锅法反应合成了目标化合物,并经MS和1H NMR对其结构进行了表征。本合成路线原料易得、操作简便且收率较高,适合于工业化生产。反应总收率86%。
In the paper, we introduced a approach to synthetize the title compound, was realized and manufactured from ethyl acetoacetate via two steps. Its structure was verified by MS and JH NMR. This synthetic route has the advantages of convenient operation and mild reaction conditions. The total product yield was 86%. This program is suitable for industrial production.
出处
《广东化工》
CAS
2014年第8期15-15,14,共2页
Guangdong Chemical Industry
基金
贵州省中药现代化项目
合同编号:黔科合中药字[2010]5022号
贵州省教育厅自然科学课题
合同编号:黔教合KY字[2012]044号
贵州省高层次人才科研条件特助经费项目
合同编号:TZJF-2010年-055号
