摘要
本文介绍了臭氧氧化、亚硫酸钠还原生产洋茉莉醛反应条件的优化选择试验。按照所选择的优化条件进行的重复试验,洋茉莉醛的平均收率为93.6％。这一收率接近于以臭氧氧化、二甲基硫醚还原的收率(96.0％)。本文最后还对优化条件进行了讨论。
This paper introduces the test of the best reaction condition's selection producing pipcroaal with O_3 as oxidizer and Na_2SO_3 as reducing agent. According to the selected best reaction conditions repeated experiments have been made and the average yield ratio of piperonal amounts to 93.6 percent. The yield ratio approaches that with O_3 as oxidizer and (CH_3)_2 S as reducing agent.The selected best reaction conditions are discussed in this. paper.
出处
《广州化工》
CAS
1991年第2期17-23,34,共7页
GuangZhou Chemical Industry
